TW340839B - Simultaneous preparation of caprolactam and hexamethylenediamine - Google Patents
Simultaneous preparation of caprolactam and hexamethylenediamineInfo
- Publication number
- TW340839B TW340839B TW084101079A TW84101079A TW340839B TW 340839 B TW340839 B TW 340839B TW 084101079 A TW084101079 A TW 084101079A TW 84101079 A TW84101079 A TW 84101079A TW 340839 B TW340839 B TW 340839B
- Authority
- TW
- Taiwan
- Prior art keywords
- distillation
- product
- hexamethylenediamine
- give
- column
- Prior art date
Links
Classifications
-
- C—CHEMISTRY; METALLURGY
- C07—ORGANIC CHEMISTRY
- C07C—ACYCLIC OR CARBOCYCLIC COMPOUNDS
- C07C209/00—Preparation of compounds containing amino groups bound to a carbon skeleton
- C07C209/44—Preparation of compounds containing amino groups bound to a carbon skeleton by reduction of carboxylic acids or esters thereof in presence of ammonia or amines, or by reduction of nitriles, carboxylic acid amides, imines or imino-ethers
- C07C209/48—Preparation of compounds containing amino groups bound to a carbon skeleton by reduction of carboxylic acids or esters thereof in presence of ammonia or amines, or by reduction of nitriles, carboxylic acid amides, imines or imino-ethers by reduction of nitriles
-
- C—CHEMISTRY; METALLURGY
- C07—ORGANIC CHEMISTRY
- C07D—HETEROCYCLIC COMPOUNDS
- C07D201/00—Preparation, separation, purification or stabilisation of unsubstituted lactams
- C07D201/16—Separation or purification
-
- C—CHEMISTRY; METALLURGY
- C07—ORGANIC CHEMISTRY
- C07D—HETEROCYCLIC COMPOUNDS
- C07D201/00—Preparation, separation, purification or stabilisation of unsubstituted lactams
- C07D201/02—Preparation of lactams
- C07D201/08—Preparation of lactams from carboxylic acids or derivatives thereof, e.g. hydroxy carboxylic acids, lactones or nitriles
Landscapes
- Chemical & Material Sciences (AREA)
- Organic Chemistry (AREA)
- Organic Low-Molecular-Weight Compounds And Preparation Thereof (AREA)
- Low-Molecular Organic Synthesis Reactions Using Catalysts (AREA)
- Preparation Of Compounds By Using Micro-Organisms (AREA)
- Polyamides (AREA)
Applications Claiming Priority (1)
Application Number | Priority Date | Filing Date | Title |
---|---|---|---|
DE19500222A DE19500222A1 (de) | 1995-01-05 | 1995-01-05 | Verfahren zur gleichzeitigen Herstellung von Caprolactam und Hexamethylendiamin |
Publications (1)
Publication Number | Publication Date |
---|---|
TW340839B true TW340839B (en) | 1998-09-21 |
Family
ID=7751046
Family Applications (1)
Application Number | Title | Priority Date | Filing Date |
---|---|---|---|
TW084101079A TW340839B (en) | 1995-01-05 | 1995-02-09 | Simultaneous preparation of caprolactam and hexamethylenediamine |
Country Status (18)
Country | Link |
---|---|
EP (1) | EP0801647B1 (zh) |
JP (1) | JP3708549B2 (zh) |
KR (1) | KR100386706B1 (zh) |
CN (1) | CN1064353C (zh) |
AT (1) | ATE242217T1 (zh) |
AU (1) | AU4347396A (zh) |
BG (1) | BG63431B1 (zh) |
BR (1) | BR9510133A (zh) |
CZ (1) | CZ289886B6 (zh) |
DE (2) | DE19500222A1 (zh) |
ES (1) | ES2201127T3 (zh) |
FI (1) | FI972839A0 (zh) |
MY (1) | MY112196A (zh) |
PL (1) | PL187887B1 (zh) |
RU (1) | RU2153493C2 (zh) |
SK (1) | SK84297A3 (zh) |
TW (1) | TW340839B (zh) |
WO (1) | WO1996020931A1 (zh) |
Families Citing this family (17)
Publication number | Priority date | Publication date | Assignee | Title |
---|---|---|---|---|
DE19636765A1 (de) * | 1996-09-10 | 1998-03-12 | Basf Ag | Verfahren zur gleichzeitigen Herstellung von 6-Aminocapronitril und Hexamethylendiamin |
DE19636766A1 (de) * | 1996-09-10 | 1998-03-12 | Basf Ag | Verfahren zur gleichzeitigen Herstellung von 6-Aminocapronitril und Hexamethylendiamin |
DE19704612A1 (de) * | 1997-02-07 | 1998-08-13 | Basf Ag | Verfahren zur Gewinnung von Hexamethylendiamin aus Hexamethylendiamin enthaltenden Mischungen |
