CN102353763A - Small simulation device for testing spontaneous combustion period of coal - Google Patents
Small simulation device for testing spontaneous combustion period of coal Download PDFInfo
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- CN102353763A CN102353763A CN2011102708995A CN201110270899A CN102353763A CN 102353763 A CN102353763 A CN 102353763A CN 2011102708995 A CN2011102708995 A CN 2011102708995A CN 201110270899 A CN201110270899 A CN 201110270899A CN 102353763 A CN102353763 A CN 102353763A
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- 239000003245 coal Substances 0.000 title claims abstract description 55
- 238000002485 combustion reaction Methods 0.000 title claims abstract description 26
- 230000002269 spontaneous effect Effects 0.000 title claims abstract description 26
- 238000012360 testing method Methods 0.000 title claims abstract description 12
- 238000004088 simulation Methods 0.000 title abstract description 6
- 238000006243 chemical reaction Methods 0.000 claims abstract description 23
- 238000004868 gas analysis Methods 0.000 claims abstract description 7
- XEEYBQQBJWHFJM-UHFFFAOYSA-N Iron Chemical compound [Fe] XEEYBQQBJWHFJM-UHFFFAOYSA-N 0.000 claims description 20
- 229910052742 iron Inorganic materials 0.000 claims description 10
- 239000010425 asbestos Substances 0.000 claims description 5
- 229910052895 riebeckite Inorganic materials 0.000 claims description 5
- 238000000034 method Methods 0.000 abstract description 5
- 230000003647 oxidation Effects 0.000 abstract description 3
- 238000007254 oxidation reaction Methods 0.000 abstract description 3
- 239000004576 sand Substances 0.000 abstract 2
- 239000007789 gas Substances 0.000 description 13
- QVGXLLKOCUKJST-UHFFFAOYSA-N atomic oxygen Chemical compound [O] QVGXLLKOCUKJST-UHFFFAOYSA-N 0.000 description 4
- 238000002474 experimental method Methods 0.000 description 4
- 239000001301 oxygen Substances 0.000 description 4
- 229910052760 oxygen Inorganic materials 0.000 description 4
- 230000036760 body temperature Effects 0.000 description 3
- 238000004458 analytical method Methods 0.000 description 2
- 238000005516 engineering process Methods 0.000 description 2
- 238000012544 monitoring process Methods 0.000 description 2
- 230000001105 regulatory effect Effects 0.000 description 2
- 238000003556 assay Methods 0.000 description 1
- 230000009286 beneficial effect Effects 0.000 description 1
- 230000005540 biological transmission Effects 0.000 description 1
- 230000005587 bubbling Effects 0.000 description 1
- 238000001816 cooling Methods 0.000 description 1
- 238000011161 development Methods 0.000 description 1
- 238000010586 diagram Methods 0.000 description 1
- 230000009977 dual effect Effects 0.000 description 1
- 230000000694 effects Effects 0.000 description 1
- 230000005611 electricity Effects 0.000 description 1
- 238000004519 manufacturing process Methods 0.000 description 1
- 238000004375 physisorption Methods 0.000 description 1
- 230000006798 recombination Effects 0.000 description 1
- 238000005215 recombination Methods 0.000 description 1
- 238000007789 sealing Methods 0.000 description 1
- XLYOFNOQVPJJNP-UHFFFAOYSA-N water Substances O XLYOFNOQVPJJNP-UHFFFAOYSA-N 0.000 description 1
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Abstract
本发明公开了一种煤炭自燃发火期小型模拟装置设备，此设备包括自燃反应炉、沙浴装置、温度采集系统、温度补偿系统、供气系统和气体分析系统。其中自然反应炉首创了双层煤炭氧化炉嵌套结构，真正解决了已有煤炭自燃发火模拟装置的热量散失问题；沙浴装置控温范围更大、控温精度更高，具有热量传导均匀、适合高温工作、无安全隐患的优点，并作为双层煤炭氧化炉嵌套结构外部的又一层温度保护结构，为模拟煤自燃发火的全过程提供良好的温度保护。本发明工作稳定，模拟相似度高，能够很好地模拟煤炭自燃发火过程，可用于测试煤炭最短自然发火期及实际条件下的煤自燃发火条件、地点和时间的判定及预测等。
The invention discloses a small-scale simulation device for spontaneous combustion of coal, which includes a spontaneous combustion reaction furnace, a sand bath device, a temperature acquisition system, a temperature compensation system, a gas supply system and a gas analysis system. Among them, the natural reaction furnace pioneered the nested structure of double-layer coal oxidation furnace, which truly solved the heat loss problem of the existing coal spontaneous combustion simulation device; the sand bath device has a larger temperature control range and higher temperature control accuracy, and has uniform heat conduction, It is suitable for high-temperature work and has the advantages of no safety hazards, and as another layer of temperature protection structure outside the nested structure of the double-layer coal oxidation furnace, it provides good temperature protection for the whole process of simulating the spontaneous combustion of coal. The invention works stably, has high simulation similarity, can well simulate the coal spontaneous combustion process, and can be used for testing the shortest coal spontaneous combustion period and determining and predicting coal spontaneous combustion conditions, locations and times under actual conditions.
