CN102293404A - Perilla effervescent tablets and preparation method thereof - Google Patents
Perilla effervescent tablets and preparation method thereof Download PDFInfo
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Abstract
本发明公开了一种紫苏泡腾片，其组分包含紫苏提取物干燥粉、柠檬酸、碳酸氢钠、阿拉伯胶、聚乙烯吡咯烷酮、三氯蔗糖、消泡剂、聚乙二醇8000、维生素C和胶原蛋白肽；本发明紫苏泡腾片是一种酸甜可口、风味独特、具有一定营养价值与促进健康作用、食用方便、便于携带的新型固态食品；本发明具有重要的技术参考价值及广阔的市场开发前景。
The invention discloses a perilla effervescent tablet, which comprises perilla extract dry powder, citric acid, sodium bicarbonate, gum arabic, polyvinylpyrrolidone, sucralose, defoaming agent, polyethylene glycol 8000 , vitamin C and collagen peptide; perilla effervescent tablet of the present invention is a kind of sour-sweet good to eat, unique flavor, has certain nutritive value and health-promoting effect, easy to eat, portable novel solid food; the present invention has important technology Reference value and broad market development prospects.
Description
Technical field
The present invention relates to belong to field of food, being specifically related to the perilla leaf is the purple perilla nutrition or the healthy effervescent tablet of raw material processing.
Background technology
Purple perilla (Pefilla frutescens) has another name called perillaseed, fragrant Soviet Union etc., and its seed is called perillaseed, and its leaf is called Su Ye, and cording has the Labiatae annual herb plant of special fragrance.Purple perilla is at the cultivation history in existing more than 2000 year of China, traditional conventional Chinese medicine for the Compendium of Material Medica record, having very high edible nourishing simultaneously is worth, be present emerging in the world a kind of fashion vegetables and medical health product raw material, therefore purple perilla has the dietotherapeutic characteristics, become China Ministry of Public Health first batch of approval, one of 60 kinds of " integration of drinking and medicinal herbs " kinds.Perilla leaf is the important edible part of purple perilla, except that containing certain protein, multivitamin and mineral matter, also contain multiple bioactivators such as Rosmarinic acid, polyphenol, flavones, perillaldehyde, perilla alcohol, perillene, alpha-linolenic acid, have multiple functions such as antiallergy, anti-oxidant, anticancer, reducing blood lipid, clearing heat and detoxicating, antibiotic, antidepression, anti-inflammatory, so the edible health that is of value to of perilla leaf.In view of peculiar active material of perilla leaf and nutritional labeling thereof, perilla leaf becomes a kind of dietotherapeutic plant that enjoys domestic and international extensive concern in recent years, has important economic development value at nutritional health food and field of medicaments.
Perilla leaf has obtained certain development and utilization in recent years as a kind of vegetables that contain the better nutritivity composition and have tempting color and luster and local flavor.Finding through the literature search to prior art, is that the food processing product of development of raw materials is mainly liquid beverage (perilla vinegar beverage and preparation method thereof, publication number: CN101731705A at present with the perilla leaf; Perilla greengage wine and preparation method thereof, publication number: CN101519630; Perilla beverage, publication number: CN1292236A), flavoring (is used for purple perilla flavouring of cooking aquatic product and preparation method thereof, publication number: CN101406280; A kind of purple perilla flavoring liquid and preparation method thereof, publication number: CN101401632; ), perilla herb oil (purple perilla grease and its production and application, publication number: CN1566297A), the purple perilla tealeaves (preparation method of purple perilla tea, publication number: CN1488272A), preserved fruit, candy, cake (Lu Jiejing, literary composition is refined. the research overview progress [J] of purple perilla. and processing of farm products, 2009,6:32-34.) etc.But above these products are compared with solid product mainly based on liquid state, and inconvenient consumer carries and be edible, transportation and packing cost height, and the product shelf life is shorter relatively.
