CN104352385A - anti aging serum - Google Patents
anti aging serum Download PDFInfo
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- CN104352385A CN104352385A CN201410559124.3A CN201410559124A CN104352385A CN 104352385 A CN104352385 A CN 104352385A CN 201410559124 A CN201410559124 A CN 201410559124A CN 104352385 A CN104352385 A CN 104352385A
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Abstract
Description
技术领域 technical field
本发明属于日化产品技术领域,尤其涉及一种抗衰老精华液。 The invention belongs to the technical field of daily chemical products, and in particular relates to an anti-aging essence. the
背景技术 Background technique
人体的老化是生命生长的必然规律,其中以皮肤的变化最为明显,一般女性在25岁以后,皮肤呈下滑趋势,30岁之后,衰老初现端倪。皮肤衰老是指皮肤表面粗糙和出现皱纹。 The aging of the human body is an inevitable law of life growth, among which the changes in the skin are the most obvious. Generally, after the age of 25, the skin of women shows a downward trend, and after the age of 30, the signs of aging begin to appear. Skin aging is the appearance of rough and wrinkled skin surfaces.
具体而言,皮肤衰老的形式主要为自然衰老(即内源性衰老)和光老化(即外源性衰老),自然衰老主要由机体遗传因素引起,限于全身部位,明显特征为皱纹和松弛,并出现色素沉着等现象。光老化主要是紫外线损害累积所致的皮肤衰老,是自然衰老和紫外线照射共同作用的结果,限于皮肤暴露部位,主要特征为皮肤粗糙无光泽,走稳加粗加深,色素沉着加深,皮肤微循环变差,弹性组织变形,表皮表现为清除力、胶原蛋白和弹性蛋白合成能力及免疫力下降,真皮厚度变薄、易发生过敏发炎等现象。 Specifically, the forms of skin aging are mainly natural aging (i.e. endogenous aging) and photoaging (i.e. exogenous aging). Natural aging is mainly caused by genetic factors of the body and is limited to the whole body. Pigmentation and other phenomena appear. Photoaging is mainly skin aging caused by the accumulation of ultraviolet damage. It is the result of the combined action of natural aging and ultraviolet radiation. It is limited to the exposed parts of the skin. Deterioration, elastic tissue deformation, epidermis manifests as debridement, collagen and elastin synthesis ability and immunity decrease, dermis thickness becomes thinner, prone to allergies and inflammation and other phenomena.
本发明旨在提供一种抗衰老精华液,其对肌肤能够养颜防衰老,促进新陈代谢,活化肌肤细胞,改善微循环,增加皮肤紧密度。 The present invention aims to provide an anti-aging essence, which can nourish skin and prevent aging, promote metabolism, activate skin cells, improve microcirculation and increase skin tightness.
发明内容 Contents of the invention
本发明的目的在于:提供一种抗衰老精华液,其对肌肤能够养颜防衰老,促进新陈代谢,活化肌肤细胞,改善微循环,增加皮肤紧密度。 The object of the present invention is to provide an anti-aging essence, which can nourish the skin and prevent aging, promote metabolism, activate skin cells, improve microcirculation, and increase skin tightness.
为了达到上述目的,本发明采用如下技术方案: In order to achieve the above object, the present invention adopts following technical scheme:
抗衰老精华液,按质量百分比计,其包括以下组分: Anti-aging essence, by mass percentage, it includes the following components:
A组分:甘油5%~10%,汉生胶1%~10%和去离子水55%~75%; Component A: 5%-10% glycerin, 1%-10% xanthan gum and 55%-75% deionized water;
B组分:甘油硬脂酸酯1.0%~3.0%,生育酚乙酸酯1.0%~3.0%,聚二甲基硅氧烷1.0%~3.0%,泛醇0.05%~0.5%,精油0.01%~0.15%和丙烯酸羟乙酯-丙烯酰二甲基牛磺酸钠共聚物0.5%~3.0%; Component B: Glyceryl Stearate 1.0%-3.0%, Tocopheryl Acetate 1.0%-3.0%, Dimethicone 1.0%-3.0%, Panthenol 0.05%-0.5%, Essential Oil 0.01% ~0.15% and 0.5%~3.0% of hydroxyethyl acrylate-sodium acryloyldimethyl taurate copolymer;
C组分:保湿剂1.0%~3.0%,朝鲜蓟提取物1.0%~3.0%,益母草提取物1.0%~3.0%,角鲨烷1%~10%,烟酰胺0.5%~2.0%和防腐剂0.1%~0.6%。 Component C: humectant 1.0%-3.0%, artichoke extract 1.0%-3.0%, motherwort extract 1.0%-3.0%, squalane 1%-10%, niacinamide 0.5%-2.0%, and preservatives 0.1% to 0.6%.
