Conforms to US OSHA Hazard Communication 29CFR1910.

1200

SAFETY DATA SHEET

Electrospray Tuning Mix

Section 1. Identification
Product name : Electrospray Tuning Mix
Part No. : G2431A, G2421-60001, G2431-60001
Validation date : 09/05/2013.
Relevant identified uses of the substance or mixture and uses advised against
Material uses : Analytical chemistry.
A 1x100ml. container

Supplier/Manufacturer : Agilent Technologies, Inc.

Logistics Center - Americas
500 Ships Landing Way
New Castle, Delaware 19720
800-227-9770

In case of emergency : CHEMTREC®: 1-800-424-9300

Section 2. Hazards identification

OSHA/HCS status : This material is considered hazardous by the OSHA Hazard Communication Standard
(29 CFR 1910.1200).
Classification of the : FLAMMABLE LIQUIDS - Category 2
substance or mixture ACUTE TOXICITY: SKIN - Category 4
ACUTE TOXICITY: INHALATION - Category 4
SERIOUS EYE DAMAGE/ EYE IRRITATION - Category 2A
SPECIFIC TARGET ORGAN TOXICITY (REPEATED EXPOSURE) [blood system,
central nervous system (CNS), kidneys and liver] - Category 2

GHS label elements

Hazard pictograms :

Signal word : Danger

Hazard statements : Highly flammable liquid and vapor.
Harmful in contact with skin or if inhaled.
Causes serious eye irritation.
May cause damage to organs through prolonged or repeated exposure. (blood system,
central nervous system (CNS), kidneys, liver)
Precautionary statements
Prevention : P280 - Wear protective gloves. Wear eye or face protection. Wear protective clothing.
P210 - Keep away from heat, sparks, open flames and hot surfaces. - No smoking.
P241 - Use explosion-proof electrical, ventilating, lighting and all material-handling
equipment.
P242 - Use only non-sparking tools.
P243 - Take precautionary measures against static discharge.
P233 - Keep container tightly closed.
P271 - Use only outdoors or in a well-ventilated area.
P260 - Do not breathe vapor.

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Section 2. Hazards identification

P264 - Wash hands thoroughly after handling.
Response : P314 - Get medical attention if you feel unwell.
P304 + P340 + P312 - IF INHALED: Remove victim to fresh air and keep at rest in a
position comfortable for breathing. Call a POISON CENTER or physician if you feel
unwell.
P303 + P361 + P353 - IF ON SKIN (or hair): Take off immediately all contaminated
clothing. Rinse skin with water or shower.
P302 + P352 + P312 - IF ON SKIN: Wash with plenty of soap and water. Call a
POISON CENTER or physician if you feel unwell.
P305 + P351 + P338 - IF IN EYES: Rinse cautiously with water for several minutes.
Remove contact lenses, if present and easy to do. Continue rinsing.
P337 + P313 - If eye irritation persists: Get medical attention.
Storage : P403 - Store in a well-ventilated place.
P235 - Keep cool.
Disposal : P501 - Dispose of contents and container in accordance with all local, regional, national
and international regulations.
Hazards not otherwise : None known.
classified

Section 3. Composition/information on ingredients

Substance/mixture : Mixture

Ingredient name % CAS number

Acetonitrile 60 - 100 75-05-8
Any concentration shown as a range is to protect confidentiality or is due to batch variation.
There are no additional ingredients present which, within the current knowledge of the supplier and in the
concentrations applicable, are classified as hazardous to health or the environment and hence require reporting
in this section.
Occupational exposure limits, if available, are listed in Section 8.

