CN102640755A - Insecticidal and acaricidal composition - Google Patents
Insecticidal and acaricidal composition Download PDFInfo
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- CN102640755A CN102640755A CN2012100677198A CN201210067719A CN102640755A CN 102640755 A CN102640755 A CN 102640755A CN 2012100677198 A CN2012100677198 A CN 2012100677198A CN 201210067719 A CN201210067719 A CN 201210067719A CN 102640755 A CN102640755 A CN 102640755A
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- CN
- China
- Prior art keywords
- difenoconazole
- acid amides
- rice blast
- bactericide
- parts
- Prior art date
- Legal status (The legal status is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the status listed.)
- Pending
Links
- 239000000203 mixture Substances 0.000 title claims abstract description 15
- 230000000895 acaricidal effect Effects 0.000 title abstract 2
- 230000000749 insecticidal effect Effects 0.000 title abstract 2
- 235000007164 Oryza sativa Nutrition 0.000 claims abstract description 26
- 235000009566 rice Nutrition 0.000 claims abstract description 26
- 239000005760 Difenoconazole Substances 0.000 claims abstract description 12
- 239000003899 bactericide agent Substances 0.000 claims abstract description 12
- BQYJATMQXGBDHF-UHFFFAOYSA-N difenoconazole Chemical compound O1C(C)COC1(C=1C(=CC(OC=2C=CC(Cl)=CC=2)=CC=1)Cl)CN1N=CN=C1 BQYJATMQXGBDHF-UHFFFAOYSA-N 0.000 claims abstract description 12
- 150000003852 triazoles Chemical class 0.000 claims abstract description 8
- 239000000839 emulsion Substances 0.000 claims abstract description 4
- 239000008187 granular material Substances 0.000 claims abstract description 3
- 239000004530 micro-emulsion Substances 0.000 claims abstract description 3
- 239000004562 water dispersible granule Substances 0.000 claims abstract description 3
- 241000209094 Oryza Species 0.000 claims description 25
- 150000001408 amides Chemical class 0.000 claims description 23
- 239000000642 acaricide Substances 0.000 claims description 8
- 239000000843 powder Substances 0.000 claims description 5
- 239000000375 suspending agent Substances 0.000 claims description 5
- 238000009736 wetting Methods 0.000 claims description 5
- 238000009472 formulation Methods 0.000 claims description 3
- FFSJPOPLSWBGQY-UHFFFAOYSA-N triazol-4-one Chemical compound O=C1C=NN=N1 FFSJPOPLSWBGQY-UHFFFAOYSA-N 0.000 claims description 3
- 239000004480 active ingredient Substances 0.000 claims description 2
- 230000000844 anti-bacterial effect Effects 0.000 abstract description 6
- XLYOFNOQVPJJNP-UHFFFAOYSA-N water Substances O XLYOFNOQVPJJNP-UHFFFAOYSA-N 0.000 abstract description 5
- 201000010099 disease Diseases 0.000 abstract description 4
- 208000037265 diseases, disorders, signs and symptoms Diseases 0.000 abstract description 4
- 241000209140 Triticum Species 0.000 abstract description 3
- 235000021307 Triticum Nutrition 0.000 abstract description 3
- 230000002195 synergetic effect Effects 0.000 abstract description 3
- 239000004563 wettable powder Substances 0.000 abstract description 3
- 229920000742 Cotton Polymers 0.000 abstract description 2
- 240000008067 Cucumis sativus Species 0.000 abstract description 2
- 241000219146 Gossypium Species 0.000 abstract description 2
- 235000007688 Lycopersicon esculentum Nutrition 0.000 abstract description 2
- 240000003768 Solanum lycopersicum Species 0.000 abstract description 2
- 244000061456 Solanum tuberosum Species 0.000 abstract description 2
- 235000002595 Solanum tuberosum Nutrition 0.000 abstract description 2
