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WO2002041907A1 - The additive in food, drug, cosmetics for supplying $g(g) linolenic acid and the process of producing them - Google Patents

The additive in food, drug, cosmetics for supplying $g(g) linolenic acid and the process of producing them Download PDF

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Publication number
WO2002041907A1
WO2002041907A1 PCT/CN2001/001572 CN0101572W WO0241907A1 WO 2002041907 A1 WO2002041907 A1 WO 2002041907A1 CN 0101572 W CN0101572 W CN 0101572W WO 0241907 A1 WO0241907 A1 WO 0241907A1
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oil
linolenic acid
green
food
medicine
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PCT/CN2001/001572
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Chinese (zh)
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Sheng Ruan
Yanmei Zhu
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Sheng Ruan
Yanmei Zhu
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Priority to AU2002221496A priority Critical patent/AU2002221496A1/en
Publication of WO2002041907A1 publication Critical patent/WO2002041907A1/en

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    • A—HUMAN NECESSITIES
    • A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
    • A61K—PREPARATIONS FOR MEDICAL, DENTAL OR TOILETRY PURPOSES
    • A61K31/00—Medicinal preparations containing organic active ingredients
    • A61K31/185—Acids; Anhydrides, halides or salts thereof, e.g. sulfur acids, imidic, hydrazonic or hydroximic acids
    • A61K31/19—Carboxylic acids, e.g. valproic acid
    • A61K31/20—Carboxylic acids, e.g. valproic acid having a carboxyl group bound to a chain of seven or more carbon atoms, e.g. stearic, palmitic, arachidic acids
    • A—HUMAN NECESSITIES
    • A23—FOODS OR FOODSTUFFS; TREATMENT THEREOF, NOT COVERED BY OTHER CLASSES
    • A23D—EDIBLE OILS OR FATS, e.g. MARGARINES, SHORTENINGS OR COOKING OILS
    • A23D9/00—Other edible oils or fats, e.g. shortenings or cooking oils
    • A—HUMAN NECESSITIES
    • A23—FOODS OR FOODSTUFFS; TREATMENT THEREOF, NOT COVERED BY OTHER CLASSES
    • A23L—FOODS, FOODSTUFFS OR NON-ALCOHOLIC BEVERAGES, NOT OTHERWISE PROVIDED FOR; PREPARATION OR TREATMENT THEREOF
    • A23L33/00—Modifying nutritive qualities of foods; Dietetic products; Preparation or treatment thereof
    • A23L33/10—Modifying nutritive qualities of foods; Dietetic products; Preparation or treatment thereof using additives
    • A23L33/115—Fatty acids or derivatives thereof; Fats or oils
    • A23L33/12—Fatty acids or derivatives thereof
    • A—HUMAN NECESSITIES
    • A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
    • A61P—SPECIFIC THERAPEUTIC ACTIVITY OF CHEMICAL COMPOUNDS OR MEDICINAL PREPARATIONS
    • A61P9/00—Drugs for disorders of the cardiovascular system
    • A—HUMAN NECESSITIES
    • A23—FOODS OR FOODSTUFFS; TREATMENT THEREOF, NOT COVERED BY OTHER CLASSES
    • A23V—INDEXING SCHEME RELATING TO FOODS, FOODSTUFFS OR NON-ALCOHOLIC BEVERAGES AND LACTIC OR PROPIONIC ACID BACTERIA USED IN FOODSTUFFS OR FOOD PREPARATION
    • A23V2002/00—Food compositions, function of food ingredients or processes for food or foodstuffs