其中,甘油具有滋润皮肤、防止干裂的作用,汉生胶又叫黄原胶,其具有低浓度高粘度的特性(1%水溶液的粘度相当于明胶的100倍),是一种高效的增稠剂;而且其对不溶性固体和油滴具有良好的悬浮作用。黄原胶溶胶分子能形成超结合带状的螺旋共聚体,构成脆弱的类似胶的网状结构,所以能够支持固体颗粒、液滴和气泡的形态,显示出很强的乳化稳定作用和高悬浮能力。此外,其在水中能快速溶解,有很好的水溶性。特别在冷水中也能溶解,可省去繁杂的加工过程,使用方便。 Among them, glycerin has the effect of moisturizing the skin and preventing cracking. Xanthan gum, also known as xanthan gum, has the characteristics of low concentration and high viscosity (the viscosity of 1% aqueous solution is equivalent to 100 times that of gelatin), and is an efficient thickener. agent; and it has a good suspending effect on insoluble solids and oil droplets. Xanthan gum sol molecules can form super-bonded ribbon-shaped helical copolymers to form a fragile glue-like network structure, so they can support the shape of solid particles, liquid droplets and air bubbles, showing strong emulsification stability and high suspension ability. In addition, it can quickly dissolve in water and has good water solubility. In particular, it can be dissolved in cold water, which can save complicated processing and is convenient to use.
甘油硬脂酸酯具有很强的乳化性能,且稳定性高,从而提高精华液的均匀性和稳定性,本身安全、无毒,对人体无害;生育酚乙酸酯即维生素E,它是一种脂溶性维生素,是最主要的抗氧化剂之一。维生素E可有效对抗自由基,抑制过氧化脂质生成,祛除黄褐斑;抑制酪氨酸酶的活性,从而减少黑色素生成。酯化形式的维生素E还能消除由紫外线、空气污染等外界因素造成的过多的氧自由基,起到延缓光老化、预防晒伤和抑制日晒红斑生成等作用。 Glyceryl stearate has strong emulsifying properties and high stability, thereby improving the uniformity and stability of the essence. It is safe, non-toxic, and harmless to the human body; tocopheryl acetate is vitamin E, which is A fat-soluble vitamin that is one of the most important antioxidants. Vitamin E can effectively fight against free radicals, inhibit the production of lipid peroxide, and remove chloasma; inhibit the activity of tyrosinase, thereby reducing melanin production. The esterified form of vitamin E can also eliminate excessive oxygen free radicals caused by external factors such as ultraviolet rays and air pollution, and play a role in delaying photoaging, preventing sunburn, and inhibiting the formation of sunburn erythema.
聚二甲基硅氧烷与多种组分有高度的相容性,可降低产品的粘腻感。泛醇,即维生素B5,其是一种保湿剂和柔软剂,易氧化,能够促进皮肤正常角化,促进伤口愈合和皮肤组织修复,刺激细胞分裂再生,对促进疤痕愈合非常有效。丙烯酸羟乙酯-丙烯酰二甲基牛磺酸钠共聚物则作为增稠剂使用。 Polydimethylsiloxane is highly compatible with various components and can reduce the stickiness of the product. Panthenol, vitamin B5, is a moisturizer and softener, easy to oxidize, can promote normal keratinization of the skin, promote wound healing and skin tissue repair, stimulate cell division and regeneration, and is very effective in promoting scar healing. Hydroxyethyl acrylate-sodium acryloyldimethyl taurate copolymer is used as a thickener.
朝鲜蓟提取物中含有多酚化合物,这些多酚化合物具有较强的氧化性,从而具有抗衰老的功效,而且朝鲜蓟提取物中的绿原酸、洋蓟酸、木樨草素-7-芸香糖苷以及菜蓟糖苷具有较高的抗微生物、抗真菌和抗细菌活性;益母草提取物具有益颜美容、抗衰防老的功效。 Artichoke extract contains polyphenolic compounds, which have strong oxidative properties, thus having anti-aging effects, and chlorogenic acid, cynic acid, luteolin-7-rutacein in artichoke extract Glycosides and artichoke glycosides have high antimicrobial, antifungal and antibacterial activities; Motherwort extract has the effects of beautifying, anti-aging and anti-aging.