- 235000012015 potatoes Nutrition 0.000 abstract description 2
- PXMNMQRDXWABCY-UHFFFAOYSA-N 1-(4-chlorophenyl)-4,4-dimethyl-3-(1H-1,2,4-triazol-1-ylmethyl)pentan-3-ol Chemical compound C1=NC=NN1CC(O)(C(C)(C)C)CCC1=CC=C(Cl)C=C1 PXMNMQRDXWABCY-UHFFFAOYSA-N 0.000 abstract 2
- IUOKJNROJISWRO-UHFFFAOYSA-N N-(2-cyano-3-methylbutan-2-yl)-2-(2,4-dichlorophenoxy)propanamide Chemical compound CC(C)C(C)(C#N)NC(=O)C(C)OC1=CC=C(Cl)C=C1Cl IUOKJNROJISWRO-UHFFFAOYSA-N 0.000 abstract 2
- KAESVJOAVNADME-UHFFFAOYSA-N Pyrrole Chemical compound C=1C=CNC=1 KAESVJOAVNADME-UHFFFAOYSA-N 0.000 abstract 2
- 239000005839 Tebuconazole Substances 0.000 abstract 2
- 235000009849 Cucumis sativus Nutrition 0.000 abstract 1
- 240000007594 Oryza sativa Species 0.000 abstract 1
- 239000002552 dosage form Substances 0.000 abstract 1
- 239000003995 emulsifying agent Substances 0.000 abstract 1
- 239000000945 filler Substances 0.000 abstract 1
- 239000003960 organic solvent Substances 0.000 abstract 1
- 230000002265 prevention Effects 0.000 abstract 1
- 239000000243 solution Substances 0.000 abstract 1
- 239000004094 surface-active agent Substances 0.000 abstract 1
- 239000000725 suspension Substances 0.000 abstract 1
- 235000013311 vegetables Nutrition 0.000 abstract 1
- 239000003814 drug Substances 0.000 description 11
- 230000001154 acute effect Effects 0.000 description 10
- NNPRCLUGHFXSOU-UHFFFAOYSA-N 4-chloro-n-[cyano(ethoxy)methyl]benzamide Chemical compound CCOC(C#N)NC(=O)C1=CC=C(Cl)C=C1 NNPRCLUGHFXSOU-UHFFFAOYSA-N 0.000 description 8
- 229940079593 drug Drugs 0.000 description 6
- 230000000694 effects Effects 0.000 description 6
- 238000002360 preparation method Methods 0.000 description 6
- 239000000126 substance Substances 0.000 description 5
- 239000002131 composite material Substances 0.000 description 4
- JHIVVAPYMSGYDF-UHFFFAOYSA-N cyclohexanone Chemical compound O=C1CCCCC1 JHIVVAPYMSGYDF-UHFFFAOYSA-N 0.000 description 4
- 231100000053 low toxicity Toxicity 0.000 description 4
- IXQGCWUGDFDQMF-UHFFFAOYSA-N o-Hydroxyethylbenzene Natural products CCC1=CC=CC=C1O IXQGCWUGDFDQMF-UHFFFAOYSA-N 0.000 description 4
- -1 phenethyl phenolformaldehyde resin Chemical compound 0.000 description 4
- 230000003449 preventive effect Effects 0.000 description 4
- 230000000638 stimulation Effects 0.000 description 4
- LYCAIKOWRPUZTN-UHFFFAOYSA-N Ethylene glycol Chemical compound OCCO LYCAIKOWRPUZTN-UHFFFAOYSA-N 0.000 description 3
- 241000283973 Oryctolagus cuniculus Species 0.000 description 3
- YXFVVABEGXRONW-UHFFFAOYSA-N Toluene Chemical compound CC1=CC=CC=C1 YXFVVABEGXRONW-UHFFFAOYSA-N 0.000 description 3
- 150000001875 compounds Chemical class 0.000 description 3
- 239000012895 dilution Substances 0.000 description 3
- 238000010790 dilution Methods 0.000 description 3
- 238000002474 experimental method Methods 0.000 description 3
- 239000000463 material Substances 0.000 description 3
- 239000002994 raw material Substances 0.000 description 3
- 239000007921 spray Substances 0.000 description 3
- 231100000820 toxicity test Toxicity 0.000 description 3
- 239000003053 toxin Substances 0.000 description 3
- 235000013305 food Nutrition 0.000 description 2
- 238000004519 manufacturing process Methods 0.000 description 2
- 229920001568 phenolic resin Polymers 0.000 description 2
- 239000011734 sodium Substances 0.000 description 2
- 229910052708 sodium Inorganic materials 0.000 description 2
- PHLBKPHSAVXXEF-UHFFFAOYSA-N trazodone Chemical compound ClC1=CC=CC(N2CCN(CCCN3C(N4C=CC=CC4=N3)=O)CC2)=C1 PHLBKPHSAVXXEF-UHFFFAOYSA-N 0.000 description 2