Definitions

  • the present invention is a food, medicine, cosmetic additive and process for supplementing Y-linolenic acid. Background technique
  • the designer of this invention relies on many years of practical experience in various fields of research, production, and processing of various nutritional and health care products, and based on repeated research and demonstration, makes a brand-new design, which finally results in the invention.
  • the purpose of the present invention is to provide a food, a medicine, a cosmetic additive rich in gamma linolenic acid without a toxic amount, and a preparation process thereof.
  • the food, medicine and cosmetic additive for supplementing ⁇ -linolenic acid according to the present invention are made from green fragrant oil.
  • the green fragrant oil is oil squeezed from green pine tree seeds or oil from green pine leaves or oil from green pine tree flowers.
  • the oil may be crude oil, refined oil or emulsified oil.
  • ⁇ -linolenic acid has functions of lowering blood lipids, thrombolysis, and cholesterol.
  • Current ⁇ -linolenic acid is derived from evening primrose.
  • a herbaceous plant originating in North America, China is mainly in the northeast mountainous area, the oil content is about 20%, and the refined ⁇ -linolenic acid is only 7-10%.
  • Y-linolenic acid has a lipid-lowering effect on serum triglycerides. It is the best drug for treating hyperlipidemia. It has a good effect on reducing total cholesterol and ⁇ -lipoprotein. It can lower blood lipids, prevent arrhythmia, and lose weight.
  • the additive oil of the present invention has a very rich linolenic acid content, which is more than double the content of the products of existing manufacturers in the world. , More than double the evening primrose oil content, does not contain poison. It is an additive rich in linolenic acid.
  • the raw materials obtained by the present invention are very rich, and are particularly suitable for the development of poverty-stricken areas.
  • the samples of the invention and other varieties of linolenic acid, linoleic acid, and oleic acid are shown in Table 1 below.
  • Embodiment 1 The food, medicine and cosmetic additives of this embodiment are made of green fragrant oil.
  • the green fragrant oil is oil squeezed from the green pine tree seeds.
  • Embodiment 2 The food, medicine and cosmetic additives of this embodiment are made of green fragrant oil.
  • the green fragrant oil is oil squeezed from the green pine tree seeds.
  • Embodiment 3 The food, medicine, and cosmetic additives of this embodiment are made of green fragrant oil.
  • the green fragrant oil is oil extracted from the flowers of the green pine tree.
  • Qingsong is Yunnan Qingsong.
  • the specific implementation process of the present invention is to clean the green pine tree seeds, leaves or camellia raw materials, and then enter the pre-treatment section, use a closed grinder to pulverize, and put the pulverized raw materials into a clean bag for CO 2 supercritical. extraction; 002 is to use supercritical extraction process 002 is a supercritical fluid, under high pressure conditions in contact with the raw meal to be extracted, the operating pressure and temperature regulation systems, the green vanilla extract oil. Subsequently, by reducing the pressure or adjusting the temperature, the density of the supercritical fluid is reduced, and the extracted green fragrant oil is contacted with. 0 2 The supercritical fluid is separated in a separator.
  • the present invention can provide a natural plant application, through which an additive rich in y linolenic acid and not containing a toxic amount can be obtained.
  • the present invention is a novel, progressive and highly practical
  • the above-mentioned new inventions are the specific embodiments of the present invention and the technical principles used. If the equivalent changes are made according to the concept of the present invention, the functional effects still do not exceed those covered by the description and drawings. It should be noted that the spirit should be within the scope of the present invention. Table 1

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  • Food Science & Technology (AREA)
  • Polymers & Plastics (AREA)
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  • General Health & Medical Sciences (AREA)
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  • General Chemical & Material Sciences (AREA)
  • Nuclear Medicine, Radiotherapy & Molecular Imaging (AREA)
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Abstract

The invention disclosed a additive in food, drug, cosmetic for supplying η linolenic acid and the process thereof. The characteristic of the invention is the application of the oil extracted from the seed, leaf and flower of pine tree. The oil said above are rich in η linolenic acid and linoleic acid and have the effect of reducing blood fat, dissolving thrombus, reducing cholesterol. It can be added in food, drug and Cosmetic and are beneficial to the health of human body.