DE19704620A1 (de) | 1997-02-07 | 1998-08-13 | Basf Ag | Verfahren zur Abtrennung von 6-Aminocapronitril aus Mischungen, die 6-Aminocapronitril und ein Imin enthalten |
DE19704614A1 (de) * | 1997-02-07 | 1998-08-13 | Basf Ag | Verfahren zur Abtrennnung eines Imins aus einer Mischung enthaltend ein Amin und ein Imin |
DE19704616A1 (de) * | 1997-02-07 | 1998-08-13 | Basf Ag | Verfahren zur Abtrennung von 2-Aminomethylcyclopentylamin aus einer Mischung enthaltend Hexamethylendiamin und 2-Aminomethylcyclopentylamin |
DE19704613A1 (de) | 1997-02-07 | 1998-08-13 | Basf Ag | Verfahren zur Abtrennung von 6-Aminocapronsäurenitril aus Mischungen, die 6-Aminocapronsäurenitril und ein Imin enthalten |
DE19812427A1 (de) * | 1998-03-20 | 1999-09-23 | Basf Ag | Verfahren zur Abtrennung eines Azepin-Derivats aus einer Mischung enthaltend ein Amin und ein Azepin-Derivat |
DE19842905A1 (de) * | 1998-09-18 | 2000-03-23 | Basf Ag | Verfahren zur gleichzeitigen Herstellung eines cyclischen Lactams und eines cyclischen Amins |
DE10010825A1 (de) * | 2000-03-08 | 2001-09-13 | Basf Ag | Verfahren zur Abtrennung eines Azepin-Derivats aus einer Mischung enthaltend ein Amin und ein Azepin-Derivat |
MY127068A (en) * | 2000-06-05 | 2006-11-30 | Basf Ag | Removal of ammonia from solutions including caprolactam and ammonia |
DE10029187A1 (de) * | 2000-06-19 | 2001-12-20 | Basf Ag | Verfahren zur Abtrennung von 6-Aminocapronitril aus Gemischen, die 6-Aminocapronitril, Adipodinitril und Hexamethylendiamin enthalten |
DE10223827A1 (de) | 2002-05-28 | 2003-12-11 | Basf Ag | Verfahren zur Reduzierung des Gehalts an einem ungesättigten Amin in einer Mischung enthaltend ein Aminonitril, ein Diamin, ein Dinitril oder deren Gemische |
US7208632B2 (en) * | 2004-09-10 | 2007-04-24 | Invista North America S.A R.L. | Separation of 6-aminocapronitrile and hexamethylenediamine from a mixture comprising hexamethylenediamine, 6-aminocapronitrile and tetrahydroazepine |
FR2892118B1 (fr) | 2005-10-18 | 2010-12-10 | Rhodia Recherches & Tech | Procede de fabrication d'hexamethylene diamine et d'aminocapronitrile. |
FR2902425B1 (fr) * | 2006-06-20 | 2008-07-18 | Rhodia Recherches & Tech | Procede de fabrication de diamines primaires |
CN112876381B (zh) * | 2021-04-14 | 2024-01-26 | 江苏扬农化工集团有限公司 | 一种气相法制备6-氨基己腈的模拟移动床装置及方法 |
Family Cites Families (3)
Publication number | Priority date | Publication date | Assignee | Title |
---|---|---|---|---|
DE954416C (de) * | 1952-11-04 | 1956-12-20 | Basf Ag | Verfahren zur Herstellung von Aminonitrilen und Diaminen |
GB1179706A (en) * | 1966-07-22 | 1970-01-28 | Ici Ltd | Organic Amines |
DE2606364C3 (de) * | 1976-02-18 | 1988-05-26 | Basf Ag, 6700 Ludwigshafen | Verfahren zur Stofftrennung aus einem flüssigen Gemisch durch fraktionierte Kristallisation |
-
1995
- 1995-01-05 DE DE19500222A patent/DE19500222A1/de not_active Withdrawn
- 1995-02-09 TW TW084101079A patent/TW340839B/zh active
- 1995-12-20 MY MYPI95003990A patent/MY112196A/en unknown
- 1995-12-22 WO PCT/EP1995/005115 patent/WO1996020931A1/de active IP Right Grant
- 1995-12-22 CZ CZ19972027A patent/CZ289886B6/cs not_active IP Right Cessation
- 1995-12-22 RU RU97113741/04A patent/RU2153493C2/ru not_active IP Right Cessation
- 1995-12-22 BR BR9510133A patent/BR9510133A/pt not_active IP Right Cessation
- 1995-12-22 AU AU43473/96A patent/AU4347396A/en not_active Abandoned
- 1995-12-22 ES ES95942198T patent/ES2201127T3/es not_active Expired - Lifetime
- 1995-12-22 DE DE59510717T patent/DE59510717D1/de not_active Expired - Fee Related
- 1995-12-22 SK SK842-97A patent/SK84297A3/sk unknown
- 1995-12-22 CN CN95197256A patent/CN1064353C/zh not_active Expired - Fee Related
- 1995-12-22 KR KR1019970704616A patent/KR100386706B1/ko not_active IP Right Cessation