Description
Technical field
The present invention relates to the small-sized analogue means of a kind of comprehensive coal face goaf and tunnel loose coal spontaneous combustion ignition, realizes the experimental simulation of spontaneous combustion of coal overall process, has solved judgement and the forecasting problem of spontaneous combustion of coal condition, place and the time under the physical condition.
Background technology
In the prior art; The analogue means that two kinds of test spontaneous combustion of coal phases are arranged; Its principle is basic identical: the air supply system of forming with air compressor and air supply pipe is to coal sample reaction vessel air feed; Make coal and airborne oxygen generation coal oxygen recombination reaction, emit heat and then intensification gradually, reach spontaneous combustion at last.Temperature to coal reaction in the experimentation is carried out the overall process collection, to the CH that discharges in the overall process
4, CO
2, gas such as CO analyzes.The prior art key is to adopt the temperature protection system that spontaneous combustion of coal is heated up to carry out temperature protection; Promptly adopt temperature control equipment to follow the tracks of the temperature in the coal reaction container; And in view of the above the temperature protection medium is heated, medium is equated with the coal reaction vessel temp, thereby realize temperature protection.Present technology has two kinds of temperature protection systems: bath temperature protection system and temperature programme oven temperature, degree protection system.Bath temperature protection system water is as the temperature protection medium, and the disadvantage of this medium is that medium maximum temperature (100 ℃) is low excessively, can not satisfy the required temperature more than 300 ℃ of spontaneous combustion of coal; Temperature programme oven temperature, degree protection system adopts air as the temperature protection medium, and the shortcoming of this medium is can produce heat flow when being heated, and it is inhomogeneous to cause conducting heat.
Summary of the invention
In order to address the above problem; The purpose of this invention is to provide a kind of in order to generation, development, the change procedure of grasping coal spontaneous combustion and the cooling rule after stopping oxygen supply; Its experimental precision is high, and the simulation similarity is good, the test spontaneous combustion of coal ignition small-sized analogue means of phase that result of use is good.
Wherein the hypergolic reaction stove is the container of coal sample hypergolic reaction, is double-layer nested device.Coal sample is placed in two reacting furnaces, through air supply, makes coal generation physisorption, chemisorption and chemical reaction, and then the coal temperature is risen gradually, reach spontaneous combustion at last.Temperature acquisition system is through temperature collecting device and transmission, analysis software, reaches the system of temperature data in the real-time monitoring storage reaction device.Temperature-compensated system is to realize that through temperature controller and sand-bath device hypergolic reaction stove inside and outside temperature difference is zero system.Air supply system is that reaction is carried out indispensable for experiment provides hypergolic reaction necessary oxygen.Gas analysis system is to carry out the real-time and effective analysis through the gas that gas is collected and stratographic analysis reaches the experiment generation, judges the purpose of the degree of spontaneous combustion of coal reaction.