- 229960003991 trazodone Drugs 0.000 description 2
- 239000005995 Aluminium silicate Substances 0.000 description 1
- 235000010799 Cucumis sativus var sativus Nutrition 0.000 description 1
- DGAQECJNVWCQMB-PUAWFVPOSA-M Ilexoside XXIX Chemical compound C[C@@H]1CC[C@@]2(CC[C@@]3(C(=CC[C@H]4[C@]3(CC[C@@H]5[C@@]4(CC[C@@H](C5(C)C)OS(=O)(=O)[O-])C)C)[C@@H]2[C@]1(C)O)C)C(=O)O[C@H]6[C@@H]([C@H]([C@@H]([C@H](O6)CO)O)O)O.[Na+] DGAQECJNVWCQMB-PUAWFVPOSA-M 0.000 description 1
- 229920001732 Lignosulfonate Polymers 0.000 description 1
- ZMXDDKWLCZADIW-UHFFFAOYSA-N N,N-Dimethylformamide Chemical class CN(C)C=O ZMXDDKWLCZADIW-UHFFFAOYSA-N 0.000 description 1
- CTQNGGLPUBDAKN-UHFFFAOYSA-N O-Xylene Chemical compound CC1=CC=CC=C1C CTQNGGLPUBDAKN-UHFFFAOYSA-N 0.000 description 1
- RCEAADKTGXTDOA-UHFFFAOYSA-N OS(O)(=O)=O.CCCCCCCCCCCC[Na] Chemical class OS(O)(=O)=O.CCCCCCCCCCCC[Na] RCEAADKTGXTDOA-UHFFFAOYSA-N 0.000 description 1
- 206010034133 Pathogen resistance Diseases 0.000 description 1
- 235000012211 aluminium silicate Nutrition 0.000 description 1
- OOCMUZJPDXYRFD-UHFFFAOYSA-L calcium;2-dodecylbenzenesulfonate Chemical compound [Ca+2].CCCCCCCCCCCCC1=CC=CC=C1S([O-])(=O)=O.CCCCCCCCCCCCC1=CC=CC=C1S([O-])(=O)=O OOCMUZJPDXYRFD-UHFFFAOYSA-L 0.000 description 1
- HCWYXKWQOMTBKY-UHFFFAOYSA-N calcium;dodecyl benzenesulfonate Chemical class [Ca].CCCCCCCCCCCCOS(=O)(=O)C1=CC=CC=C1 HCWYXKWQOMTBKY-UHFFFAOYSA-N 0.000 description 1
- 238000013329 compounding Methods 0.000 description 1
- 238000007796 conventional method Methods 0.000 description 1
- 230000000857 drug effect Effects 0.000 description 1
- 235000018927 edible plant Nutrition 0.000 description 1
- 150000002170 ethers Chemical class 0.000 description 1
- 230000000855 fungicidal effect Effects 0.000 description 1
- 239000000417 fungicide Substances 0.000 description 1
- 230000002070 germicidal effect Effects 0.000 description 1
- NLYAJNPCOHFWQQ-UHFFFAOYSA-N kaolin Chemical compound O.O.O=[Al]O[Si](=O)O[Si](=O)O[Al]=O NLYAJNPCOHFWQQ-UHFFFAOYSA-N 0.000 description 1
- 230000002045 lasting effect Effects 0.000 description 1
- 239000000575 pesticide Substances 0.000 description 1
- 244000144977 poultry Species 0.000 description 1
- QLNJFJADRCOGBJ-UHFFFAOYSA-N propionamide Chemical compound CCC(N)=O QLNJFJADRCOGBJ-UHFFFAOYSA-N 0.000 description 1
- 229940080818 propionamide Drugs 0.000 description 1
- 238000001228 spectrum Methods 0.000 description 1
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- Agricultural Chemicals And Associated Chemicals (AREA)
Abstract
The invention discloses an insecticidal and acaricidal composition, which is a bactericide, a binary bactericidal complex compounded by a fenoxanil azole bactericide (containing but not limited to difenoconazole and tebuconazole) as a main component. The weight ratio of the fenoxanil to triazole bactericide (containing but not limited to difenoconazole and tebuconazole) is (20:1)-(1:20). The active component is 5-80% in percentage by weight. The processed dosage form comprises suspensions, wettable powder, granules, water dispersible granules, emulsifiable solutions, microemulsions and water emulsions; and the auxiliary component in the binary complex comprises acceptable organic solvents, emulsifiers, surfactants, inert fillers and the like. The composition is compounded to be used for the prevention and treatment of various diseases of rice, wheat, cotton, tomatoes, cucumbers, potatoes and other vegetables, and has an obvious synergistic effect.
