CN100355368C - Health-care products with improving immunity and preventing radiative harm and production thereof - Google Patents
Health-care products with improving immunity and preventing radiative harm and production thereof Download PDFInfo
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- CN100355368C CN100355368C CNB2005100201887A CN200510020188A CN100355368C CN 100355368 C CN100355368 C CN 100355368C CN B2005100201887 A CNB2005100201887 A CN B2005100201887A CN 200510020188 A CN200510020188 A CN 200510020188A CN 100355368 C CN100355368 C CN 100355368C
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- 230000036039 immunity Effects 0.000 title claims abstract description 9
- LFQSCWFLJHTTHZ-UHFFFAOYSA-N Ethanol Chemical compound CCO LFQSCWFLJHTTHZ-UHFFFAOYSA-N 0.000 claims abstract description 78
- LRHPLDYGYMQRHN-UHFFFAOYSA-N N-Butanol Chemical compound CCCCO LRHPLDYGYMQRHN-UHFFFAOYSA-N 0.000 claims abstract description 48
- 239000000284 extract Substances 0.000 claims abstract description 36
- 239000000843 powder Substances 0.000 claims abstract description 26
- 244000077995 Coix lacryma jobi Species 0.000 claims abstract description 22
- XLYOFNOQVPJJNP-UHFFFAOYSA-N water Substances O XLYOFNOQVPJJNP-UHFFFAOYSA-N 0.000 claims abstract description 22
- 239000007788 liquid Substances 0.000 claims abstract description 18
- 230000005855 radiation Effects 0.000 claims abstract description 9
- 239000002775 capsule Substances 0.000 claims abstract description 7
- 241001061264 Astragalus Species 0.000 claims abstract 2
- 235000006533 astragalus Nutrition 0.000 claims abstract 2
- 239000000706 filtrate Substances 0.000 claims description 21
- 238000000605 extraction Methods 0.000 claims description 11
- 239000000047 product Substances 0.000 claims description 8
- 229920006395 saturated elastomer Polymers 0.000 claims description 7
- 238000010992 reflux Methods 0.000 claims description 5
- 239000006189 buccal tablet Substances 0.000 claims description 3
- 239000007910 chewable tablet Substances 0.000 claims description 3
- 230000002708 enhancing effect Effects 0.000 claims description 3
- 239000000796 flavoring agent Substances 0.000 claims description 3
- 239000003826 tablet Substances 0.000 claims description 3
- 239000012141 concentrate Substances 0.000 claims 2
- 240000008866 Ziziphus nummularia Species 0.000 claims 1
- 239000002021 butanolic extract Substances 0.000 claims 1
- 239000012530 fluid Substances 0.000 claims 1
- 235000013355 food flavoring agent Nutrition 0.000 claims 1
- 210000000582 semen Anatomy 0.000 claims 1
- 239000007921 spray Substances 0.000 claims 1
- 210000004233 talus Anatomy 0.000 claims 1
- 235000015112 vegetable and seed oil Nutrition 0.000 abstract description 14
- 244000269722 Thea sinensis Species 0.000 abstract description 6
- 150000004676 glycans Chemical class 0.000 abstract description 6
- 239000000463 material Substances 0.000 abstract description 6
- 229920001282 polysaccharide Polymers 0.000 abstract description 6
- 239000005017 polysaccharide Substances 0.000 abstract description 6
- 238000002360 preparation method Methods 0.000 abstract description 4
- 241000209140 Triticum Species 0.000 abstract description 3
- 235000021307 Triticum Nutrition 0.000 abstract description 3
- 238000000034 method Methods 0.000 abstract description 3
- 239000008267 milk Substances 0.000 abstract description 3
- 235000013336 milk Nutrition 0.000 abstract description 3
- 210000004080 milk Anatomy 0.000 abstract description 3
- 239000000203 mixture Substances 0.000 abstract description 3
- 239000000375 suspending agent Substances 0.000 abstract description 3
- 206010003549 asthenia Diseases 0.000 abstract description 2
- 238000000227 grinding Methods 0.000 abstract description 2
- 235000010110 Astragalus glycyphyllos Nutrition 0.000 abstract 1
- 208000006083 Hypokinesia Diseases 0.000 abstract 1
- 235000017784 Mespilus germanica Nutrition 0.000 abstract 1
- 244000182216 Mimusops elengi Species 0.000 abstract 1