Effervescent tablet is domestic and international a kind of novel solid beverage products of focus Application and Development in recent years.The disintegrant of effervescent tablet be with a kind of or several organic acids (sour agent) and a kind of or several meet acid and can produce CO
2Common composition of inorganic salts (alkaline agent), meet the reaction of water generation acid-base neutralization and emit CO
2Make rapid disintegration of tablet and thawing.Take common solid tablet, active ingredient often will just can discharge through decomposition after a while; Though it is fast that liquid preparation discharges active ingredient, carries inconvenience, apt to deteriorate.Effervescent tablet has just in time overcome the shortcoming of these two kinds of formulations, and has following advantage: 1, little, the steady quality of effervescent tablet volume, production automation degree height, easy to carry and transport, and storage period is long; 2, effervescent tablet is taken facing with before being made into liquid, and its liquid preparation is easy to swallow, the bioavilability height, and is little to GI irritation, is specially adapted to the patient of the elderly and bradymassesis; 3, the active ingredient solubility height of effervescent tablet, the disintegrant calving disaggregation is powerful, and whole tablet can dissolve rapidly at short notice; 4, effervescent tablet is met water and is just produced bubble and seethe (being effervesce) up and down, and interesting, the carbon dioxide that produces during disintegration is partially dissolved in the drinking-water, and the aesthetic feeling as the carbonated drink is arranged when making drinking-water drink in the inlet, causes the interest that children drink easily.
Therefore in view of the technical deficiency in the above purple perilla existing product exploitation and the advantage of effervescent tablet, it is raw material that the present invention adopts perilla leaf, use the tablet consumable products technology of preparing that novelty is adopted in food-processing method and combination, a kind of sweet and sour taste, unique flavor are provided, have certain nutritive value and promote health benefit, instant, new portable solid food---purple perilla effervescent tablet.Consult relevant technical literature, before the present invention finishes, all do not have with the perilla leaf be the development of raw materials effervescent tablet report, and also do not have Related product to sell on the market, so the product of the present invention's development has important techniques reference value and brilliant market developing prospect.
Summary of the invention
The objective of the invention is to overcome above-mentioned deficiency of the prior art, a kind of sweet and sour taste, unique flavor are provided, have certain nutritive value and promote health benefit, instant, new portable solid food---purple perilla effervescent tablet and preparation method thereof.
For achieving the above object, the present invention is by the following technical solutions:
A kind of purple perilla effervescent tablet, its component comprises extractive of perilla xeraphium and auxiliary material, described extractive of perilla xeraphium is that perilla leaf is added ethanolic solution making beating, lixiviate, concentrates and the dry extractive of perilla xeraphium that makes, and described auxiliary material comprises citric acid, sodium acid carbonate, Arabic gum, polyvinylpyrrolidone, Sucralose, defoamer and polyethylene glycol 8000.Described auxiliary material also comprises vitamin C and/or collagen peptide; The percentage by weight of described component is:
Extractive of perilla xeraphium 5～30%; Citric acid 20～60%;
Sodium acid carbonate 15～50%; Arabic gum 2～10%;
Polyvinylpyrrolidone 0.45～0.6%; Sucralose 0.1～1%;
Defoamer 0.05～1%; Polyethylene glycol 8000 (PEG8000) 0.5～3%;
Vitamin C 0.0～1.0%; Collagen peptide 0.0～10%.
The present invention also provides a kind of method for preparing described purple perilla effervescent tablet, it is characterized in that may further comprise the steps:
A. be raw material with the perilla leaf, add the food grade ethanolic solution, smash to pieces with beater, lixiviate, fully filter with 100～400 eye mesh screens the reaction back, filtrate is carried out centrifugal, gets the spray-dried or freeze drying of supernatant and make the extractive of perilla xeraphium;
B. citric acid, sodium acid carbonate, Arabic gum, Sucralose and defoamer are mixed and pulverize, cross 100 mesh sieves and add in the granule-forming machine with the extractive of perilla xeraphium, after mixing, adding the ethanol solution contain polyvinylpyrrolidone (PVP) again mixes and makes softwood, the described ethanol solution volume (ml) that contains PVP: material gross weight (g)=15～20: 100, and be cut into coarse granule automatically;
C. above-mentioned coarse granule is crossed 14～20 mesh sieves and carry out granulation, drying is volatilized ethanol fully then, and pellet moisture content is controlled at below 2%;
D. drying is good particle is crossed 14～20 mesh sieves and is carried out whole grain, adds the PEG8000 powder, is dosed into tablet forming in the rotary pelleting machine after mixing, and gets product purple perilla effervescent tablet of the present invention;
The composition weight percentage composition of above-mentioned adding is: extractive of perilla xeraphium 5～30%; Citric acid 20～60%; Sodium acid carbonate 15～50%; Arabic gum 2～10%; Polyvinylpyrrolidone 0.45～0.6%; Sucralose 0.1～1%; Defoamer 0.05～1%; PEG80000.5～3%.