角鲨烷对皮肤具有较好的亲和性,滋润而不油腻,保湿性强,具有抗皱的功效,而且能够抑制皮肤脂质的过氧化,有效地深入肌肤,促进皮肤基底细胞的增殖,对延缓皮肤老化,改善并消除黄褐斑具有明显的生理效果。而且其还能使皮肤的毛孔张开,促进血液微循环,增进细胞的新陈代谢,帮助修复破损细胞;其还能加强修复表皮,有效形成天然保护膜,帮助肌肤与皮脂间的平衡,不会引起过敏和刺激,并能加速配方中其他活性成分向皮肤中渗透,纯净、无色、无异味。 Squalane has good affinity to the skin, moisturizing but not greasy, strong moisturizing, has anti-wrinkle effect, and can inhibit the peroxidation of skin lipids, effectively penetrate into the skin, promote the proliferation of skin basal cells, Delaying skin aging, improving and eliminating chloasma has obvious physiological effects. Moreover, it can also open the pores of the skin, promote blood microcirculation, increase cell metabolism, and help repair damaged cells; it can also strengthen the repair of the epidermis, effectively form a natural protective film, and help the balance between the skin and sebum without causing skin irritation. Allergy and irritation, and can accelerate the penetration of other active ingredients in the formula into the skin, pure, colorless, and odorless.
烟酰胺即维生素PP,是一种水溶性维生素,其能减轻和预防皮肤在早期衰老过程中产生的肤色黯淡、发黄、菜色。烟酰胺还可以修复受损的角质层脂质屏障,提高皮肤抵抗力。烟酰胺还具有深层锁水功效,所以,含有烟酰胺的护肤品对都有极强的锁水、保湿功效。 Niacinamide, vitamin PP, is a water-soluble vitamin that can reduce and prevent dull, yellow, and disheveled skin in the early aging process. Niacinamide can also repair the damaged stratum corneum lipid barrier and improve skin resistance. Niacinamide also has a deep water-locking effect, so skin care products containing niacinamide have strong water-locking and moisturizing effects.
作为本发明抗衰老精华液的一种改进,按质量百分比计,其包括以下组分: As an improvement of the anti-aging essence of the present invention, it includes the following components by mass percentage:
A组分:甘油6%~8%,汉生胶2%~8%和去离子水60%~70%; Component A: 6%-8% glycerin, 2%-8% xanthan gum and 60%-70% deionized water;
B组分:甘油硬脂酸酯1.2%~2.0%,生育酚乙酸酯1.2%~2.0%,聚二甲基硅氧烷1.5%~2.5%,泛醇0.1%~0.3%,精油0.05%~0.12%和丙烯酸羟乙酯-丙烯酰二甲基牛磺酸钠共聚物0.7%~1.5%; Component B: Glyceryl Stearate 1.2%-2.0%, Tocopheryl Acetate 1.2%-2.0%, Dimethicone 1.5%-2.5%, Panthenol 0.1%-0.3%, Essential Oil 0.05% ~0.12% and 0.7%~1.5% of hydroxyethyl acrylate-sodium acryloyldimethyl taurate copolymer;
C组分:保湿剂1.5%~2.5%,朝鲜蓟提取物1.5%~2.5%,益母草提取物1.5%~2.5%,角鲨烷2%~8%,烟酰胺0.7%~1.5%和防腐剂0.2%~0.5%。 Component C: humectant 1.5%-2.5%, artichoke extract 1.5%-2.5%, motherwort extract 1.5%-2.5%, squalane 2%-8%, niacinamide 0.7%-1.5% and preservatives 0.2% to 0.5%.
作为本发明抗衰老精华液的一种改进,按质量百分比计,其包括以下组分: As an improvement of the anti-aging essence of the present invention, it includes the following components by mass percentage:
A组分:甘油7%,汉生胶3.2%和去离子水59.3%; Component A: 7% glycerin, 3.2% xanthan gum and 59.3% deionized water;
B组分:甘油硬脂酸酯1.5%,生育酚乙酸酯15%,聚二甲基硅氧烷2.0%,泛醇0.2%,精油0.10%和丙烯酸羟乙酯-丙烯酰二甲基牛磺酸钠共聚物1.0%; Component B: Glyceryl Stearate 1.5%, Tocopheryl Acetate 15%, Dimethicone 2.0%, Panthenol 0.2%, Essential Oil 0.10% and Hydroxyethyl Acrylate-Acryloyl Dimethyl Bovine Sodium sulfonate copolymer 1.0%;
C组分:保湿剂2.0%,朝鲜蓟提取物2.0%,益母草提取物2.0%,角鲨烷3.2%,烟酰胺1.2%和防腐剂0.3%。 Component C: Humectant 2.0%, Artichoke Extract 2.0%, Motherwort Extract 2.0%, Squalane 3.2%, Niacinamide 1.2% and Preservative 0.3%.