Technical scheme of the present invention is: a kind of test spontaneous combustion of coal ignition small-sized analogue means of phase, and this analogue means is made up of hypergolic reaction stove, temperature acquisition system, temperature-compensated system, air supply system and gas analysis system;
Said hypergolic reaction stove is made up of outside stove and inner furnace; Said outside stove is made up of body of heater II and outside stove blind flange; Be provided with outside stove iron net in the said body of heater II; The below of one wing furnace wall is provided with outside stove air inlet valve, and top, the right side of opposite side furnace wall is provided with the outside stove valve of giving vent to anger, and is provided with sheet asbestos between said body of heater II and the said outside stove blind flange; Said inner furnace is made up of body of heater I and inner furnace blind flange; Be provided with inner furnace iron net in the said body of heater I; The bottom of said body of heater I is provided with inner furnace air inlet valve, and said inner furnace blind flange is provided with the inner furnace valve of giving vent to anger, and is provided with O-ring seal between said body of heater I and the inner furnace blind flange;
Said temperature acquisition system comprises that inner furnace temperature sensor, outside furnace temperature sensor, sand-bath temperature sensor and temperature data acquisition device constitute;
Said temperature-compensated system comprises sand-bath device, inner furnace draft tube, outside stove draft tube and temperature controller;
Said air supply system comprises gas meter and Air compressing bottle;
Said gas analysis system comprises chromatograph and PC;
Wherein, Said inner furnace is nested in the said outside stove; Said outside stove places in the said sand-bath device; Said Air compressing bottle is connected with outside stove air inlet valve with said inner furnace air inlet valve respectively with the inner furnace draft tube through said outside stove draft tube, and the said outside stove valve of giving vent to anger is connected with said chromatograph through outside furnace outlet duct, and the said inner furnace valve of giving vent to anger passes through the inner furnace escape pipe and is connected with said chromatograph; Said inner furnace temperature sensor places the inner lead that passes through of said inner furnace to be connected with said temperature data acquisition device; Said outside furnace temperature sensor places said outside furnace interior through lead and said temperature controller control linkage; Said chromatograph is connected with said PC data with said temperature data acquisition device, and said sand-bath temperature sensor places said sand-bath device inner through lead and said temperature controller control linkage; Said chromatograph is connected with said PC data with said temperature data acquisition device.
Further, said outside stove draft tube and inner furnace draft tube are provided with the gas meter that is used to measure.
The invention has the beneficial effects as follows:
1, electricity consumption sand-bath is protected the temperature of outside stove.The sand-bath temperature is regulated by automatic temp controller, and automatic temp controller can be followed the tracks of outside stove coal sample temperature, makes sand-bath temperature and outside furnace temperature be consistent, and then realizes outside stove body temperature protection.
2, the temperature of the double-layer nested unit protection inner furnace of coal sample reacting furnace.The double-layer nested device of so-called reacting furnace is with being placed on the less coal sample reacting furnace (inner furnace) of build the bigger reacting furnace of build (outside stove) the inside.Two reacting furnaces are all put into the fresh coal sample of same size, the place of production, granularity, and make them begin bubbling air simultaneously, let them begin reaction simultaneously.Like this, the coal sample reaction process in outside stove and the inner furnace is identical, and promptly the temperature of inner furnace and outside stove keeps identical in real time, and the inner furnace inside and outside does not have temperature difference so, has so just realized the temperature protection of inner body of heater.So first kind of temperature protection measure realized the temperature protection of sand-bath to outside stove, second kind of temperature protection measure realized the temperature protection of outside stove for inner furnace.These two kinds of temperature protection measures have just formed inner stove body temperature protection dual fail-safe.Because we only measure the coal reaction in the inner furnace, therefore, through these two kinds of temperature protection, the temperature protection effect of this device inner furnace is very good.The air-flow cushion is all arranged at top, bottom at two-layer body of heater, makes air-flow from bottom to top evenly through the experiment coal body, and experimental gas is through the preheating of coal sample in battle field in the sand-bath and the outside stove, and temperature is identical with the coal temperature of inner body of heater, sends into from bottom of furnace body then.
Description of drawings
Fig. 1 tests the structural representation of spontaneous combustion of coal ignition small-sized analogue means of phase for the present invention.
Fig. 2 is the cross-sectional schematic of sand-bath device of the present invention.
Fig. 3 is a natural reaction furnace structure synoptic diagram of the present invention.