Section 4. First aid measures

Description of necessary first aid measures
Eye contact : Immediately flush eyes with plenty of water, occasionally lifting the upper and lower
eyelids. Check for and remove any contact lenses. Continue to rinse for at least 10
minutes. Get medical attention.
Inhalation : Remove victim to fresh air and keep at rest in a position comfortable for breathing. If it
is suspected that fumes are still present, the rescuer should wear an appropriate mask
or self-contained breathing apparatus. If not breathing, if breathing is irregular or if
respiratory arrest occurs, provide artificial respiration or oxygen by trained personnel. It
may be dangerous to the person providing aid to give mouth-to-mouth resuscitation.
Get medical attention following exposure or if feeling unwell. If necessary, call a poison
center or physician. If unconscious, place in recovery position and get medical attention
immediately. Maintain an open airway. Loosen tight clothing such as a collar, tie, belt
or waistband. In case of inhalation of decomposition products in a fire, symptoms may
be delayed. The exposed person may need to be kept under medical surveillance for
48 hours.
Skin contact : Wash with plenty of soap and water. Remove contaminated clothing and shoes. Wash
contaminated clothing thoroughly with water before removing it, or wear gloves.
Continue to rinse for at least 10 minutes. Get medical attention following exposure or if
feeling unwell. If necessary, call a poison center or physician. Wash clothing before
reuse. Clean shoes thoroughly before reuse.

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Section 4. First aid measures

Ingestion : Wash out mouth with water. Remove dentures if any. Remove victim to fresh air and
keep at rest in a position comfortable for breathing. If material has been swallowed and
the exposed person is conscious, give small quantities of water to drink. Stop if the
exposed person feels sick as vomiting may be dangerous. Do not induce vomiting
unless directed to do so by medical personnel. If vomiting occurs, the head should be
kept low so that vomit does not enter the lungs. Get medical attention following
exposure or if feeling unwell. Never give anything by mouth to an unconscious person.
If unconscious, place in recovery position and get medical attention immediately.
Maintain an open airway. Loosen tight clothing such as a collar, tie, belt or waistband.

Most important symptoms/effects, acute and delayed

Potential acute health effects
Eye contact : Causes serious eye irritation.
Inhalation : Harmful if inhaled. Exposure to decomposition products may cause a health hazard.
Serious effects may be delayed following exposure.
Skin contact : Harmful in contact with skin.
Ingestion : Irritating to mouth, throat and stomach.
Over-exposure signs/symptoms
Eye contact : Adverse symptoms may include the following:
pain or irritation
watering
redness
Inhalation : No specific data.
Skin contact : No specific data.
Ingestion : No specific data.

Indication of immediate medical attention and special treatment needed, if necessary

Notes to physician : In case of inhalation of decomposition products in a fire, symptoms may be delayed.
The exposed person may need to be kept under medical surveillance for 48 hours.
Specific treatments : No specific treatment.
Protection of first-aiders : No action shall be taken involving any personal risk or without suitable training. If it is
suspected that fumes are still present, the rescuer should wear an appropriate mask or
self-contained breathing apparatus. It may be dangerous to the person providing aid to
give mouth-to-mouth resuscitation. Wash contaminated clothing thoroughly with water
before removing it, or wear gloves.

See toxicological information (Section 11)

Section 5. Fire-fighting measures

Extinguishing media
Suitable extinguishing : Use dry chemical, CO₂, water spray (fog) or foam.
media
Unsuitable extinguishing : Do not use water jet.
media

Specific hazards arising : Highly flammable liquid and vapor. In a fire or if heated, a pressure increase will occur
from the chemical and the container may burst, with the risk of a subsequent explosion. The vapor/gas is
heavier than air and will spread along the ground. Vapors may accumulate in low or
confined areas or travel a considerable distance to a source of ignition and flash back.
Runoff to sewer may create fire or explosion hazard.

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Section 5. Fire-fighting measures

Hazardous thermal : Decomposition products may include the following materials:
decomposition products carbon dioxide
carbon monoxide
nitrogen oxides
cyanides

Special protective actions : Promptly isolate the scene by removing all persons from the vicinity of the incident if
for fire-fighters there is a fire. No action shall be taken involving any personal risk or without suitable
training. Move containers from fire area if this can be done without risk. Use water
spray to keep fire-exposed containers cool.
Special protective : Fire-fighters should wear appropriate protective equipment and self-contained breathing
equipment for fire-fighters apparatus (SCBA) with a full face-piece operated in positive pressure mode.

Section 6. Accidental release measures

Personal precautions, protective equipment and emergency procedures
For non-emergency : No action shall be taken involving any personal risk or without suitable training.
personnel Evacuate surrounding areas. Keep unnecessary and unprotected personnel from
entering. Do not touch or walk through spilled material. Shut off all ignition sources.
No flares, smoking or flames in hazard area. Avoid breathing vapor or mist. Provide
adequate ventilation. Wear appropriate respirator when ventilation is inadequate. Put
on appropriate personal protective equipment.
For emergency responders : If specialised clothing is required to deal with the spillage, take note of any information
in Section 8 on suitable and unsuitable materials. See also the information in "For non-
emergency personnel".