作为本发明抗衰老精华液的一种改进,B组分中,精油为玫瑰精油、天竺葵精油和熏衣草精油中的至少一种。其中,玫瑰精油具有很好的美容护肤作用,能以内养外淡化斑点,促进黑色素分解,加速养份与水份的平衡,强化细胞毒素的排出,从而达到对皮肤内外环境的整体调节与控制,改善皮肤干燥,恢复皮肤弹性,让女性拥有白皙、充满弹性的健康肌肤;其还具有抗老、防皱及保湿功效。天竺葵精油能平衡皮脂分泌,使皮肤饱满,对松垮、毛孔阻塞及油性皮肤也很好,且能促进血液循环,使苍白的皮肤较为红润有活力。熏衣草精油可以清热解毒,清洁皮肤,控制油分,祛斑美白,祛皱嫩肤、祛除眼袋黑眼圈,还可促进受损组织再生恢复。 As an improvement of the anti-aging essence of the present invention, in component B, the essential oil is at least one of rose essential oil, geranium essential oil and lavender essential oil. Among them, rose essential oil has a very good beauty and skin care effect. It can dilute spots by nourishing the inside and outside, promote the decomposition of melanin, accelerate the balance of nutrients and water, and strengthen the discharge of cytotoxins, so as to achieve the overall regulation and control of the internal and external environment of the skin. Improves dry skin, restores skin elasticity, and allows women to have white, elastic and healthy skin; it also has anti-aging, anti-wrinkle and moisturizing effects. Geranium essential oil can balance sebum secretion, make skin plump, and is also good for loose, clogged pores and oily skin, and can promote blood circulation, making pale skin more rosy and energetic. Lavender essential oil can clear away heat and detoxify, cleanse the skin, control oil content, remove freckles, whiten skin, remove wrinkles and rejuvenate skin, remove eye bags and dark circles, and promote the regeneration and recovery of damaged tissues.
作为本发明抗衰老精华液的一种改进,C组分中,所述保湿剂为木糖醇葡萄糖苷、脱水木糖醇和木糖醇的混合物,三者的质量比例为(0.3~3)(0.5~4):1。 As an improvement of the anti-aging essence of the present invention, in component C, the moisturizer is a mixture of xylitol glucoside, anhydroxylitol and xylitol, and the mass ratio of the three is (0.3-3) ( 0.5~4): 1.
作为本发明抗衰老精华液的一种改进,所述防腐剂为苯氧乙醇、羟苯甲酯、羟苯乙酯和汉生胶中的至少一种。采用天然植物来源的木糖醇葡萄糖苷、脱水木糖醇和木糖醇,能有效保湿和重建皮肤结构体系,促进神经酰胺合成,加强皮肤屏障作用,减少水份流失。 As an improvement of the anti-aging essence of the present invention, the preservative is at least one of phenoxyethanol, methylparaben, ethylparaben and xanthan gum. Using natural plant-derived xylitol glucoside, anhydroxylitol and xylitol, it can effectively moisturize and rebuild the skin structure system, promote the synthesis of ceramide, strengthen the skin barrier function, and reduce water loss.
相对于现有技术,本发明的活性成分中,朝鲜蓟提取物具有抗衰老和抗菌的作用,益母草提取物则具有益颜美容、抗衰防老的功效,而角鲨烷则具有抗皱的功效,而且能够抑制皮肤脂质的过氧化,有效地深入肌肤,促进皮肤基底细胞的增殖,对延缓皮肤老化,改善并消除黄褐斑具有明显的生理效果,再加上烟酰胺和生育酚等维生素共同配伍,相互协调增效,可以有效地增进微循环,促进新陈代谢,增加细胞间物质交换,从而达到愈合更新细胞,促进细胞生长,活化肌肤细胞,有效活化滋润肌肤的作用,同时还可有效对抗自由基,抑制过氧化脂质生成,祛除黄褐斑,延缓衰老;烟酰胺的深层锁水功效加上角鲨烷强大的保湿能力使得本发明具有很好的保湿效果。长期使用本发明的精华液,皱纹明显变浅,皮肤变得水润、紧致,有弹性。 Compared with the prior art, among the active ingredients of the present invention, artichoke extract has anti-aging and antibacterial effects, motherwort extract has the effects of beautifying, anti-aging and anti-aging, and squalane has anti-wrinkle effects. Moreover, it can inhibit the peroxidation of skin lipids, effectively penetrate into the skin, promote the proliferation of skin basal cells, and have obvious physiological effects on delaying skin aging, improving and eliminating chloasma, together with vitamins such as niacinamide and tocopherol Compatibility, mutual coordination and synergy, can effectively enhance microcirculation, promote metabolism, increase the exchange of substances between cells, so as to heal and renew cells, promote cell growth, activate skin cells, effectively activate and moisturize the skin, and at the same time effectively fight against freedom base, inhibit the generation of lipid peroxide, remove chloasma, and delay aging; the deep water-locking effect of niacinamide and the strong moisturizing ability of squalane make the present invention have a good moisturizing effect. Long-term use of the essence of the present invention will obviously lighten wrinkles, and the skin will become hydrated, firm and elastic.