- 235000000560 Mimusops elengi Nutrition 0.000 abstract 1
- 208000013738 Sleep Initiation and Maintenance disease Diseases 0.000 abstract 1
- 235000007837 Vangueria infausta Nutrition 0.000 abstract 1
- 206010022437 insomnia Diseases 0.000 abstract 1
- 238000002156 mixing Methods 0.000 abstract 1
- 235000021018 plums Nutrition 0.000 abstract 1
- 230000001376 precipitating effect Effects 0.000 abstract 1
- 230000002265 prevention Effects 0.000 abstract 1
- 230000001681 protective effect Effects 0.000 abstract 1
- 210000000952 spleen Anatomy 0.000 abstract 1
- 210000002784 stomach Anatomy 0.000 abstract 1
- 235000012054 meals Nutrition 0.000 description 6
- 238000004064 recycling Methods 0.000 description 6
- 238000001291 vacuum drying Methods 0.000 description 6
- 238000005406 washing Methods 0.000 description 6
- 238000006243 chemical reaction Methods 0.000 description 4
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- 239000009636 Huang Qi Substances 0.000 description 3
- 230000002051 biphasic effect Effects 0.000 description 3
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- KJCVRFUGPWSIIH-UHFFFAOYSA-N 1-naphthol Chemical compound C1=CC=C2C(O)=CC=CC2=C1 KJCVRFUGPWSIIH-UHFFFAOYSA-N 0.000 description 2
- 244000241838 Lycium barbarum Species 0.000 description 2
- 235000015459 Lycium barbarum Nutrition 0.000 description 2
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- 239000001116 FEMA 4028 Substances 0.000 description 1
- WQZGKKKJIJFFOK-GASJEMHNSA-N Glucose Natural products OC[C@H]1OC(O)[C@H](O)[C@@H](O)[C@@H]1O WQZGKKKJIJFFOK-GASJEMHNSA-N 0.000 description 1
- 208000007443 Neurasthenia Diseases 0.000 description 1
- 244000000231 Sesamum indicum Species 0.000 description 1
- 235000003434 Sesamum indicum Nutrition 0.000 description 1
- 230000002924 anti-infective effect Effects 0.000 description 1
- WHGYBXFWUBPSRW-FOUAGVGXSA-N beta-cyclodextrin Chemical compound OC[C@H]([C@H]([C@@H]([C@H]1O)O)O[C@H]2O[C@@H]([C@@H](O[C@H]3O[C@H](CO)[C@H]([C@@H]([C@H]3O)O)O[C@H]3O[C@H](CO)[C@H]([C@@H]([C@H]3O)O)O[C@H]3O[C@H](CO)[C@H]([C@@H]([C@H]3O)O)O[C@H]3O[C@H](CO)[C@H]([C@@H]([C@H]3O)O)O3)[C@H](O)[C@H]2O)CO)O[C@@H]1O[C@H]1[C@H](O)[C@@H](O)[C@@H]3O[C@@H]1CO WHGYBXFWUBPSRW-FOUAGVGXSA-N 0.000 description 1
- 235000011175 beta-cyclodextrine Nutrition 0.000 description 1
- 229960004853 betadex Drugs 0.000 description 1
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Landscapes
- Medicines Containing Plant Substances (AREA)
- Coloring Foods And Improving Nutritive Qualities (AREA)
Abstract
The present invention relates to a health-care product with the functions of immunity enhancement and radiation prevention and a preparation method thereof. The product is prepared from coix seeds, acanthopanax roots, milkvetch roots, spina date seeds, smoked plums and medlars. The method comprises: 1. extracting by water till the relative density of alcohol liquid concentration is 1.16 to 1.18, precipitating alcohol, extracting by normal butyl alcohol to obtain powdered extracts, and preparing the powdered extracts into capsules or tablets; 2. respectively extracting coix seed oil and spine date seed oil by 85 to 95% ethanol or in a supercritical mode, and preparing the coix seed oil, the spine date seed oil, polysaccharide powder and the powdered extracts into two-phase capsules; 3. grinding the coix seeds into superfine powder of 200 to 300 meshes, extracting the rest of the five medicinal materials by water to obtain powdered extracts, mixing the coix seed superfine powder and powdered extracts according to the proportion of 1:0.3 to 1, adding a suspending agent, and preparing the mixture into wheat tea or milk tea. The health-care product has the functions of replenishing qi, invigorating the spleen, nourishing the stomach and relieving uneasiness, and is suitable for people with spleen-kidney yang vacuity, asthenia, hypodynamia, insomnia and low organism immunity; the product also has a protective effect on radiation hazards.