Description
One, technical field
The present invention relates to technical field of pesticide, relate to the agriculture chemical compounding technology, particularly with the compounded technology of rice blast acid amides.
Two, background technology
Rice blast acid amides (zarilamid) is a kind of brand-new, efficient germicide.
Chemical name: N-(cyanic acid-1,2-dimethyl propyl)-2-(2,4 dichloro benzene oxygen base) propionamide
Molecular formula: C
15H
18CI
2N
2O
2
Relative molecular weight: 329.22
Structural formula:
Rice blast acid amides (zarilamid) belongs to novel acid amide fungicides.It is a kind of brand-new, high-efficiency broad spectrum property bactericide, does not have the cross resistance problem with other existing bactericide, and the difference of various crop is fallen ill all has fine preventive effect and outstanding lasting effect, and low toxicity, low-residual, safety are good.
As safe as a house to crop under different temperature conditions, to person poultry safety, low toxicity.Be suitable for the production of pollution-free green food.
The complex preparation that with the rice blast acid amides is main component has certain effect to improving drug effect with selectivity, and existing lot of documents is reported.
Three, summary of the invention
The object of the present invention is to provide a kind of is the efficient of main body composition with the rice blast acid amides, wide range, complex preparation cheaply.
The objective of the invention is to realize like this, is first component with the rice blast acid amides, is second component with triazole bactericidal agent, is equipped with various auxiliary materials and obtains efficiently, wide range, binary built preparation cheaply.
The desinsection that the present invention relates to, miticide composition comprise rice blast acid amides and triazole bactericidal agent at least, and the active ingredient weight percent content is 5～80%, and the mass ratio of rice blast acid amides and triazole bactericidal agent is between 20: 1～1: 20.
The desinsection that the present invention relates to, miticide composition, said triazole bactericidal agent are selected from a kind of in Difenoconazole, the triazolone.
The desinsection that the present invention relates to, the formulation of miticide composition are a kind of in missible oil, wetting powder, suspending agent, granule, microemulsion, aqueous emulsion, the water-dispersible granules.
The desinsection that the present invention relates to, miticide composition adopt by the conventional method preparation, can be mixed with various formulations, and be easy to use.Characteristics, particularly its high efficiency, low toxicity, low-residual such as have efficient, low toxicity, low-residual, fungicidal spectrum is wide, synergistic effect is remarkable, use cost is low are particularly advantageous in the production of pollution-free food.Can be used for the multiple diseases control on paddy rice, wheat, cotton, tomato, cucumber, the potatoes and other crops.
Four, embodiment
Below in conjunction with embodiment the technical scheme that invention relates to is further specified, but not as the restriction to technical scheme.
Except that mentioning especially, component ratio is weight portion among the embodiment.
Embodiment one
25% rice blast acid amides Difenoconazole missible oil
Raw material is formed: 15 parts of former medicines of rice blast acid amides, 10 parts of difenoconazole technical materials, 10 parts of cyclohexanone; 5 parts of dimethyl formamides, 4 parts of calcium dodecyl benzene sulfonates, 5 parts of triphen ethyl-phenol APEOs; 2 parts of phenethyl phenolformaldehyde resin APEOs, all the other supply 100 parts with toluene.Press the usual manner preparation.