本发明还提供了一种抗衰老精华液的制备方法,包括以下步骤: The present invention also provides a preparation method of anti-aging essence, comprising the following steps:
第一步,把A组分投入真空乳化锅中,搅拌加热至80~85℃,均质3~9分钟,保温20~30分钟后降温; In the first step, put component A into a vacuum emulsification pot, stir and heat to 80-85°C, homogenize for 3-9 minutes, keep warm for 20-30 minutes and then cool down;
第二步,降温至45~55℃后边搅拌边加入B组分,真空均质3~9分钟; In the second step, cool down to 45-55°C, add component B while stirring, and homogenize in vacuum for 3-9 minutes;
第三步,加入C组分,真空搅拌均匀,料体无异常出料,即得抗衰老精华液。 The third step is to add component C, stir evenly under vacuum, and the material body is discharged without abnormality, and the anti-aging essence is obtained.
该方法操作简单,易于实现,而且得到的产品的感官和理化指标均符合我国润肤乳行业标准要求。 The method is simple to operate and easy to realize, and the sensory and physical and chemical indexes of the obtained product all meet the standard requirements of the skin care milk industry in my country.
具体实施方式 Detailed ways
以下将结合具体实施例对本发明及其有益效果作进一步详细的说明,但是,本发明的具体实施方式并不局限于此。 The present invention and its beneficial effects will be further described in detail below in conjunction with specific examples, however, the specific embodiments of the present invention are not limited thereto.
实施例1 Example 1
本实施例提供的抗衰老精华液,按质量百分比计,其包括以下组分: The anti-aging essence provided by the present embodiment, by mass percentage, it comprises the following components:
A组分:甘油7%,汉生胶3.2%和去离子水59.3%; Component A: 7% glycerin, 3.2% xanthan gum and 59.3% deionized water;
B组分:甘油硬脂酸酯1.5%,生育酚乙酸酯15%,聚二甲基硅氧烷2.0%,泛醇0.2%,玫瑰精油0.10%和丙烯酸羟乙酯-丙烯酰二甲基牛磺酸钠共聚物1.0%; Component B: Glyceryl Stearate 1.5%, Tocopheryl Acetate 15%, Dimethicone 2.0%, Panthenol 0.2%, Rose Essential Oil 0.10%, and Hydroxyethyl Acrylate-Acryloyldimethyl Sodium taurine copolymer 1.0%;
C组分:木糖醇葡萄糖苷0.5%,脱水木糖醇1%,木糖醇0.5%,朝鲜蓟提取物2.0%,益母草提取物2.0%,角鲨烷3.2%,烟酰胺1.2%和苯氧乙醇0.3%。 Component C: xylitol glucoside 0.5%, anhydroxylitol 1%, xylitol 0.5%, artichoke extract 2.0%, motherwort extract 2.0%, squalane 3.2%, niacinamide 1.2% and benzene Oxygen ethanol 0.3%.
其制备方法包括以下步骤: Its preparation method comprises the following steps:
第一步,把A组分投入真空乳化锅中,搅拌加热至82℃,均质4分钟,保温25分钟后降温; In the first step, put component A into a vacuum emulsification pot, stir and heat to 82°C, homogenize for 4 minutes, keep warm for 25 minutes and then cool down;
第二步,降温至50℃后边搅拌边加入B组分,真空均质6分钟; In the second step, after cooling down to 50°C, add component B while stirring, and homogenize under vacuum for 6 minutes;
第三步,加入C组分,真空搅拌均匀,降温至40℃料体无异常出料,即得抗衰老精华液。 The third step is to add component C, stir evenly under vacuum, cool down to 40°C, and the material body will be discharged without abnormality, and then the anti-aging essence will be obtained.