Description
Technical field: the present invention relates to health products, particularly a kind of have the immunity of enhancing and radiation hazradial bundle had health products of defencive function and preparation method thereof.
Background technology: the harm of radiation is greatly, all may produce damage to all kinds of crowds, causes bringing out various morbid state, as: neurasthenia syndrome, hemopoietic system is impaired, and anti-infection ability descends, especially show as body's immunity and descend, make human body be in " subhealthy status ".In the prior art, to radiation hazradial bundle have the health products of assistant protection function mostly be greatly food form as; Sesame cream, noodles, biscuit etc., dose is big, takes inconvenience, and some taste should not be accepted.
Summary of the invention: the object of the present invention is to provide a kind of have strengthen immunity and radiation hazradial bundle had health products of defencive function and preparation method thereof; it is that article with dietotherapeutic are the health products that make on the basis by theory of traditional Chinese medical science, can reach the purpose that strengthens immunity and radiation hazradial bundle is had assistant protection function.
Formation of the present invention: it is to be made by the material medicine of following consumption: coix seed 15～25g, wilsonii 15～25g, the Radix Astragali 9～30g, spina date seed 15～25g, dark plum 15～25g, matrimony vine 6～12g.
(1) the medicinal decocting of above Six-element boils three times, add 10～12 times of amounts of water at every turn, the each decoction 1～1.5 hour, filter, merging filtrate, being concentrated into relative density is 1.08 (60 ℃), add ethanol, make to contain alcohol amount and reach 65%, left standstill 48 hours, filter, filtrate recycling ethanol, be condensed into liquid extract that relative density is 1.16～1.18 (room temperatures) or with 50%～90% hydrous ethanol refluxing extraction 5 times, each alcohol adding amount is 6～8 times, extracts 1～1.5 hour at every turn, filter, merging filtrate, reclaiming ethanol to relative density is the liquid extract of 1.16～1.18 (room temperatures), the said extracted thing is with water saturated extracting n-butyl alcohol 5 times, merge butanol extraction liquid, washing, recovered under reduced pressure n-butanol, spray-dried or vacuum drying, get extract powder, it is incapsulated or compressing tablet, sugar coating or film-coating, or the adding flavor enhancement is made buccal tablet and chewable tablets;
(2) coix seed, spina date seed is ground into meal respectively, extract 5 times with 85%～95% alcohol reflux respectively, each alcohol adding amount is 6～8 times, the each extraction 1 hour, filter, merging filtrate, reclaiming ethanol to relative density is 1.16～1.18 (room temperatures), get coix seed, the spine date seed oil liquid extract, or extract coix seed oil and spine date seed oil with supercritical carbon dioxide extraction method, oily later coix seed powder 1000g poach three times have been extracted, add 10～12 times in water at every turn, boiled 1 hour, filter, it is 1.08 (60 ℃) that filtrate is concentrated into relative density, add ethanol, make to contain the alcohol amount and reach 50%, the precipitation that filtering produces, reclaim ethanol and be concentrated into small size, add ethanol and make and contain the alcohol amount and reach more than 85%, left standstill 48 hours, filter, precipitation is dry, get the polysaccharide powder, extracted the oily later spiny jujuba seed powder and the Radix Astragali, wilsonii, dark plum and structure Qi four traditional Chinese medicine material meal mix, and use poach three times, add 10～12 times in water at every turn, boiled 1 hour, and filtered, it is 1.08 (60 ℃) that filtrate is concentrated into relative density, add ethanol, make to contain alcohol amount and reach 60%, filter filtrate recycling ethanol, be condensed into the liquid extract that relative density is 1.16～1.18 (room temperatures), with water saturated extracting n-butyl alcohol 5 times, merge butanol extraction liquid, washing, the recovered under reduced pressure n-butanol, spray-dried or vacuum drying, dry extract, above-mentioned coix seed oil, spine date seed oil, polysaccharide powder and extract powder adopt biphasic capsule to load and make the biphasic capsule agent;
(3) coix seed is ground into 200～300 purpose ultra micro powder with ultra micro powder technology, standby, all the other five tastes medicinal materials are ground into meal poach three times, add 10～12 times in water at every turn, boiled 1 hour, and filtered, it is 1.08 (60 ℃) that filtrate is concentrated into relative density, add ethanol, make to contain alcohol amount and reach 60%, filter filtrate recycling ethanol, be condensed into the liquid extract that relative density is 1.16～1.18 (room temperatures), with water saturated extracting n-butyl alcohol 5 times, merge butanol extraction liquid, washing, the recovered under reduced pressure n-butanol, spray-dried or vacuum drying, dry extract, coix seed ultra micro powder mixes with 1: 0.3～1 ratio with extract powder, the suspending agent of adding 0.1～0.5% is made wheat tea or milk tea according to a conventional method after the seasoning.