Description

用于补充 Y亚麻酸的食品， 药品， 化妆品添加剂及其工艺 技术领域  Food, medicine, cosmetic additive and technology for supplementing Y-linolenic acid
本发明为一种用于补充 Y亚麻酸的食品， 药品， 化妆品添加剂及其工艺。 背景技术  The present invention is a food, medicine, cosmetic additive and process for supplementing Y-linolenic acid. Background technique
现有的食品， 药品， 化妆品添加剂种类很多， 也富含营养成份， 但多数不含 或少量含有 y亚麻酸。 有的虽含有 y亚麻酸但有含有相当高的蓄毒量， 这些蓄毒 量又不易分离提纯： 如沙棘； 现广泛使用的为月见草油。 发明内容  There are many types of existing food, pharmaceutical, and cosmetic additives, and they are also rich in nutrients, but most of them do not contain or contain a small amount of linolenic acid. Some contain ylinolenic acid but have a relatively high toxic amount, which is not easy to separate and purify: such as sea buckthorn; now widely used is evening primrose oil. Summary of the Invention
有鉴于此， 如何能应用一种天然植物， 通过其能得到一种富含 γ亚麻酸又不 含有蓄毒量的添加剂， 正是本发明的研创动机所在。  In view of this, how to apply a natural plant to obtain an additive rich in gamma linolenic acid without containing a toxic amount is exactly the motivation for the research and development of the present invention.
本发明设计人凭借多年从事各类营养保健品技术研究生产加工等领域的实际 经验， 在反复研究论证的基础上， 做一全新设计， 终得本发明的产生。  The designer of this invention relies on many years of practical experience in various fields of research, production, and processing of various nutritional and health care products, and based on repeated research and demonstration, makes a brand-new design, which finally results in the invention.
本发明的发明目的就是要提供一种含有丰富 γ亚麻酸又不含蓄毒量的食品， 药品， 化妆品添加剂及其制备工艺。  The purpose of the present invention is to provide a food, a medicine, a cosmetic additive rich in gamma linolenic acid without a toxic amount, and a preparation process thereof.
本发明的用于补充 γ亚麻酸的食品， 药品， 化妆品添加剂是应用青香子油。 所述的青香子油是从青松树子中榨出的油或者青松树叶中搾出的油或者青松树花 中搾出的油。 所述的油可以是粗油， 也可以是精炼油或乳化油。  The food, medicine and cosmetic additive for supplementing γ-linolenic acid according to the present invention are made from green fragrant oil. The green fragrant oil is oil squeezed from green pine tree seeds or oil from green pine leaves or oil from green pine tree flowers. The oil may be crude oil, refined oil or emulsified oil.
本发明的效果是这样的， 根据研究， γ亚麻酸有降血脂， 溶血栓， 降胆固醇 的作用， 目前的 γ亚麻酸是来源于月见草中提炼的， 月见草是构叶菜科多年生草 本植物， 原产北美洲， 中国主要在东北山区， 含油量约为 20%， 提炼出的 γ亚麻 酸仅为 7-10%, 而青香子特别适合于中国云南独特的气候条件下生长， 年产量达 The effect of the present invention is as follows. According to research, γ-linolenic acid has functions of lowering blood lipids, thrombolysis, and cholesterol. Current γ-linolenic acid is derived from evening primrose. A herbaceous plant originating in North America, China is mainly in the northeast mountainous area, the oil content is about 20%, and the refined γ-linolenic acid is only 7-10%. Output reached
1-5千万公斤， 含油量为 38.2， 其中 Y亚麻酸的含量约为 21%， 由此看出， 青香 子在资源和质量上均具有优势， 发明人通过多年来对中国云南多产的上百种木 本、 草本植物做了研究， 最终发现了青香子为 γ亚麻酸含量的植物， 故以其应用 于食品药品及化妆品添加剂的使用， Y亚麻酸对血清甘油三脂有降脂作用， 是治 疗高血脂症疗效最佳药物， 对降低血清总胆固醇， β脂蛋白均有较好的疗效， 降 血脂、 抗心律不齐、 减肥， 用于防治动脉粥样硬化、 高血脂、 肥胖等症； 作为食 品添加剂， 开发一系列含 Y亚麻酸的营养调整剂特种食品和营养品， 特别适用于 婴儿、 老年人及恢复期病人； Υ亚麻酸还具有重要的生理生化功能， 在人体皮肤 的营养健美、 保护及疗效方面， 可以起重要的作用， 可使皮肤变嫩， 可防衰老作 用， 由上可知本发明的添加剂油， 其 γ亚麻酸含量非常丰富， 超过世界现有厂商 产品含量的一倍以上， 超过月见草油含量一倍以上， 不含蓄毒。 为一种 Υ亚麻酸 含量丰富的添加剂。 另外， 本发明所获得的原料非常丰富， 特别适合贫困地区开 发脱困。 发明样品与其它品种亚麻酸， 亚油酸， 油酸含量见下表 1。 