实施例2 Example 2
本实施例提供的抗衰老精华液,按质量百分比计,其包括以下组分: The anti-aging essence provided by the present embodiment, by mass percentage, it comprises the following components:
A组分:甘油5%,汉生胶5.3%和去离子水68.48%; Component A: glycerin 5%, xanthan gum 5.3% and deionized water 68.48%;
B组分:甘油硬脂酸酯2%,生育酚乙酸酯1.5%,聚二甲基硅氧烷1.8%,泛醇0.3%,天竺葵精油0.12%和丙烯酸羟乙酯-丙烯酰二甲基牛磺酸钠共聚物2.5%; Component B: Glyceryl Stearate 2%, Tocopheryl Acetate 1.5%, Dimethicone 1.8%, Panthenol 0.3%, Geranium Essential Oil 0.12%, and Hydroxyethyl Acrylate-Acryloyl Dimethicone Sodium taurine copolymer 2.5%;
C组分:木糖醇葡萄糖苷0.6%、脱水木糖醇0.6%和木糖醇0.6%,朝鲜蓟提取物2.5%,益母草提取物1.5%,角鲨烷6.5%,烟酰胺1.5%和苯氧乙醇0.2%。 Component C: xylitol glucoside 0.6%, anhydroxylitol 0.6% and xylitol 0.6%, artichoke extract 2.5%, motherwort extract 1.5%, squalane 6.5%, niacinamide 1.5% and benzene Oxygen ethanol 0.2%.
其制备方法包括以下步骤: Its preparation method comprises the following steps:
第一步,把A组分投入真空乳化锅中,搅拌加热至80℃,均质5分钟,保温20分钟后降温; In the first step, put component A into a vacuum emulsification pot, stir and heat to 80°C, homogenize for 5 minutes, keep warm for 20 minutes and then cool down;
第二步,降温至45℃后边搅拌边加入B组分,真空均质7分钟; In the second step, after cooling down to 45°C, add component B while stirring, and homogenize in vacuum for 7 minutes;
第三步,加入C组分,真空搅拌均匀,降温至37℃料体无异常出料,即得抗衰老精华液。 The third step is to add component C, stir evenly under vacuum, cool down to 37°C, and the material body will not be discharged abnormally, and then the anti-aging essence will be obtained.
实施例3 Example 3
本实施例提供的抗衰老精华液,按质量百分比计,其包括以下组分: The anti-aging essence provided by the present embodiment, by mass percentage, it comprises the following components:
A组分:甘油3%,汉生胶5%和去离子水72.57%; Component A: 3% glycerin, 5% xanthan gum and 72.57% deionized water;
B组分:甘油硬脂酸酯2.5%,生育酚乙酸酯1.2%,聚二甲基硅氧烷2.6%,泛醇0.25%,熏衣草精油0.08%和丙烯酸羟乙酯-丙烯酰二甲基牛磺酸钠共聚物1.3%; Component B: Glyceryl Stearate 2.5%, Tocopheryl Acetate 1.2%, Dimethicone 2.6%, Panthenol 0.25%, Lavender Essential Oil 0.08%, and Hydroxyethyl Acrylate-Acryloyl Dimethicone Sodium methyl taurate copolymer 1.3%;
C组分:木糖醇葡萄糖苷0.5%、脱水木糖醇0.7%和木糖醇1.0%,朝鲜蓟提取物2.0%,益母草提取物2.0%,角鲨烷4.5%,烟酰胺0.6%和羟苯乙酯0.2%。 Component C: xylitol glucoside 0.5%, anhydroxylitol 0.7% and xylitol 1.0%, artichoke extract 2.0%, motherwort extract 2.0%, squalane 4.5%, niacinamide 0.6% and hydroxyl Phenyl ethyl ester 0.2%.
其制备方法包括以下步骤: Its preparation method comprises the following steps:
第一步,把A组分投入真空乳化锅中,搅拌加热至85℃,均质9分钟,保温30分钟后降温; In the first step, put component A into a vacuum emulsification pot, stir and heat to 85°C, homogenize for 9 minutes, keep warm for 30 minutes and then cool down;
第二步,降温至55℃后边搅拌边加入B组分,真空均质3分钟; In the second step, after cooling down to 55°C, add component B while stirring, and homogenize in vacuum for 3 minutes;
第三步,加入C组分,真空搅拌均匀,降温至35℃料体无异常出料,即得抗衰老精华液。 The third step is to add component C, stir evenly under vacuum, cool down to 35°C, and the material body will be discharged without abnormality, and then the anti-aging essence will be obtained.