The polysaccharide powder has following properties: white amorphous powder, every 1g powder dissolution in 25ml water the time pH value be 7.0, soluble in water; Color reaction: Molish reaction, alphanaphthol reaction is positive reaction; Obtain glucose after the hydrolysis, galactolipin.
Compared with the prior art, the present invention gives full play to the theoretical advantage of China's Traditional health care, in conjunction with subjects such as modern pharmacology, galenic pharmacy, Food Sciences, enrichment effect component is made and can be shown effect performance, technology advanced person, formulation is reasonable, is convenient to the new health care product of taking and carrying.
The specific embodiment: embodiment (one): the medicinal decocting of above Six-element boils three times, add 10～12 times of amounts of water at every turn, the each decoction 1～1.5 hour, filter, merging filtrate, being concentrated into relative density is 1.08 (60 ℃), adds ethanol, make and contain alcohol amount and reach 65%, left standstill 48 hours, and filtered filtrate recycling ethanol, be condensed into liquid extract that relative density is 1.16～1.18 (room temperatures) or with 50%～90% hydrous ethanol refluxing extraction 5 times, each alcohol adding amount is 6～8 times, extracts 1～1.5 hour at every turn, filters, merging filtrate, reclaiming ethanol is the liquid extract of 1.16～1.18 (room temperatures) to relative density.The said extracted thing merges butanol extraction liquid with water saturated extracting n-butyl alcohol 5 times, washing, the recovered under reduced pressure n-butanol, spray-dried or vacuum drying, extract powder.Incapsulate or compressing tablet sugar coating or film-coating.Or the adding flavor enhancement is made buccal tablet and chewable tablets.
Embodiment (two): coix seed, spina date seed are ground into meal respectively, extract 5 times with 85%～95% alcohol reflux respectively, each alcohol adding amount is 6～8 times, the each extraction 1 hour, filter, merging filtrate, reclaiming ethanol to relative density is 1.16～1.18 (room temperatures), gets coix seed, spine date seed oil liquid extract.Or extract coix seed oil and spine date seed oil with supercritical carbon dioxide extraction method.Extracted oily later coix seed powder 1000g poach three times, added 10～12 times in water at every turn, boiled 1 hour, filter, it is 1.08 (60 ℃) that filtrate is concentrated into relative density, adds ethanol, make and contain alcohol amount and reach 50%, the precipitation that filtering produces reclaims ethanol and is concentrated into small size, adds ethanol and makes and contain the alcohol amount and reach more than 85%, left standstill 48 hours, filter, precipitation is dry, gets the polysaccharide powder.Having extracted oily later spiny jujuba seed powder mixes with the Radix Astragali, wilsonii, dark plum and matrimony vine four traditional Chinese medicine material meal, with poach three times, add 10～12 times in water at every turn, boiled 1 hour, filter, it is 1.08 (60 ℃) that filtrate is concentrated into relative density, adds ethanol, make and contain alcohol amount and reach 60%, filter, filtrate recycling ethanol is condensed into the liquid extract that relative density is 1.16～1.18 (room temperatures), with water saturated extracting n-butyl alcohol 5 times, merge butanol extraction liquid, washing, recovered under reduced pressure n-butanol, spray-dried or vacuum drying, dry extract.Above-mentioned coix seed oil, spine date seed oil adopt beta-cyclodextrin inclusion compound to get the inclusion compound powder, press 0.5～2: 50～150 with coix seed polysaccharide powder and dry extract again; 30～100 ratio is mixed, and adopts biphasic capsule to load and makes capsule.