本发明具体实施方式 10-50 million kg, with an oil content of 38.2, of which the content of Y linolenic acid is about 21%. It can be seen that Qingxiangzi has advantages in terms of resources and quality. The inventor has over the years Hundreds of woody and herbaceous plants have been researched. Finally, green incense was found to be a plant with γ-linolenic acid content. Therefore, it is used in food and pharmaceutical and cosmetic additives. Y-linolenic acid has a lipid-lowering effect on serum triglycerides. It is the best drug for treating hyperlipidemia. It has a good effect on reducing total cholesterol and β-lipoprotein. It can lower blood lipids, prevent arrhythmia, and lose weight. It is used to prevent atherosclerosis, hyperlipidemia, obesity, etc. Disease Product additives, to develop a series of special foods and nutrition products containing Y linolenic acid, especially suitable for infants, the elderly and patients in recovery period; linolenic acid also has important physiological and biochemical functions, nutrition and bodybuilding in human skin, In terms of protection and efficacy, it can play an important role in making the skin tender and anti-aging. It can be seen from the above that the additive oil of the present invention has a very rich linolenic acid content, which is more than double the content of the products of existing manufacturers in the world. , More than double the evening primrose oil content, does not contain poison. It is an additive rich in linolenic acid. In addition, the raw materials obtained by the present invention are very rich, and are particularly suitable for the development of poverty-stricken areas. The samples of the invention and other varieties of linolenic acid, linoleic acid, and oleic acid are shown in Table 1 below. DETAILED DESCRIPTION OF THE INVENTION
实施例 1， 本实施例食品， 药品， 化妆品添加剂是应用青香子油。 所述的青 香子油是从青松树子中榨出的油。  Embodiment 1. The food, medicine and cosmetic additives of this embodiment are made of green fragrant oil. The green fragrant oil is oil squeezed from the green pine tree seeds.
实施例 2， 本实施例食品， 药品， 化妆品添加剂是应用青香子油。 所述的青 香子油是从青松树子中榨出的油。  Embodiment 2. The food, medicine and cosmetic additives of this embodiment are made of green fragrant oil. The green fragrant oil is oil squeezed from the green pine tree seeds.
实施例 3， 本实施例食品， 药品， 化妆品添加剂是应用青香子油。 所述的青 香子油是从青松树花中榨出的油。 青松为云南青松。  Embodiment 3. The food, medicine, and cosmetic additives of this embodiment are made of green fragrant oil. The green fragrant oil is oil extracted from the flowers of the green pine tree. Qingsong is Yunnan Qingsong.
本发明的具体实现工艺是将青松树子、 树叶或茶花原料， 经清洗干燥后进入 予处理工段，采用封闭型粉碎机进行粉碎，将粉碎过的原料装入洁净袋中，供 CO2 超临界萃取； 002超临界萃取过程是采用 002为超临界流体， 在高压条件下与待 萃取的原料粉接触， 调节系统的操作压力和温度， 萃取出青香子油。 随后通过降 压或调节温度的方法， 降低超临界流体的密度， 使萃取出的青香子油与。02超临 界流体在分离器中分离。 The specific implementation process of the present invention is to clean the green pine tree seeds, leaves or camellia raw materials, and then enter the pre-treatment section, use a closed grinder to pulverize, and put the pulverized raw materials into a clean bag for CO 2 supercritical. extraction; 002 is to use supercritical extraction process 002 is a supercritical fluid, under high pressure conditions in contact with the raw meal to be extracted, the operating pressure and temperature regulation systems, the green vanilla extract oil. Subsequently, by reducing the pressure or adjusting the temperature, the density of the supercritical fluid is reduced, and the extracted green fragrant oil is contacted with. 0 2 The supercritical fluid is separated in a separator.