Toxicity test, rat acute per os LD50＞1500mg/kg, chmice acute per os LD50＞1500mg/kg; Rabbit is acute through skin LD502000mg/kg, and rat acute has no stimulation to skin through skin LD50＞2000mg/kg; Eye is had no stimulation, show that compound drug belongs to low-toxin farm chemicals.
Using dosage: convert and prevent and treat rice sheath blight disease, 2000～3000 times of water dilutions, spray medicine 3～7 days, effect is obvious, and preventive effect is more than 90%.
Rice blast acid amides (zarilamid) and Difenoconazole are pressed 20/1,10/1,5/1 respectively; 3/1,3/2,1/1; 1/3,1/10,1/20 ratio is composite; Do check experiment with 20% rice blast acid amides (zarilamid) suspending agent and 10% Difenoconazole wetting powder, 3: 2 proportioning medicament co-toxicity coefficient 293.53 wherein, the result shows and has significant synergies.
Embodiment nine
80% rice blast acid amides trazodone wettable powder
Raw material is formed: 75 parts of former medicines of rice blast acid amides, and 5 parts of triazolones, 7 parts of di-2-ethylhexylphosphine oxide bitter edible plant sodium sulfonates, 5 parts of sodium lignin sulfonates, 2 parts of dodecyl sodium sulfates are supplied 100 parts with kaolin, prepare by the composite mode of conventional wetting powder.
Toxicity test, rat acute per os LD50＞10000mg/kg, rabbit is acute through skin LD50＞10000mg/kg, and skin is had faint spread effect, and eye is had faint spread effect, shows that compound drug belongs to low-toxin farm chemicals.
Using dosage: the control wheat sharp eyespot, convert 5000～6000 times of water dilutions, spray medicine 2-3 days, effect is obvious, and preventive effect is more than 90%.
Rice blast acid amides (zarilamid) and triazolone are pressed 20/1,15/1 respectively, 10: 1; 5/1,1/1,1/10 ratio is composite; Do check experiment with 20% rice blast acid amides (zarilamid) suspending agent and 10% trazodone wettable powder; Co-toxicity coefficient is 154.35～192.25, and the result shows and has significant synergies, and is wherein the most obvious with 15: 1 synergistic effects.
Embodiment 11
5% rice blast acid amides Difenoconazole aqueous emulsion
Raw material is formed: 3 parts of former medicines of rice blast acid amides, 2 parts of difenoconazole technical materials, 10 parts of cyclohexanone; 10 parts of xylol, 1 part of calcium dodecyl benzene sulfonate, 3 parts of triphen ethyl-phenol APEOs; 2 parts of phenethyl phenolformaldehyde resin APEOs; 8 parts of polyoxyethylene nonylphenol ethers, 5 parts of ethylene glycol, water are supplied 100 parts.Press the usual manner preparation.
Toxicity test, rat acute per os LD50＞1500mg/kg, chmice acute per os LD50＞1500mg/kg; Rabbit acute through skin LD50 greater than 2000mg/kg, rat acute has no stimulation to skin through skin LD50＞2000mg/kg; Eye is had no stimulation, show that compound drug belongs to low-toxin farm chemicals.
Using dosage: prevent and treat rice sheath blight disease, convert 800～1000 times of water dilutions, spray medicine 3～7 days, effect is obvious, and preventive effect is more than 90%.
Rice blast acid amides (zarilamid) and Difenoconazole are pressed 20/1,10/1,5/1 respectively; 3/1,3/2,1/1; 1/3,1/10,1/20 ratio is composite; Do check experiment with 20% rice blast acid amides (zarilamid) suspending agent and 10% Difenoconazole wetting powder, the result shows and has significant synergies, wherein 3: 2 proportioning medicament co-toxicity coefficient 293.53.
Claims (3)
1. a desinsection, miticide composition comprise rice blast acid amides and triazole bactericidal agent at least, and the active ingredient weight percent content is 5～80%, and the mass ratio of rice blast acid amides and triazole bactericidal agent is between 20: 1～1: 20.