- 1995-12-22 JP JP52005596A patent/JP3708549B2/ja not_active Expired - Fee Related
- 1995-12-22 EP EP95942198A patent/EP0801647B1/de not_active Expired - Lifetime
- 1995-12-22 AT AT95942198T patent/ATE242217T1/de not_active IP Right Cessation
- 1995-12-22 PL PL32126795A patent/PL187887B1/pl not_active IP Right Cessation
-
1997
- 1997-06-24 BG BG101661A patent/BG63431B1/bg unknown
- 1997-07-02 FI FI972839A patent/FI972839A0/fi not_active IP Right Cessation
Also Published As
Publication number | Publication date |
---|---|
CN1171782A (zh) | 1998-01-28 |
WO1996020931A1 (de) | 1996-07-11 |
BG63431B1 (bg) | 2002-01-31 |
CZ202797A3 (cs) | 1998-02-18 |
SK84297A3 (en) | 1998-03-04 |
DE59510717D1 (de) | 2003-07-10 |
FI972839A (fi) | 1997-07-02 |
EP0801647A1 (de) | 1997-10-22 |
AU4347396A (en) | 1996-07-24 |
EP0801647B1 (de) | 2003-06-04 |
MX9704863A (es) | 1997-10-31 |
JP3708549B2 (ja) | 2005-10-19 |
CZ289886B6 (cs) | 2002-04-17 |
JPH10511361A (ja) | 1998-11-04 |
ES2201127T3 (es) | 2004-03-16 |
KR19980701227A (ko) | 1998-05-15 |
MY112196A (en) | 2001-04-30 |
BR9510133A (pt) | 1997-12-30 |
DE19500222A1 (de) | 1996-07-11 |
CN1064353C (zh) | 2001-04-11 |
ATE242217T1 (de) | 2003-06-15 |
PL187887B1 (pl) | 2004-10-29 |
FI972839A0 (fi) | 1997-07-02 |
PL321267A1 (en) | 1997-11-24 |
BG101661A (en) | 1998-02-27 |
KR100386706B1 (ko) | 2003-08-21 |
RU2153493C2 (ru) | 2000-07-27 |
Similar Documents
Publication | Publication Date | Title |
---|---|---|
TW340839B (en) | Simultaneous preparation of caprolactam and hexamethylenediamine | |
CA1182775A (en) | Process for the purification of n-caprolactam | |
US6599398B1 (en) | Recovery of adiponitrile from a mixture of adiponitrile, aminocapronitrile and hexamethylenediamine | |
KR890002082A (ko) | 감마-부티로락톤을 제조하는 방법 | |
KR100527321B1 (ko) | 헥사메틸렌 디아민을 함유하는 혼합물에서 이를 회수하는 방법 | |
CA2220463A1 (en) | Process for improving color and color stability of oleic acid | |
WO1999048872A2 (de) | Verfahren zur abtrennung eines azepin-derivats aus einer mischung enthaltend ein amin und ein azepin-derivat | |
US6887352B2 (en) | Distillative method for separating hexamethylenediamine from a mixture comprising hexamethylenediamine, 6-aminocapronitrile and tetrahydroazepine | |
CA2321848A1 (en) | Production of polyamides by reactive distillation | |
US3850760A (en) | Separation of isopropyl-amines by plural stage distillation | |
MY127355A (en) | Process for the production of nylon 6 | |
CA1172201A (en) | Enhanced distillation of cyclohexanol from phenol with additional cyclohexanone feed | |
EP1328503B1 (en) | Recovery of hexamethylenediame (hmd) with low polarographically reducible impurities (pri) from mixtures of hmd, aminocapronitrile and pri | |
US7468119B2 (en) | Separation of 6-aminocapronitrile and hexamethylenediamine from a mixture comprising hexamethylenediamine, 6-aminocapronitrile and tetrahydroazepine | |
US7208632B2 (en) | Separation of 6-aminocapronitrile and hexamethylenediamine from a mixture comprising hexamethylenediamine, 6-aminocapronitrile and tetrahydroazepine | |
TW375603B (en) | Separation of 2-aminomethyl cyclopentylamine from a mixture comprising hexamethylenediamine and 2-aminomethyl cyclopentylamine | |
MY133976A (en) | Method for removing 6-aminocapronitrile from mixtures that contain 6-aminocapronitrile, adipodinitrile and hexamethylenediamine | |
TH31625A (th) | การเตรียมคาโพรแลคแทม และเฮกซาเมทิลีนไดเอมีนขึ้นพร้อทม ๆ กัน | |
TH28260A (th) | กระบวนการผลิตไนโตรเจนโดยใช้หอคู่ที่มีส่วนช่วยการแยกที่ความดันต่ำ | |
MXPA99006690A (en) | Method for separating 6-aminocapronitrile from mixtures containing 6-aminocapronitrile and an imine | |
TH20474A (th) | วิธีการผลิตบิวทิรัลดิไฮด์ | |
TH16355B (th) | วิธีการผลิตบิวทิรัลดิไฮด์ | |
TH33142A (th) | การแยก 2-อะมิโนเมธิลไซโคลแอมีน ออกจากสารผสมที่ประกอบด้วยเฮกซะเมธีลีนไดแอมีน และ 2-อะมิโนเมธิลไซโคลเพนทิล แอมีน |