The food grade volumes of aqueous ethanol concentration that adds described in the described step a is 80%, described raw material quality (g): described volumes of aqueous ethanol (ml)=1: 2; Extracting condition is at 50 ℃ of following stirring and leaching 60min among the described step a; Centrifugal condition is 8000rpm/min among the described step a; Carry out vacuum among the described step a before centrifugal earlier and concentrate, to solid content be 5～10%; Also can add percentage by weight among the described step b in the granule-forming machine and be 0.0～1.0% vitamin C and/or 0.0～10% collagen peptide and mix with the extractive of perilla xeraphium; Drying condition is 40～50 ℃ among the described step c, dry 30 minutes; Described defoamer is bubble enemy defoamer.
Advantage of the present invention is:
1. the purple perilla nutrient effervescent tablets of the present invention's preparation contains the multiple nutrients health-care components.Nutritional labeling mainly comprises protein, vitamin (V
C, V
K1, V
D, VB
2And beta carotene), reach trace element (Ca, Fe, Zn, Mg, Mn) etc.Wholesome functional component mainly comprises the flavones with antioxidation that derives from purple perilla and the collagen peptide of Rosmarinic acid and interpolation, can eliminate free radical, prevent lipid peroxidation, and, health care anti-aging for the mankind has very unique significance because.
2. the present invention adopts non-water granulating tabletting process to prepare the purple perilla effervescent tablet, makes wetting agent with 3% PVP ethanol solution, and sour agent, alkaline agent mixing are in non-water environment, therefore can not react, and the dried particle of softwood is difficult for moisture absorption, and compressing tablet is sticking not, and the tablet of extrusion is difficult for the moisture absorption.In the whole process of production, need the production equipment and the preparation technology of usefulness simple, easy operating helps realizing industrialized production and processing.
The purple perilla nutrition of the present invention preparation or healthy effervescent tablet be easy to preserve, be convenient for carrying and transport, edible easy, nutritional labeling enters human body by liquid form, helps the nutritive and health protection components absorption in vivo, has improved the bioavilability of these compositions.
Citric acid is acid effervescent agent, and sodium acid carbonate is alkaline effervescent agent, after the two mixes, meets water chemical effervesce reaction takes place, and produces great amount of carbon dioxide gas at once, and citric acid also can be adjusted the tart flavour of effervescent tablet solid beverage, improves mouthfeel; Vitamin C is a water soluble vitamin, not only can strengthen immunity, anti-oxidant especially, as to protect cell even effective antitumor nutritional labeling; Collagen peptide averagemolecular wt amount is below 3000Da, but angiocardiopathy preventing, reducing weight and blood fat, replenish the calcium, prevent wrinkle of skin, anti-aging, beautifying face and moistering lotion, nourishing hair, the powerful metabolism that promotes skin, hair, nail etc., it is a kind of effective efficiency composition of beautifying face and moistering lotion, edible applicable to special population, as climacteric women; Arabic gum, polyvinylpyrrolidone (PVP) are as the adhesive of effervescent tablet, and bonding effect is good, and PVP is dissolved in the absolute ethyl alcohol, joins in the supplementary material mixture as bonding, wetting agent with the solution form and makes softwood; Sucralose is the conventional high-intensity sweeteners of food tablet, and sugariness is about 600 times of sucrose, is used for improving the sugariness of tablet, reduces the volume of effervescent tablet, is easy to carry and stores; Bubble enemy defoamer is mainly prepared burden and is dimethyl silicone polymer, glycerin monostearate calcium carbonate, polyoxyethylene sorbitan monostearate (polysorbate60), be used for eliminating the white foam that purple perilla effervescence tablet beverage surface is difficult to decorporate, do not influence effervesce disintegration effect, foaming phenomenon and gas production, also can improve the effervescence tablet beverage outward appearance; Polyethylene glycol (PEG) 8000 is a lubricant, and lubricity is strong, and anti-adhesive is good, makes effervescent tablet in pressing process, smoothly slice.