Among the figure:
1, outside stove, 2, inner furnace, 3, the body of heater II, 4, outside stove blind flange, 5, outside stove iron net; 6, outside stove air inlet valve, 7, the outside stove valve of giving vent to anger, 8, sheet asbestos, 9, the body of heater I, 10, the inner furnace blind flange; 11, inner furnace iron net, 12, inner furnace air inlet valve, 13, the inner furnace valve of giving vent to anger, 14, O-ring seal, 15 inner furnace temperature sensors; 16, outside furnace temperature sensor, 17, the sand-bath temperature sensor, 18, the temperature data acquisition device, 19, the sand-bath device, 20, the inner furnace draft tube; 21, outside stove draft tube, 22, temperature controller, 23, gas meter, 24, Air compressing bottle; 25, chromatograph, 26, PC, 27, outside furnace outlet duct, 28, the inner furnace escape pipe.
Embodiment
Below in conjunction with figure technical scheme of the present invention is explained further details.
Like Fig. 1, Fig. 2, shown in Figure 3, the present invention tests spontaneous combustion of coal ignition small-sized analogue means of phase, and this analogue means is by outside stove 1, inner furnace 2, body of heater II 3; Outside stove blind flange 4, outside stove iron net 5, outside stove air inlet valve 6, the outside stove valve 7 of giving vent to anger, sheet asbestos 8; Body of heater I 9, inner furnace blind flange 10, inner furnace iron net 11, inner furnace air inlet valve 12, the inner furnace valve 13 of giving vent to anger; O-ring seal 14, inner furnace temperature sensor 15, outside furnace temperature sensor 16, sand-bath temperature sensor 17, temperature data acquisition device 18; Sand-bath device 19, inner furnace draft tube 20, outside stove draft tube 21, temperature controller 22, gas meter 23; Air compressing bottle 24, chromatograph 25, PC 26, outside furnace outlet duct 27 constitutes with inner furnace escape pipe 28;
Wherein, Inner furnace 2 comprises body of heater I 9 and inner furnace blind flange 10, is provided with inner furnace iron net 11 in the body of heater I 9, and the bottom is provided with inner furnace air inlet valve 7; Inner furnace blind flange 10 is provided with the inner furnace valve 13 of giving vent to anger, and is provided with O-ring seal 14 sealings between body of heater I 9 and the inner furnace blind flange 10; Outside stove 1 comprises body of heater II 3 and outside stove blind flange 4, is provided with outside stove iron net 11 in the body of heater II 3, and the below, left side of body of heater II 3 is provided with outside stove air inlet valve 12, and the top, right side is provided with the outside stove valve 13 of giving vent to anger; Be provided with high density sheet asbestos 8 between body of heater II 3 and the outside stove blind flange 4; Inner furnace 2 is nested in the outside stove 1; Outside stove 1 places in the sand-bath device 19; Air compressing bottle 24 is connected with outside stove air inlet valve 6 with inner furnace air inlet valve 12 respectively with inner furnace draft tube 20 through outside stove draft tube 21; Outside stove draft tube 6 is provided with gas meter 23 with inner furnace draft tube 12, and the outside stove valve 7 of giving vent to anger is connected with chromatograph 25 through outside furnace outlet duct 27, and the inner furnace valve 13 of giving vent to anger passes through inner furnace escape pipe 27 and is connected with chromatograph 25; Inner furnace temperature sensor 15 places the said inner furnace 2 inner leads that pass through to be connected with temperature data acquisition device 18; Outside furnace temperature sensor 16 places outside stove 1 inner lead and temperature controller 22 control linkages passed through; Sand-bath temperature sensor 19 places sand-bath device 19 inner through lead and temperature controller 22 control linkages, and chromatograph 25 is connected with PC 26 data with temperature data acquisition device 18.
Principle of work:
1, the coal crusher that will newly gather to granularity is carried out classification then less than 10mm, carries out proportioning in proportion.Coal sample below the 1mm accounts for 35%, and the coal sample between 1mm and 2mm accounts for 20%, and the coal sample between 2mm and 4mm accounts for 25%, and what 4mm was above accounts for 20%, and coal sample is fully mixed.