Environmental precautions : Avoid dispersal of spilled material and runoff and contact with soil, waterways, drains
and sewers. Inform the relevant authorities if the product has caused environmental
pollution (sewers, waterways, soil or air).

Methods and materials for containment and cleaning up

Stop leak if without risk. Move containers from spill area. Use spark-proof tools and explosion-proof equipment. Dilute
with water and mop up if water-soluble. Alternatively, or if water-insoluble, absorb with an inert dry material and place in an
appropriate waste disposal container. Dispose of via a licensed waste disposal contractor.

Section 7. Handling and storage

Precautions for safe handling
Protective measures : Put on appropriate personal protective equipment (see Section 8). Do not breathe
vapor or mist. Do not ingest. Avoid contact with eyes, skin and clothing. Use only with
adequate ventilation. Wear appropriate respirator when ventilation is inadequate. Do
not enter storage areas and confined spaces unless adequately ventilated. Keep in the
original container or an approved alternative made from a compatible material, kept
tightly closed when not in use. Store and use away from heat, sparks, open flame or
any other ignition source. Use explosion-proof electrical (ventilating, lighting and
material handling) equipment. Use only non-sparking tools. Take precautionary
measures against electrostatic discharges. Empty containers retain product residue
and can be hazardous. Do not reuse container.
Advice on general : Eating, drinking and smoking should be prohibited in areas where this material is
occupational hygiene handled, stored and processed. Workers should wash hands and face before eating,
drinking and smoking. Remove contaminated clothing and protective equipment before
entering eating areas. See also Section 8 for additional information on hygiene
measures.

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Section 7. Handling and storage

Conditions for safe storage, : Store in accordance with local regulations. Store in a segregated and approved area.
including any Store in original container protected from direct sunlight in a dry, cool and well-ventilated
incompatibilities area, away from incompatible materials (see Section 10) and food and drink. Eliminate
all ignition sources. Separate from oxidizing materials. Keep container tightly closed
and sealed until ready for use. Containers that have been opened must be carefully
resealed and kept upright to prevent leakage. Do not store in unlabeled containers.
Use appropriate containment to avoid environmental contamination.

Section 8. Exposure controls/personal protection

Control parameters
Occupational exposure limits
Ingredient name Exposure limits
Acetonitrile ACGIH TLV (United States, 3/2012).
Absorbed through skin.
TWA: 20 ppm 8 hours.
NIOSH REL (United States, 1/2013).
TWA: 34 mg/m³ 10 hours.
TWA: 20 ppm 10 hours.
OSHA PEL (United States, 6/2010).
TWA: 70 mg/m³ 8 hours.
TWA: 40 ppm 8 hours.
OSHA PEL 1989 (United States, 3/1989).
STEL: 105 mg/m³ 15 minutes.
STEL: 60 ppm 15 minutes.
TWA: 70 mg/m³ 8 hours.
TWA: 40 ppm 8 hours.

Appropriate engineering : Use only with adequate ventilation. Use process enclosures, local exhaust ventilation or
controls other engineering controls to keep worker exposure to airborne contaminants below any
recommended or statutory limits. The engineering controls also need to keep gas,
vapor or dust concentrations below any lower explosive limits. Use explosion-proof
ventilation equipment.
Environmental exposure : Emissions from ventilation or work process equipment should be checked to ensure
controls they comply with the requirements of environmental protection legislation. In some
cases, fume scrubbers, filters or engineering modifications to the process equipment
will be necessary to reduce emissions to acceptable levels.