Embodiment (three): the coix seed ultramicro grinding becomes 200～300 purpose ultra micro powder, and is standby.All the other five tastes medicinal materials are ground into meal poach three times, add 10～12 times in water at every turn, boil 1 hour, filter, it is 1.08 (60 ℃) that filtrate is concentrated into relative density, adds ethanol, make to contain alcohol amount and reach 60%, filter filtrate recycling ethanol, be condensed into the liquid extract that relative density is 1.16～1.18 (room temperatures),, merge butanol extraction liquid with water saturated extracting n-butyl alcohol 5 times, washing, the recovered under reduced pressure n-butanol, spray-dried or vacuum drying gets dry extract.Coix seed ultra micro powder mixes with 1: 0.3～1 ratio with extract powder, adds 0.1～0.5% suspending agent, makes wheat tea or milk tea after the seasoning according to a conventional method.
Claims (1)
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| Application Number | Priority Date | Filing Date | Title |
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| CNB2005100201887A CN100355368C (en) | 2005-01-11 | 2005-01-11 | Health-care products with improving immunity and preventing radiative harm and production thereof |
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| Application Number | Priority Date | Filing Date | Title |
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| CNB2005100201887A CN100355368C (en) | 2005-01-11 | 2005-01-11 | Health-care products with improving immunity and preventing radiative harm and production thereof |
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| Publication Number | Publication Date |
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| CN1644095A CN1644095A (en) | 2005-07-27 |
| CN100355368C true CN100355368C (en) | 2007-12-19 |
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| CNB2005100201887A Expired - Fee Related CN100355368C (en) | 2005-01-11 | 2005-01-11 | Health-care products with improving immunity and preventing radiative harm and production thereof |
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Families Citing this family (10)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN101596246B (en) * | 2009-07-02 | 2011-10-26 | 北京中农普康生物科技有限公司 | Smoked plum extractive and wild jujube seed extractive compound preparation as well as preparation method and application thereof |
| CN102578315B (en) * | 2012-02-16 | 2013-05-15 | 王裕森 | Anti-radiation health care tea and preparation method thereof |
| CN102919373B (en) * | 2012-11-29 | 2013-09-11 | 仲珉 | Health milk tea granule |
| CN102936561B (en) * | 2012-11-29 | 2013-11-13 | 蒋朝芳 | Health white spirit |
| CN103053907B (en) * | 2013-01-22 | 2014-01-01 | 山西大学 | Functional food for regulating yang-deficiency susceptible constitution and preparation method thereof |
| CN103599265B (en) * | 2013-11-26 | 2016-03-30 | 中国人民解放军海军医学研究所 | A kind of compound traditional Chinese medicine for radiation protection |
| CN104116101A (en) * | 2014-06-26 | 2014-10-29 | 焦敏 | Syzygium samarangense and wild jujube seed nerve-calming milk tea and preparation method thereof |
| CN106337309B (en) * | 2015-07-08 | 2018-03-09 | 中国中医科学院西苑医院 | A kind of high-purity and in high yield Job's tears water-soluble cellulose preparation method |
| CN110974873A (en) * | 2018-12-06 | 2020-04-10 | 泰州医药城国科化物生物医药科技有限公司 | Spina date seed oil inclusion compound and preparation method and application thereof |
| CN110679812A (en) * | 2019-11-08 | 2020-01-14 | 遵义医药高等专科学校 | Research method of preparation process of lachryma-jobi seed compound anti-radiation beverage |
Citations (2)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN1170588A (en) * | 1996-07-16 | 1998-01-21 | 郝来勤 | Pure natural plant human life energy nutritive substrate |
| CN1528209A (en) * | 2003-09-29 | 2004-09-15 | �������¿��汣��ʳƷ����˾ | Health-care food with immune modulation and cltiradiation function and preparing method thereof |
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2005
- 2005-01-11 CN CNB2005100201887A patent/CN100355368C/en not_active Expired - Fee Related
Patent Citations (2)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN1170588A (en) * | 1996-07-16 | 1998-01-21 | 郝来勤 | Pure natural plant human life energy nutritive substrate |
| CN1528209A (en) * | 2003-09-29 | 2004-09-15 | �������¿��汣��ʳƷ����˾ | Health-care food with immune modulation and cltiradiation function and preparing method thereof |
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| CN1644095A (en) | 2005-07-27 |
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