2, the coal sample that mixes being got 1kg puts in the inner furnace 2; 15kg is put in the outside stove 1; Inner furnace 2 is put in the outside stove 1, then by outside stove 1 (wherein this moment will) is put in the sand-bath 19, two air storage bottle 24 is connected with outside stove 1 with inner furnace 5 respectively with outside stove draft tube 21 through inner furnace draft tube 20 then; Simultaneously inner furnace temperature sensor 15, outside furnace temperature sensor 16 and sand-bath temperature sensor 17 are placed on inner furnace 2 respectively; In outside stove 1 and the sand-bath 19, and they are linked to each other with the temperature controller 22 of outside with lead, during with test experience whether under identical temperature conditions.Outside sand-bath 19 ones, chromatograph 25, PC 26 and data acquisition unit 18 are connected, and with outside furnace outlet duct 27, inner furnace escape pipe 28 couples together the give vent to anger valve 7,13 of chromatograph 25 with inner furnace 2, outside stove 1, carries out gas analysis.
3, after instrument connects fully, carry out air tight test, after the assay was approved; Connect the sand-bath power supply; Open Temperature sampler power supply, start-up temperature acquisition software, open temperature controller, the control inner furnace infeeds the air that flow is 40 ml/min; Outside stove infeeds the air of 600ml/min, and experiment promptly begins to start.
After the energized, coal sample in the spontaneous combustion temperature-rise period, in inside and outside two reacting furnaces temperature and all gases concentration all in time, wind supply quantity and radiating condition and change.Follow the tracks of coal body temperature variations in the stove by automatic temperature control system, the temperature difference of regulating sand-bath and outer reaction stove is 0.1 ℃.When reaching uniform temperature; Coal sample in inner furnace and the outside stove begins oxidation slowly and produces gas; With temperature variation in the Temperature sampler continuous monitoring coal body; And 10 ℃ of exhaust 0.5L that collect inner furnace of every intensification feed gas chromatograph and detect the variation that coal sample produces gas under the differential responses temperature, and record.
Claims (2)
1. a test spontaneous combustion of coal ignition small-sized analogue means of phase is characterized in that this analogue means is made up of hypergolic reaction stove, temperature acquisition system, temperature-compensated system, air supply system and gas analysis system;
Said hypergolic reaction stove is made up of outside stove (1) and inner furnace (2); Said outside stove (1) is made up of body of heater II (3) and outside stove blind flange (4); Be provided with outside stove iron net (5) in the said body of heater II (3); The below of one wing furnace wall is provided with outside stove air inlet valve (6), and top, the right side of opposite side furnace wall is provided with the outside stove valve (7) of giving vent to anger, and is provided with sheet asbestos (8) between said body of heater II (3) and the said outside stove blind flange (4); Said inner furnace (2) is made up of body of heater I (9) and inner furnace blind flange (10); Be provided with inner furnace iron net (11) in the said body of heater I (9); The bottom of said body of heater I (9) is provided with inner furnace air inlet valve (12); Said inner furnace blind flange (10) is provided with the inner furnace valve (13) of giving vent to anger, and is provided with O-ring seal (14) between said body of heater I (9) and the inner furnace blind flange (10);
Said temperature acquisition system comprises that inner furnace temperature sensor (15), outside furnace temperature sensor (16), sand-bath temperature sensor (17) and temperature data acquisition device (18) constitute;
Said temperature-compensated system comprises sand-bath device (19), inner furnace draft tube (20), outside stove draft tube (21) and temperature controller (22);
Said air supply system comprises gas meter (23) and Air compressing bottle (24);
Said gas analysis system comprises chromatograph (25) and PC (26);
Wherein, Said inner furnace (2) is nested in the said outside stove (1); Said outside stove (1) places in the said sand-bath device (19); Said Air compressing bottle (24) is connected with outside stove air inlet valve (6) with said inner furnace air inlet valve (12) respectively with inner furnace draft tube (20) through said outside stove draft tube (21); The said outside stove valve (7) of giving vent to anger is connected with said chromatograph (25) through outside furnace outlet duct (27), and the said inner furnace valve (13) of giving vent to anger passes through inner furnace escape pipe (28) and is connected with said chromatograph (25); Said inner furnace temperature sensor (15) places the inner lead that passes through of said inner furnace (2) to be connected with said temperature data acquisition device (18), and said chromatograph (25) is connected with said PC (26) data with said temperature data acquisition device (18); Said outside furnace temperature sensor (16) places said outside stove (1) inner through lead and said temperature controller (22) control linkage, and said sand-bath temperature sensor (17) places said sand-bath device (19) inner through lead and said temperature controller (22) control linkage.