综上所述， 本发明能提供一种天然植物的应用， 通过其能得到一种富含 y亚 麻酸又不含有蓄毒量的添加剂， 显然本发明为一种新颖、 进步并深具实用性的新 发明， 以上所述乃是本发明的具体实施例及所运用的技术原理， 若依本发明的构 想所作的等效改变， 其所产生的功能作用仍未超出说明书及附图所涵盖的精神 时， 均应在本发明的范围内， 特此说明。 表 1 In summary, the present invention can provide a natural plant application, through which an additive rich in y linolenic acid and not containing a toxic amount can be obtained. Obviously, the present invention is a novel, progressive and highly practical The above-mentioned new inventions are the specific embodiments of the present invention and the technical principles used. If the equivalent changes are made according to the concept of the present invention, the functional effects still do not exceed those covered by the description and drawings. It should be noted that the spirit should be within the scope of the present invention. Table 1
含亚麻酸及亚油酸的药材归类表  Classification of medicinal materials containing linolenic acid and linoleic acid
\类别 \ Category
总油 亚 油 油酸 植物 产地 ( %) 亚麻酸 酸 ( %) 来源 ( %) 药材 \ 类型  Total oil Linoleic acid Plant Origin (%) Linolenic acid (%) Source (%) Medicinal materials \ Type
样品 Υ - 23. 2 37. 09  Sample Υ-23. 2 37. 09
柳时菜科： 月见草 南、 北美洲 28. 3 Υ - 9. 85 75. 79 6. 738 黄花月见草 温带， 我国 15. 8 Υ - 7. 84 72. 00 13. 13 粉花月见草 主产东北， 23. 4 Υ - 8. 20 71. 13 6. 809 月见草 待宵草 云南等地也 17. 8 Υ- 7. 00 73. 02 9. 377 槌果月见草籽 产 24. 3 Υ - 7. 33 75. 69 9. 384 亚麻子 亚麻科亚麻成熟种子 内蒙东北等 30-48 a- 35-55 25-35 15-20 沙棘 胡秃子科沙棘的种子 三北西南等 6. 0 26. 2 36. 63 23. 16 火麻仁 桑科大麻的成熟种子 30. 0 25. 0 53. 0 12. 0 琉璃苣 紫草科琉璃苣的种子 31. 0 Y - 20. 0 37. 18 19. 12 苏子 唇形科紫苏成熟果实 45. 0 a- 57. 0  Salixaceae: Evening Primrose South, North America 28. 3 Υ-9. 85 75. 79 6. 738 Yellow flower Evening Primrose temperate, China 15. 8 Υ-7. 84 72. 00 13. 13 Pink flower month Primrose is mainly produced in the northeast, 23. 4 Υ-8. 20 71. 13 6. 809 Evening primrose is waiting for night grass. Yunnan and other places are also 17. 8 Υ-7. 00 73. 02 9. 377 Yield 24.3 Υ-7. 33 75. 69 9. 384 Flax seeds Flax family Flax mature seeds Northeast Inner Mongolia, etc. 30-48 a- 35-55 25-35 15-20 Seabuckthorn Pelicaceae Seabuckthorn seeds Three Northwest Southwest etc. 6. 0 26. 2 36. 63 23. 16 Mature seeds of hemp mulberry hemp 30. 0 25. 0 53. 0 12. 0 Borage seeds Borage Borage 31.0 Y-20. 0 37. 18 19. 12 Ripe fruits of Perilla frutescens in the labiatae family 45.0 a- 57.0
葶苈子 十字花科独行果实 15-20 7. 54 32. 5 25. 1 余甘子 大域科癸甘子的果实 26. 0 8. 3 44. 0 28. 4 黑加仑 Ribes ngrum L 引种 Y- 16. 0 40. 10 子 a- 18. 20  Gardenia cruciferae lone fruit 15-20 7. 54 32. 5 25. 1 Yuganzi large field family deciduous fruit 26. 0 8. 3 44. 0 28. 4 Blackcurrant Ribes ngrum L Introduction Y-16. 0 40. 10 Suba- 18. 20
倒提壶 紫草科倒提壶的种子 云南 Y - 27. 0  Inverted pot seed Boraginaceae Inverted pot seed Yunnan Y-27.0
苦否仁 蔷薇科山杏等的种子 生产北方 50. 1 0. 2 27. 4 67. 0 备注：以上百分比均为重量百分 Λ， 除以上所列药材夕 、，还有以下药材；女贞子（油酸和 亚麻酸等为 80. 5%,夜樱草（Y -亚麻酸 10. 0%)八月札、 苘麻子、 青果、 小茴香等均含有 亚麻酸及亚油酸。  The production of seeds from the bitter rose family Apricotaceae and other apricots in the north 50. 1 0. 2 27. 4 67. 0 Note: The above percentages are weight percentages. In addition to the herbs listed above, there are also the following herbs; Seeds (oleic acid and linolenic acid are 80.5%, night primrose (Y-linolenic acid 10.0%) August azalea, ramie seeds, green fruit, cumin, etc. all contain linoleic acid and linoleic acid.