Description of drawings
Fig. 1 is preparation technology's flow chart of purple perilla effervescent tablet.
The specific embodiment
Below among all embodiment used extractive of perilla xeraphium all by this step preparation:
Take by weighing the 1000g perilla leaf, add 2L 80% (volumetric concentration) food grade ethanolic solution, smash to pieces with beater, in 50 ℃ of following stirring and leaching 60min, filter with 400 eye mesh screens, it is 8% that the filtrate vacuum is concentrated into solid content, centrifugal 15min under the condition of 8000rpm/min, the spray-dried extractive of perilla xeraphium of making.
Embodiment 1:
The purple perilla effervescent tablet that the present embodiment preparation is 300, the every heavy 2.5g of average sheet, formulated by supplementary material: extractive of perilla xeraphium 100g by following weight, citric acid 348g, sodium acid carbonate 230g, Arabic gum 50.25g, Sucralose 3.75g, bubble enemy defoamer 6g, polyvinylpyrrolidone 4.5g, PEG80007.5g.
Concrete preparation method following (preparation flow is seen Fig. 1):
Get extractive of perilla xeraphium, citric acid, sodium acid carbonate, Arabic gum, Sucralose, the pulverizing of bubble enemy defoamer, cross 100 mesh sieves, put in the granule-forming machine, add the ethanol solution 150ml contain 3% (g/ml) PVP again and mix and make softwood, and be cut into coarse granule automatically with 800rpm.Coarse granule is crossed 18 mesh sieves, make wet granular.Place fluid bed dryer in 50 ℃ of dry 30min wet granular.Dried particles is crossed 16 mesh sieves carry out whole grain, add PEG80007.5g, be dosed into compressing tablet in the rotary pelleting machine after mixing, make the tablet that average sheet heavily is about 2.5g, promptly get product purple perilla effervescent tablet of the present invention.
The effervescent tablet product sensory attributional analysis of present embodiment preparation is as follows:
Get a clean beaker, add 45～55 ℃ of 200ml hot water, 1 of the purple perilla nutrient effervescent tablets of input above-mentioned steps one preparation, observe its bubblement, treat the complete disintegration of effervescent tablet, when no gas is emitted, measure its disintegration time limited, and qualitative characteristics such as organoleptic analysis's purple perilla beverage mouthfeel, color and luster, smell, outward appearance, repeated test 6 times, analysis result sees Table 1.
Table 1 purple perilla effervescent tablet organoleptic quality analysis result
Embodiment 2:
The purple perilla effervescent tablet that the present embodiment preparation is 300, the every heavy 2.5g of average sheet, formulated by supplementary material: extractive of perilla xeraphium 175g, citric acid 287.6g, vitamin C 3.8g by following weight, sodium acid carbonate 190g, Arabic gum 67.5g, Sucralose 7.0g, bubble enemy defoamer 3.7g, PEG800011.2g, polyvinylpyrrolidone 4.2g.
Concrete preparation method is as follows:
Get extractive of perilla xeraphium, citric acid, sodium acid carbonate, vitamin C, Arabic gum, Sucralose, the pulverizing of bubble enemy defoamer, cross 100 mesh sieves, put in the granule-forming machine, add the ethanol solution 140ml contain 3% (g/ml) PVP again and mix and make softwood, and be cut into coarse granule automatically with 1000rpm.Coarse granule is crossed 18 mesh sieves, make wet granular.Place fluid bed dryer in 45 ℃ of dry 30min wet granular.Dried particles is crossed 16 mesh sieves carry out whole grain, add PEG8000 11.2g, be dosed into compressing tablet in the rotary pelleting machine after mixing, make the tablet that average sheet heavily is about 2.5g, the gained tablet through ultraviolet sterilization, is promptly got the purple perilla effervescent tablet of a kind of Vc of being rich in of product of the present invention.