2. test spontaneous combustion of coal ignition small-sized analogue means of phase according to claim 1 is characterized in that said outside stove draft tube (21) and inner furnace draft tube (20) are provided with the gas meter (23) that is used to measure.
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Citations (17)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| SU535494A1 (en) * | 1974-09-06 | 1976-11-15 | Специальная Научно-Исследовательская Лаборатория Всесоюзного Научно-Исследовательского Института Противопожарной Обороны Мвд Ссср | Method for determining the effect of gas extinguishing agents on spontaneous combustion |
| SU979976A1 (en) * | 1981-05-13 | 1982-12-07 | Казанский Ордена Трудового Красного Знамени Авиационный Институт Им.А.Н.Туполева | Method of determination of liquid and gaseous fuel delay time and spontaneous ignition temperature |
| JPS6117063A (en) * | 1984-07-03 | 1986-01-25 | Nippon Kokan Kk <Nkk> | Forecaster spontaneous combustion |
| SU1492256A1 (en) * | 1986-07-24 | 1989-07-07 | Всесоюзный научно-исследовательский институт техники безопасности в химической промышленности | Device for determining temperature of self-ignition in dynamic mode |
| AU610970B2 (en) * | 1988-02-08 | 1991-05-30 | General Signal Corporation | Calorimetry system |
| JP3511787B2 (en) * | 1996-02-29 | 2004-03-29 | 株式会社島津製作所 | Spontaneous ignition test equipment |
| CN1595129A (en) * | 2004-07-16 | 2005-03-16 | 中国矿业大学 | Thermal insulation testing process and apparatus for simulating coal spontaneous combustion procedure |
| CN2718573Y (en) * | 2004-07-16 | 2005-08-17 | 中国矿业大学 | Heat insulation tester for analoging coal self-combusting process |
| CN101000720A (en) * | 2006-12-19 | 2007-07-18 | 煤炭科学研究总院重庆分院 | High vacuum multi-layer adiabat oxidation analog coal self-combustion device |
| CN101206211A (en) * | 2007-12-18 | 2008-06-25 | 中国矿业大学 | A method for measuring coal spontaneous combustion tendency |
| CN101520451A (en) * | 2009-03-25 | 2009-09-02 | 太原理工大学 | Radon-measuring test bed for spontaneous combustion of simulated coal |
| CN101650287A (en) * | 2009-05-14 | 2010-02-17 | 西安热工研究院有限公司 | Electrical heating type cylindrical raw coal spontaneous combustion testing device and method |
| CN201413318Y (en) * | 2009-03-25 | 2010-02-24 | 太原理工大学 | A radon test bench for simulating coal spontaneous combustion |
| CN201503431U (en) * | 2009-04-15 | 2010-06-09 | 北京凌天世纪自动化技术有限公司 | Spontaneous combustion tendency tester for coal mine |
| CN101776677A (en) * | 2009-12-23 | 2010-07-14 | 煤炭科学研究总院沈阳研究院 | Device for simulation of coal spontaneous combustion on basis of programmed temperature control |
| CN201589761U (en) * | 2009-12-23 | 2010-09-22 | 煤炭科学研究总院沈阳研究院 | Coal spontaneous combustion simulator based on program temperature control |
| CN201607437U (en) * | 2009-10-16 | 2010-10-13 | 王刚 | Analog simulation device for spontaneous combustion of float coal of goaf of coal mine |
-
2011
- 2011-09-14 CN CN201110270899.5A patent/CN102353763B/en not_active Expired - Fee Related
Patent Citations (17)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| SU535494A1 (en) * | 1974-09-06 | 1976-11-15 | Специальная Научно-Исследовательская Лаборатория Всесоюзного Научно-Исследовательского Института Противопожарной Обороны Мвд Ссср | Method for determining the effect of gas extinguishing agents on spontaneous combustion |