Individual protection measures

Hygiene measures : Wash hands, forearms and face thoroughly after handling chemical products, before
eating, smoking and using the lavatory and at the end of the working period.
Appropriate techniques should be used to remove potentially contaminated clothing.
Wash contaminated clothing before reusing. Ensure that eyewash stations and safety
showers are close to the workstation location.
Eye/face protection : Safety eyewear complying with an approved standard should be used when a risk
assessment indicates this is necessary to avoid exposure to liquid splashes, mists,
gases or dusts. If contact is possible, the following protection should be worn, unless
the assessment indicates a higher degree of protection: chemical splash goggles.
Skin protection

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Section 8. Exposure controls/personal protection

Hand protection : Chemical-resistant, impervious gloves complying with an approved standard should be
worn at all times when handling chemical products if a risk assessment indicates this is
necessary. Considering the parameters specified by the glove manufacturer, check
during use that the gloves are still retaining their protective properties. It should be
noted that the time to breakthrough for any glove material may be different for different
glove manufacturers. In the case of mixtures, consisting of several substances, the
protection time of the gloves cannot be accurately estimated.
Body protection : Personal protective equipment for the body should be selected based on the task being
performed and the risks involved and should be approved by a specialist before
handling this product. When there is a risk of ignition from static electricity, wear anti-
static protective clothing. For the greatest protection from static discharges, clothing
should include anti-static overalls, boots and gloves.
Other skin protection : Appropriate footwear and any additional skin protection measures should be selected
based on the task being performed and the risks involved and should be approved by a
specialist before handling this product.
Respiratory protection : Use a properly fitted, air-purifying or air-fed respirator complying with an approved
standard if a risk assessment indicates this is necessary. Respirator selection must be
based on known or anticipated exposure levels, the hazards of the product and the safe
working limits of the selected respirator.

Section 9. Physical and chemical properties

Appearance
Physical state : Liquid.
Color : Colorless.
Odor : Ether-like
Odor threshold : Not available.
pH : Not applicable.
Melting point : -45°C (-49°F)
Boiling point : 81.6°C (178.9°F)
Flash point : Closed cup: 12.8°C (55°F)
Evaporation rate : 5.79 (butyl acetate = 1)
Flammability (solid, gas) : Not available.
Lower and upper explosive : Lower: 4.4%
(flammable) limits Upper: 16%
Vapor pressure : 11.6 kPa (87 mm Hg) [room temperature]
Vapor density : 1.42 [Air = 1]
Relative density : 0.787
Solubility : Soluble in the following materials: cold water and hot water.
Solubility in water : Not available.
Partition coefficient: n- : Not available.
octanol/water
Auto-ignition temperature : Not available.
Decomposition temperature : Not available.
Viscosity : Not available.

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Section 10. Stability and reactivity

Reactivity : No specific test data related to reactivity available for this product or its ingredients.

Chemical stability : The product is stable.

Possibility of hazardous : Under normal conditions of storage and use, hazardous reactions will not occur.
reactions

Conditions to avoid : Avoid all possible sources of ignition (spark or flame). Do not pressurize, cut, weld,
braze, solder, drill, grind or expose containers to heat or sources of ignition. Do not
allow vapor to accumulate in low or confined areas.

Incompatible materials : Reactive or incompatible with the following materials:

oxidizing materials
Other: metals, acids, alkalis and moisture.

Hazardous decomposition : Under normal conditions of storage and use, hazardous decomposition products should
products not be produced.

Section 11. Toxicological information

Information on toxicological effects
Acute toxicity
Product/ingredient name Result Species Dose Exposure
Acetonitrile LC50 Inhalation Gas. Rat 17100 ppm 4 hours
LD50 Dermal Rabbit 980 mg/kg -
LD50 Oral Rat 2460 mg/kg -
Irritation/Corrosion
Product/ingredient name Result Species Score Exposure Observation
Acetonitrile Eyes - Moderate irritant Rabbit - 24 hours 100 -
microliters
Skin - Mild irritant Rabbit - 500 -
milligrams
Sensitization
Not available.

Mutagenicity
Not available.

Carcinogenicity
Not available.

Reproductive toxicity
Not available.

Teratogenicity
Not available.

Specific target organ toxicity (single exposure)

Not available.

Specific target organ toxicity (repeated exposure)

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Section 11. Toxicological information

Name Category Route of Target organs
exposure
Acetonitrile Category 2 Not determined blood system,
central nervous
system (CNS),
kidneys and liver
Aspiration hazard
Not available.