对实施例1至3的抗衰老精华液进行性能测试: Carry out performance test to the anti-aging essence of embodiment 1 to 3:
(1)感官性能评定:取实施例1至3的抗衰老精华液在室温和非阳光直射下目测观察颗粒是否细腻,色泽是够均匀一致,所得结果见表1。 (1) Evaluation of sensory properties: Take the anti-aging essence of Examples 1 to 3 at room temperature and under direct sunlight to visually observe whether the particles are fine and the color is uniform enough. The results are shown in Table 1.
(2)pH值测试 (2) pH value test
分别称取实施例1至3的抗衰老精华液样品2.0g,放入盛有30mL水的小烧杯中,在40℃下加热溶解。用校正好的pH计测试修复精华溶液的pH值,所得结果见表1。 Weigh 2.0 g of the anti-aging essence samples of Examples 1 to 3 respectively, put them into a small beaker filled with 30 mL of water, and heat to dissolve at 40° C. Test the pH value of the repair essence solution with a calibrated pH meter, and the results are shown in Table 1.
(3)离心实验 (3) Centrifugal experiment
将实施例1至3的抗衰老精华液样品装入10mL的离心式管中,以4000r/min的转速离心30min,观察有无分层现象,所得结果见表1。 Put the anti-aging essence samples of Examples 1 to 3 into a 10mL centrifugal tube, centrifuge at a speed of 4000r/min for 30min, and observe whether there is stratification. The results are shown in Table 1.
(4)耐热、耐寒测试 (4) Heat resistance and cold resistance test
将实施例1至3的抗衰老精华液样品置于40℃的恒温烘箱和-10℃的冰箱冷冻室中,24h后取出,恢复室温后观察是否有分层,沉淀或出水现象,所得结果见表1。 Put the anti-aging essence samples of Examples 1 to 3 in a constant temperature oven at 40°C and in a freezer at -10°C, take them out after 24 hours, and observe whether there is stratification, precipitation or water out after returning to room temperature, the results are shown in Table 1.
(5)吸湿率测试 (5) Moisture absorption test
分别称取实施例1至3的抗衰老精华液样品4.0g,置于直径为3cm的称量瓶中,在室温下,放置在相对湿度为75%的环境中4h,计算4h后的吸湿率。其中,吸湿率=(m终-m始)/m始×100%,其中,m始为放置前待测样品的质量,g;m终为放置4h后样品的质量,g,所得结果见表1。 Weigh 4.0 g of the anti-aging essence samples of Examples 1 to 3 respectively, place them in a weighing bottle with a diameter of 3 cm, place them in an environment with a relative humidity of 75% for 4 hours at room temperature, and calculate the moisture absorption rate after 4 hours . Among them, the moisture absorption rate = (m end - m start ) / m start × 100%, among them, m start is the mass of the sample to be tested before placement, g; m end is the mass of the sample after being placed for 4 hours, g, and the results are shown in the table 1.
表1:实施例1至3的抗衰老精华液的理化指标。 Table 1: Physicochemical indicators of the anti-aging essences of Examples 1 to 3.
the
(6)皮肤试用实验 (6) Skin Trial Experiment
抗衰老测试: Anti-aging test:
1、皮肤弹性测试:测试对象为30为女性,年龄为35岁,身体健康。测试仪器为德国CK公司皮肤弹性测试仪MPA580的Reviscometer RV600(弹性纤维组织测试探头),测五次取平均值。 1. Skin elasticity test: The test subjects are 30 females, aged 35, in good health. The test instrument is the Reviscometer RV600 (elastic fiber tissue test probe) of the skin elasticity tester MPA580 of CK Company in Germany, and the average value is taken after five measurements.
测试条件:(1)室内环境;(2)无强烈阳光或灯光直射;(3)环境温度20±2℃,环境湿度40-60%。 Test conditions: (1) indoor environment; (2) no strong sunlight or direct light; (3) ambient temperature 20±2°C, ambient humidity 40-60%.
测试区域:左颧部。 Test area: Left palate.