| SU979976A1 (en) * | 1981-05-13 | 1982-12-07 | Казанский Ордена Трудового Красного Знамени Авиационный Институт Им.А.Н.Туполева | Method of determination of liquid and gaseous fuel delay time and spontaneous ignition temperature |
| JPS6117063A (en) * | 1984-07-03 | 1986-01-25 | Nippon Kokan Kk <Nkk> | Forecaster spontaneous combustion |
| SU1492256A1 (en) * | 1986-07-24 | 1989-07-07 | Всесоюзный научно-исследовательский институт техники безопасности в химической промышленности | Device for determining temperature of self-ignition in dynamic mode |
| AU610970B2 (en) * | 1988-02-08 | 1991-05-30 | General Signal Corporation | Calorimetry system |
| JP3511787B2 (en) * | 1996-02-29 | 2004-03-29 | 株式会社島津製作所 | Spontaneous ignition test equipment |
| CN1595129A (en) * | 2004-07-16 | 2005-03-16 | 中国矿业大学 | Thermal insulation testing process and apparatus for simulating coal spontaneous combustion procedure |
| CN2718573Y (en) * | 2004-07-16 | 2005-08-17 | 中国矿业大学 | Heat insulation tester for analoging coal self-combusting process |
| CN101000720A (en) * | 2006-12-19 | 2007-07-18 | 煤炭科学研究总院重庆分院 | High vacuum multi-layer adiabat oxidation analog coal self-combustion device |
| CN101206211A (en) * | 2007-12-18 | 2008-06-25 | 中国矿业大学 | A method for measuring coal spontaneous combustion tendency |
| CN101520451A (en) * | 2009-03-25 | 2009-09-02 | 太原理工大学 | Radon-measuring test bed for spontaneous combustion of simulated coal |
| CN201413318Y (en) * | 2009-03-25 | 2010-02-24 | 太原理工大学 | A radon test bench for simulating coal spontaneous combustion |
| CN201503431U (en) * | 2009-04-15 | 2010-06-09 | 北京凌天世纪自动化技术有限公司 | Spontaneous combustion tendency tester for coal mine |
| CN101650287A (en) * | 2009-05-14 | 2010-02-17 | 西安热工研究院有限公司 | Electrical heating type cylindrical raw coal spontaneous combustion testing device and method |
| CN201607437U (en) * | 2009-10-16 | 2010-10-13 | 王刚 | Analog simulation device for spontaneous combustion of float coal of goaf of coal mine |
| CN101776677A (en) * | 2009-12-23 | 2010-07-14 | 煤炭科学研究总院沈阳研究院 | Device for simulation of coal spontaneous combustion on basis of programmed temperature control |
| CN201589761U (en) * | 2009-12-23 | 2010-09-22 | 煤炭科学研究总院沈阳研究院 | Coal spontaneous combustion simulator based on program temperature control |
Non-Patent Citations (5)
| Title |
|---|
| LI ZENGHUA,ETC.: "Experiment study of model compound oxidation on spontaneous combustion of coal", 《PROCEDIA EARTH AND PLANETARY SCIENCE》, vol. 1, no. 1, 30 September 2009 (2009-09-30), pages 123 - 129 * |
| TEST METHOD FOR THE PROPENSITY OF COAL TO SPONTANEOUS COMBUSTION: "Wang Deming,etc.", 《PROCEDIA EARTH AND PLANETARY SCIENCE》, vol. 1, no. 1, 30 September 2009 (2009-09-30), pages 20 - 26 * |
| 周晓兵 等: "煤炭自燃仿真炉温度测控系统", 《测控技术》, vol. 18, no. 6, 30 June 1999 (1999-06-30), pages 21 - 23 * |
| 张国枢 等: "煤炭自燃模拟实验装置设计与研制", 《淮南工业学院学报》, vol. 19, no. 4, 31 December 1999 (1999-12-31), pages 11 - 13 * |
| 罗海珠 等: "《中华人民共和国国家标准》", 16 February 2006, article "GB/T 20104-2006 煤自燃倾向性色谱吸氧鉴定法", pages: 1-9 * |
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