Claims

权利要求 Rights request
1、 一种用于补充 Y亚麻酸的食品， 药品， 化妆品添加剂， 其特征在于是应 用青香子油。 1. A food, medicine, and cosmetic additive for supplementing Y-linolenic acid, which is characterized by applying green sesame oil.
2、 根据权利要求 1 所述的用于补充 Υ亚麻酸的食品， 药品， 化妆品添加剂， 其特征在于所述的青香子油是从青松树子中榨出的油。  2. The food, medicine, and cosmetic additive for supplementing linolenic acid according to claim 1, wherein the green fragrant oil is an oil squeezed from the green pine tree seeds.
3、 根据权利要求 1 所述的用于补充 Υ亚麻酸的食品， 药品， 化妆品添加剂， 其特征在于所述的青香子油是从青松树子中榨出的油。  3. The food, medicine, and cosmetic additive for supplementing linolenic acid according to claim 1, wherein the green fragrant oil is an oil extracted from the green pine tree seeds.
4、 根据权利要求 1 所述的用于补充 Υ亚麻酸的食品， 药品， 化妆品添加剂， 其特征在于所述的青香子油是从青松树花中榨出的油。  4. The food, medicine, and cosmetic additive for supplementing linolenic acid according to claim 1, wherein the green fragrant oil is an oil squeezed from the green pine tree flower.
5、 用于补充 Υ亚麻酸的食品， 药品， 化妆品添加剂的工艺， 其特征在于将 青松树子、 树叶或茶花原料， 经清洗干燥后进入予处理工段， 釆用封闭型粉碎机 进行粉碎， 将粉碎过的原料装入洁净袋中， 供 CO2超临界萃取； CO2超临界萃取 过程是采用 002为超临界流体， 在高压条件下与待萃取的原料粉接触， 调节系统 的操作压力和温度， 萃取出青香子油， 随后通过降压或调节温度的方法， 降低超 临界流体的密度， 使萃取出的青香子油与 CO2超临界流体在分离器中分离。 5. The process for supplementing linolenic acid with food, medicine, and cosmetic additives, which is characterized in that the green pine tree seeds, leaves or camellia raw materials are washed and dried and then entered into a pre-treatment section. The crushed raw materials are packed into clean bags for CO 2 supercritical extraction. The CO 2 supercritical extraction process uses 00 2 as a supercritical fluid and contacts the raw material powder to be extracted under high pressure conditions to adjust the operating pressure of the system and The green fragrant oil is extracted at a temperature, and then the density of the supercritical fluid is reduced by reducing the pressure or adjusting the temperature, so that the extracted fragrant oil is separated from the CO 2 supercritical fluid in a separator.
PCT/CN2001/001572 2000-11-24 2001-11-20 The additive in food, drug, cosmetics for supplying $g(g) linolenic acid and the process of producing them WO2002041907A1 (en)

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Citations (2)

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CN1118218A (en) * 1995-03-16 1996-03-13 姜训书 Production of pine-seed oil and edible health-care oil
CN1296761A (en) * 2000-12-01 2001-05-30 阮生 Health-care pine tea

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