测试步骤:先测量被测试区域清洁后30min的空白值(R2、R5、R7),然后规定受试者每天早晚坚持使用实施例1的产品,分别测试1周、2周、3周和4周后测试区域皮肤弹性指数R2、R5、R7值(测试过程中负压恒定为450mbar)。 Test steps: First measure the blank value (R2, R5, R7) of the tested area 30 minutes after cleaning, and then stipulate that the subjects insist on using the product of Example 1 every morning and evening, and test for 1 week, 2 weeks, 3 weeks and 4 weeks respectively The skin elasticity index R2, R5, R7 value of the post-test area (the negative pressure is constant at 450mbar during the test).
指标说明:皮肤弹性指数R2、R5、R7越接近1,皮肤的弹性越好。其中,R2=Ua/Uf;R5=Ur/Ue;R7=Ur/Uf。Uf为皮肤最大拉伸量,Ue为恒定负压加到皮肤上后,0.1s时皮肤的拉伸量,定位弹性部分拉伸量。Ur为取消负压后,皮肤会迅速恢复原状态,同样分为弹性部分值Ur,即取消负压0.1s后,皮肤的恢复值和粘弹性部分值,或称塑形部分值。Ua为从取消负压到下一次连续测试皮肤表面再加负压时皮肤的恢复值,所得结果见表2。 Index Description: The closer the skin elasticity index R2, R5, and R7 are to 1, the better the skin elasticity. Among them, R2=Ua/Uf; R5=Ur/Ue; R7=Ur/Uf. Uf is the maximum stretching amount of the skin, Ue is the stretching amount of the skin at 0.1s after the constant negative pressure is applied to the skin, and the stretching amount of the elastic part is positioned. Ur means that after the negative pressure is removed, the skin will quickly return to its original state. It is also divided into the elastic part value Ur, that is, the recovery value of the skin and the viscoelastic part value, or the plastic part value, after the negative pressure is canceled for 0.1s. Ua is the recovery value of the skin from the cancellation of the negative pressure to the next continuous test on the skin surface when the negative pressure is added. The results are shown in Table 2.
表2:皮肤弹性测试结果 Table 2: Skin Elasticity Test Results
由表2可以看出:使用实施例1的产品4周后,受试者的皮肤弹性指数有了非常大的提升,说明本发明具有较好的抗衰老效果。 It can be seen from Table 2 that after using the product of Example 1 for 4 weeks, the skin elasticity index of the test subject has been greatly improved, indicating that the present invention has a better anti-aging effect.
2、鱼尾纹测试: 2. Crow's feet test:
选择30人作为测试人员,均有明显的鱼尾纹,平均分为3组,3组受试人员的脸部分别试用实施例1至3的抗衰老精华液,每天早晚各使用1次,共用30天,观察试用效果,所得结果见表3。 Select 30 people as testers, all of whom have obvious crow's feet, and divide them into 3 groups on average. The faces of the 3 groups of testees are tested with the anti-aging essence of Examples 1 to 3, and they are used once a day in the morning and evening for 30 days , observe the trial effect, and the results are shown in Table 3.
测试指标:明显的鱼尾纹为×;较浅的鱼尾纹为○;没有鱼尾纹为√; Test indicators: Obvious crow's feet is ×; shallow crow's feet is ○; no crow's feet is √;
测试条件:(1)室内环境;(2)无强烈阳光或灯光直射;(3)环境温度20±2℃,环境湿度40-60%。 Test conditions: (1) indoor environment; (2) no strong sunlight or direct light; (3) ambient temperature 20±2°C, ambient humidity 40-60%.
表3:实施例1至3的抗衰老精华液的鱼尾纹测试结果。 Table 3: Crow's feet test results of the anti-aging serums of Examples 1 to 3.
the
由表3可以看出:本发明具有较好的消除鱼尾纹的效果。 As can be seen from Table 3: the present invention has a better effect of eliminating crow's feet.
根据上述说明书的揭示和教导,本发明所属领域的技术人员还可以对上述实施方式进行适当的变更和修改。因此,本发明并不局限于上面揭示和描述的具体实施方式,对本发明的一些修改和变更也应当落入本发明的权利要求的保护范围内。此外,尽管本说明书中使用了一些特定的术语,但这些术语只是为了方便说明,并不对本发明构成任何限制。 According to the disclosure and teaching of the above specification, those skilled in the art to which the present invention pertains can also make appropriate changes and modifications to the above embodiment. Therefore, the present invention is not limited to the specific embodiments disclosed and described above, and some modifications and changes to the present invention should also fall within the protection scope of the claims of the present invention. In addition, although some specific terms are used in this specification, these terms are only for convenience of description and do not constitute any limitation to the present invention.
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