Information on the likely : Not available.

routes of exposure
Potential acute health effects
Eye contact : Causes serious eye irritation.
Inhalation : Harmful if inhaled. Exposure to decomposition products may cause a health hazard.
Serious effects may be delayed following exposure.
Skin contact : Harmful in contact with skin.
Ingestion : Irritating to mouth, throat and stomach.

Symptoms related to the physical, chemical and toxicological characteristics

Eye contact : Adverse symptoms may include the following:
pain or irritation
watering
redness
Inhalation : No specific data.
Skin contact : No specific data.
Ingestion : No specific data.

Delayed and immediate effects and also chronic effects from short and long term exposure
Short term exposure
Potential immediate : Not available.
effects
Potential delayed effects : Not available.
Long term exposure
Potential immediate : Not available.
effects
Potential delayed effects : Not available.
Potential chronic health effects
Not available.

General : May cause damage to organs through prolonged or repeated exposure.

Carcinogenicity : No known significant effects or critical hazards.
Mutagenicity : No known significant effects or critical hazards.
Teratogenicity : No known significant effects or critical hazards.
Developmental effects : No known significant effects or critical hazards.
Fertility effects : No known significant effects or critical hazards.

Numerical measures of toxicity

Acute toxicity estimates

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Section 11. Toxicological information

Route ATE value
Oral 2589.5 mg/kg
Dermal 1031.6 mg/kg
Inhalation (gases) 18000 ppm

Section 12. Ecological information

Toxicity
Product/ingredient name Result Species Exposure
Acetonitrile Acute IC50 3685000 µg/l Fresh water Aquatic plants - Lemna minor 96 hours
Acute LC50 3600000 µg/l Fresh water Daphnia - Daphnia magna 48 hours
Acute LC50 100 mg/l Fresh water Fish - Pimephales promelas - 96 hours
Juvenile (Fledgling, Hatchling,
Weanling)
Chronic NOEC 1000000 µg/l Fresh water Aquatic plants - Lemna minor 96 hours
Chronic NOEC 160000 µg/l Fresh water Daphnia - Daphnia magna 21 days

Persistence and degradability

Product/ingredient name Aquatic half-life Photolysis Biodegradability
Acetonitrile - - Readily

Bioaccumulative potential
Product/ingredient name LogPow BCF Potential
Acetonitrile -0.34 - low

Mobility in soil
Soil/water partition : Not available.
coefficient (KOC)

Other adverse effects : No known significant effects or critical hazards.

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Section 13. Disposal considerations

Disposal methods : The generation of waste should be avoided or minimized wherever possible. Disposal
of this product, solutions and any by-products should at all times comply with the
requirements of environmental protection and waste disposal legislation and any
regional local authority requirements. Dispose of surplus and non-recyclable products
via a licensed waste disposal contractor. Waste should not be disposed of untreated to
the sewer unless fully compliant with the requirements of all authorities with jurisdiction.
Waste packaging should be recycled. Incineration or landfill should only be considered
when recycling is not feasible. This material and its container must be disposed of in a
safe way. Care should be taken when handling emptied containers that have not been
cleaned or rinsed out. Empty containers or liners may retain some product residues.
Vapor from product residues may create a highly flammable or explosive atmosphere
inside the container. Do not cut, weld or grind used containers unless they have been
cleaned thoroughly internally. Avoid dispersal of spilled material and runoff and contact
with soil, waterways, drains and sewers.
Disposal should be in accordance with applicable regional, national and local laws and regulations. Local
regulations may be more stringent than regional or national requirements.

The information presented below only applies to the material as supplied. The identification based on
characteristic(s) or listing may not apply if the material has been used or otherwise contaminated. It is the
responsibility of the waste generator to determine the toxicity and physical properties of the material generated to
determine the proper waste identification and disposal methods in compliance with applicable regulations.

Refer to Section 7: HANDLING AND STORAGE and Section 8: EXPOSURE CONTROLS/PERSONAL PROTECTION
for additional handling information and protection of employees.

Section 14. Transport information

Regulatory UN number Proper shipping Classes PG* Label Additional
information name information

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Section 14. Transport information

DOT UN1648 Acetonitrile solution 3 II Reportable quantity
RQ(Acetonitrile 5263.2 lbs / 2389.5 kg
(Neat)) [802.07 gal / 3036.2 L]
Package sizes
shipped in quantities
less than the product
reportable quantity are
not subject to the RQ
(reportable quantity)
transportation
requirements.