The organoleptic quality analysis result of the mouthfeel of the purple perilla effervescent tablet of present embodiment preparation, color and luster, local flavor, outward appearance, bubble state etc. sees Table 2.
Table 2 is rich in the purple perilla effervescent tablet organoleptic quality analysis result of Vc
Embodiment 3:
The purple perilla effervescent tablet that the present embodiment preparation is 300, the every heavy 2.5g of average sheet, formulated by supplementary material: extractive of perilla xeraphium 37.5g, citric acid 395g, collagen peptide 7.5g by following weight, sodium acid carbonate 275.5g, Arabic gum 15g, Sucralose 2.7g, bubble enemy defoamer 1.5g, PEG8000 11.25g, polyvinylpyrrolidone 4.05g.
The concrete preparation method of present embodiment is as follows:
Get extractive of perilla xeraphium, citric acid, sodium acid carbonate, collagen peptide, Arabic gum, Sucralose, the pulverizing of bubble enemy defoamer, cross 100 mesh sieves, put in the granule-forming machine, add the ethanol solution volume 135ml contain 3% (g/ml) PVP again and mix and make softwood, and be cut into coarse granule automatically with 1000rpm.Coarse granule is crossed 18 mesh sieves, make wet granular.Place fluid bed dryer in 45 ℃ of dry 30min wet granular.Dried particles is crossed 16 mesh sieves carry out whole grain, add PEG800011.25g, be dosed into compressing tablet in the rotary pelleting machine after mixing, make the tablet that average sheet heavily is about 2.5g, the gained tablet through ultraviolet sterilization, is promptly got a kind of purple perilla effervescent tablet of the present invention.
The organoleptic quality analysis result of the mouthfeel of the purple perilla effervescent tablet of present embodiment preparation, color and luster, local flavor, outward appearance, bubble state etc. sees Table 3.
Table 3 is rich in the purple perilla effervescent tablet organoleptic quality analysis result of collagen peptide
Claims (10)
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Cited By (5)
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| CN103461612A (en) * | 2013-10-09 | 2013-12-25 | 北京绿源求证科技发展有限责任公司 | Food stomach-nourishing tea electuary protecting stomach lining |
| CN112220032A (en) * | 2020-09-28 | 2021-01-15 | 王利华 | Use of a thickening component for the preparation of a food product with reduced formation of blood alcohol after drinking and food product comprising said component |
| CN112516915A (en) * | 2020-12-31 | 2021-03-19 | 安徽联谊药业股份有限公司 | Granulator is used in western medicine processing with antiseized function that connects |
| CN113598379A (en) * | 2021-08-11 | 2021-11-05 | 红华御康生物科技(江苏)股份有限公司 | Small molecular peptide multiple biological nutrient and preparation method thereof |
| CN116210911A (en) * | 2023-02-02 | 2023-06-06 | 福建省深蓝生物科技有限公司 | Shark chondroitin sulfate high-calcium tablet and preparation method thereof |
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Cited By (6)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN103461612A (en) * | 2013-10-09 | 2013-12-25 | 北京绿源求证科技发展有限责任公司 | Food stomach-nourishing tea electuary protecting stomach lining |
| CN112220032A (en) * | 2020-09-28 | 2021-01-15 | 王利华 | Use of a thickening component for the preparation of a food product with reduced formation of blood alcohol after drinking and food product comprising said component |
| CN112516915A (en) * | 2020-12-31 | 2021-03-19 | 安徽联谊药业股份有限公司 | Granulator is used in western medicine processing with antiseized function that connects |
| CN113598379A (en) * | 2021-08-11 | 2021-11-05 | 红华御康生物科技(江苏)股份有限公司 | Small molecular peptide multiple biological nutrient and preparation method thereof |
| CN116210911A (en) * | 2023-02-02 | 2023-06-06 | 福建省深蓝生物科技有限公司 | Shark chondroitin sulfate high-calcium tablet and preparation method thereof |
| CN116210911B (en) * | 2023-02-02 | 2024-07-26 | 福建省深蓝生物科技有限公司 | Shark chondroitin sulfate high-calcium tablet and preparation method thereof |
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Application publication date: 20111228 |