2. the described desinsection of claim 1, miticide composition, said triazole bactericidal agent are selected from a kind of in Difenoconazole, the triazolone.
3. the formulation of claim 1 or 2 described desinsections, miticide composition is a kind of in missible oil, wetting powder, suspending agent, granule, microemulsion, aqueous emulsion, the water-dispersible granules.
Priority Applications (1)
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| CN2012100677198A CN102640755A (en) | 2009-07-22 | 2009-07-22 | Insecticidal and acaricidal composition |
Applications Claiming Priority (1)
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| CN2012100677198A CN102640755A (en) | 2009-07-22 | 2009-07-22 | Insecticidal and acaricidal composition |
Related Parent Applications (1)
| Application Number | Title | Priority Date | Filing Date |
|---|---|---|---|
| CN 200910016868 Division CN101601384B (en) | 2009-07-22 | 2009-07-22 | Insecticide and acaricide combination |
Publications (1)
| Publication Number | Publication Date |
|---|---|
| CN102640755A true CN102640755A (en) | 2012-08-22 |
Family
ID=46654034
Family Applications (1)
| Application Number | Title | Priority Date | Filing Date |
|---|---|---|---|
| CN2012100677198A Pending CN102640755A (en) | 2009-07-22 | 2009-07-22 | Insecticidal and acaricidal composition |
Country Status (1)
| Country | Link |
|---|---|
| CN (1) | CN102640755A (en) |
Cited By (1)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN104663655A (en) * | 2015-03-19 | 2015-06-03 | 京博农化科技股份有限公司 | Use and using method of fenoxanil or fenoxanil composition |
Citations (3)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| GB2098607A (en) * | 1981-05-12 | 1982-11-24 | Ciba Geigy Ag | Novel microbicidal arylphenyl ether derivatives |
| CN87106006A (en) * | 1986-08-29 | 1988-03-16 | 施尔·阿格拉尔有限公司 | The preparation method of arylcarboxylic acid derivative and application |
| CN101690483A (en) * | 2009-06-27 | 2010-04-07 | 深圳诺普信农化股份有限公司 | Bactericidal composition containing triazole class compounds |
-
2009
- 2009-07-22 CN CN2012100677198A patent/CN102640755A/en active Pending
Patent Citations (3)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| GB2098607A (en) * | 1981-05-12 | 1982-11-24 | Ciba Geigy Ag | Novel microbicidal arylphenyl ether derivatives |
| CN87106006A (en) * | 1986-08-29 | 1988-03-16 | 施尔·阿格拉尔有限公司 | The preparation method of arylcarboxylic acid derivative and application |
| CN101690483A (en) * | 2009-06-27 | 2010-04-07 | 深圳诺普信农化股份有限公司 | Bactericidal composition containing triazole class compounds |
Cited By (2)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN104663655A (en) * | 2015-03-19 | 2015-06-03 | 京博农化科技股份有限公司 | Use and using method of fenoxanil or fenoxanil composition |
| CN104663655B (en) * | 2015-03-19 | 2016-08-24 | 京博农化科技股份有限公司 | A kind of fenoxanil or the purposes of fenoxanil compositions and using method thereof |
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Owner name: CHAMBROAD AGROCHEMICAL TECHNOLOGY CO., LTD. Free format text: FORMER OWNER: SHANDONG CHAMBROAD HOLDING CO., LTD. Effective date: 20130322 Free format text: FORMER OWNER: CHAMBROAD AGROCHEMICAL TECHNOLOGY CO., LTD. Effective date: 20130322 |
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Effective date of registration: 20130322 Address after: 256500 Boxing Economic Development Zone, Binzhou, Shandong Applicant after: Jingbo Agrochemicals Technology Co., Ltd. Address before: Hu Zhen 256500 Shandong County of Boxing province Chen Jingbo Industrial Park Applicant before: Shandong Chambroad Holding Co., Ltd. Applicant before: Jingbo Agrochemicals Technology Co., Ltd. |
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Application publication date: 20120822 |