Limited quantity
Yes.

Packaging
instruction
Passenger aircraft
Quantity limitation: 5 L
Packaging
instructions: 173.161

Cargo aircraft
Quantity limitation: 60
L
Packaging
instructions: Inner
packagings must not
exceed 250 mL or
250 g. The total
quantity in any one kit
must not exceed 1 L
or 1 kg. The total
quantity in any one
package must not
exceed 10 kg.

Special provisions
IB2, T7, TP2

Remarks
Requires Dangerous
Goods BOL

TDG UN1648 ACETONITRILE 3 II Explosive Limit and

solution Limited Quantity
Index
1

Passenger Carrying
Road or Rail Index
5
Mexico UN1648 ACETONITRILO 3 II -
solution

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Section 14. Transport information

IMDG UN1648 ACETONITRILE 3 II Emergency
solution schedules (EmS)
F-E, S-D

IATA UN1648 Acetonitrile solution 3 II Passenger and

Cargo Aircraft
Quantity limitation: 5 L
Packaging
instructions: 353
Cargo Aircraft Only
Quantity limitation: 60
L
Packaging
instructions: 364
Limited Quantities -
Passenger Aircraft
Quantity limitation: 1 L
Packaging
instructions: Y341

Remarks
A44 Requires
Shipper's Declaration
of Dangerous Goods

PG* : Packing group

Section 15. Regulatory information

U.S. Federal regulations : TSCA 8(a) PAIR: Acetonitrile
United States inventory (TSCA 8b): At least one component is not listed.
Clean Water Act (CWA) 307: Acetonitrile

Clean Air Act Section 112 : Listed

(b) Hazardous Air
Pollutants (HAPs)
Clean Air Act Section 602 : Not listed
Class I Substances
Clean Air Act Section 602 : Not listed
Class II Substances
DEA List I Chemicals : Not listed
(Precursor Chemicals)
DEA List II Chemicals : Not listed
(Essential Chemicals)
SARA 302/304
Composition/information on ingredients
No products were found.

SARA 304 RQ : Not applicable.

SARA 311/312
Classification : Fire hazard
Immediate (acute) health hazard
Delayed (chronic) health hazard
Composition/information on ingredients

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Section 15. Regulatory information

Name % Fire Sudden Reactive Immediate Delayed
hazard release of (acute) (chronic)
pressure health health
hazard hazard
Acetonitrile 60 - 100 Yes. No. No. Yes. Yes.

SARA 313
Product name CAS number %
Form R - Reporting Acetonitrile 75-05-8 60 - 100
requirements
Supplier notification Acetonitrile 75-05-8 60 - 100

SARA 313 notifications must not be detached from the SDS and any copying and redistribution of the SDS shall include
copying and redistribution of the notice attached to copies of the SDS subsequently redistributed.
State regulations
Massachusetts : The following components are listed: ACETONITRILE
New York : The following components are listed: Acetonitrile; Ethanenitrile
New Jersey : The following components are listed: ACETONITRILE; CYANOMETHANE
Pennsylvania : The following components are listed: ACETONITRILE
California Prop. 65
No products were found.
Canada inventory : Not determined.
International regulations
International lists : Australia inventory (AICS): At least one component is not listed.
China inventory (IECSC): At least one component is not listed.
Japan inventory: Not determined.
Korea inventory: Not determined.
Malaysia Inventory (EHS Register): Not determined.
New Zealand Inventory of Chemicals (NZIoC): Not determined.
Philippines inventory (PICCS): Not determined.
Taiwan inventory (CSNN): Not determined.
Chemical Weapons : Not listed
Convention List Schedule
I Chemicals
Chemical Weapons : Not listed
Convention List Schedule
II Chemicals
Chemical Weapons : Not listed
Convention List Schedule
III Chemicals

Section 16. Other information

History
Date of issue : 09/05/2013.
Date of previous issue : 08/28/2013.
Version : 4.1
Indicates information that has changed from previously issued version.
Notice to reader

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Section 16. Other information

Disclaimer: The information contained in this document is based on Agilent’s state of knowledge at the time of
preparation. No warranty as to its accurateness, completeness or suitability for a particular purpose is expressed
or implied.

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