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SI1852424T1 - Postopek za pripravo izoksazolin il acil benzolov - Google Patents

Postopek za pripravo izoksazolin il acil benzolov

Info

Publication number
SI1852424T1
SI1852424T1 SI9931067T SI9931067T SI1852424T1 SI 1852424 T1 SI1852424 T1 SI 1852424T1 SI 9931067 T SI9931067 T SI 9931067T SI 9931067 T SI9931067 T SI 9931067T SI 1852424 T1 SI1852424 T1 SI 1852424T1
Authority
SI
Slovenia
Prior art keywords
formula
isoxazole
alkylthio
alkyl
preparation
Prior art date
Application number
SI9931067T
Other languages
English (en)
Inventor
Joachim Rheinheimer
Deyn Wolfgang Von
Joachim Gebhardt
Michael Rack
Rene Lochtman
Norbert Gotz
Michael Keil
Matthias Witschel
Helmut Hagen
Ulf Misslitz
Ernst Baumann
Original Assignee
Basf Se
Priority date (The priority date is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the date listed.)
Filing date
Publication date
Priority claimed from DE19820722A external-priority patent/DE19820722C1/de
Priority claimed from DE19852095A external-priority patent/DE19852095A1/de
Application filed by Basf Se filed Critical Basf Se
Publication of SI1852424T1 publication Critical patent/SI1852424T1/sl

Links

Classifications

    • C—CHEMISTRY; METALLURGY
    • C07—ORGANIC CHEMISTRY
    • C07C—ACYCLIC OR CARBOCYCLIC COMPOUNDS
    • C07C249/00—Preparation of compounds containing nitrogen atoms doubly-bound to a carbon skeleton
    • C07C249/04—Preparation of compounds containing nitrogen atoms doubly-bound to a carbon skeleton of oximes
    • C07C249/06—Preparation of compounds containing nitrogen atoms doubly-bound to a carbon skeleton of oximes by nitrosation of hydrocarbons or substituted hydrocarbons
    • C—CHEMISTRY; METALLURGY
    • C07—ORGANIC CHEMISTRY
    • C07C—ACYCLIC OR CARBOCYCLIC COMPOUNDS
    • C07C201/00—Preparation of esters of nitric or nitrous acid or of compounds containing nitro or nitroso groups bound to a carbon skeleton
    • C07C201/06—Preparation of nitro compounds
    • C07C201/10—Preparation of nitro compounds by substitution of functional groups by nitro groups
    • C—CHEMISTRY; METALLURGY
    • C07—ORGANIC CHEMISTRY
    • C07C—ACYCLIC OR CARBOCYCLIC COMPOUNDS
    • C07C201/00—Preparation of esters of nitric or nitrous acid or of compounds containing nitro or nitroso groups bound to a carbon skeleton
    • C07C201/06—Preparation of nitro compounds
    • C07C201/12—Preparation of nitro compounds by reactions not involving the formation of nitro groups
    • C—CHEMISTRY; METALLURGY
    • C07—ORGANIC CHEMISTRY
    • C07C—ACYCLIC OR CARBOCYCLIC COMPOUNDS
    • C07C205/00—Compounds containing nitro groups bound to a carbon skeleton
    • C07C205/44—Compounds containing nitro groups bound to a carbon skeleton the carbon skeleton being further substituted by —CHO groups
    • C—CHEMISTRY; METALLURGY
    • C07—ORGANIC CHEMISTRY
    • C07C—ACYCLIC OR CARBOCYCLIC COMPOUNDS
    • C07C209/00—Preparation of compounds containing amino groups bound to a carbon skeleton
    • C07C209/62—Preparation of compounds containing amino groups bound to a carbon skeleton by cleaving carbon-to-nitrogen, sulfur-to-nitrogen, or phosphorus-to-nitrogen bonds, e.g. hydrolysis of amides, N-dealkylation of amines or quaternary ammonium compounds
    • C—CHEMISTRY; METALLURGY
    • C07—ORGANIC CHEMISTRY
    • C07C—ACYCLIC OR CARBOCYCLIC COMPOUNDS
    • C07C251/00—Compounds containing nitrogen atoms doubly-bound to a carbon skeleton
    • C07C251/32—Oximes
    • C07C251/34—Oximes with oxygen atoms of oxyimino groups bound to hydrogen atoms or to carbon atoms of unsubstituted hydrocarbon radicals
    • C07C251/48—Oximes with oxygen atoms of oxyimino groups bound to hydrogen atoms or to carbon atoms of unsubstituted hydrocarbon radicals with the carbon atom of at least one of the oxyimino groups bound to a carbon atom of a six-membered aromatic ring
    • C—CHEMISTRY; METALLURGY
    • C07—ORGANIC CHEMISTRY
    • C07C—ACYCLIC OR CARBOCYCLIC COMPOUNDS
    • C07C253/00—Preparation of carboxylic acid nitriles
    • C—CHEMISTRY; METALLURGY
    • C07—ORGANIC CHEMISTRY
    • C07C—ACYCLIC OR CARBOCYCLIC COMPOUNDS
    • C07C255/00—Carboxylic acid nitriles
    • C07C255/49—Carboxylic acid nitriles having cyano groups bound to carbon atoms of six-membered aromatic rings of a carbon skeleton
    • C07C255/50—Carboxylic acid nitriles having cyano groups bound to carbon atoms of six-membered aromatic rings of a carbon skeleton to carbon atoms of non-condensed six-membered aromatic rings
    • C—CHEMISTRY; METALLURGY
    • C07—ORGANIC CHEMISTRY
    • C07C—ACYCLIC OR CARBOCYCLIC COMPOUNDS
    • C07C315/00—Preparation of sulfones; Preparation of sulfoxides
    • C07C315/04—Preparation of sulfones; Preparation of sulfoxides by reactions not involving the formation of sulfone or sulfoxide groups
    • C—CHEMISTRY; METALLURGY
    • C07—ORGANIC CHEMISTRY
    • C07C—ACYCLIC OR CARBOCYCLIC COMPOUNDS
    • C07C319/00—Preparation of thiols, sulfides, hydropolysulfides or polysulfides
    • C07C319/14—Preparation of thiols, sulfides, hydropolysulfides or polysulfides of sulfides
    • C—CHEMISTRY; METALLURGY
    • C07—ORGANIC CHEMISTRY
    • C07D—HETEROCYCLIC COMPOUNDS
    • C07D261/00—Heterocyclic compounds containing 1,2-oxazole or hydrogenated 1,2-oxazole rings
    • C07D261/02—Heterocyclic compounds containing 1,2-oxazole or hydrogenated 1,2-oxazole rings not condensed with other rings
    • C07D261/04—Heterocyclic compounds containing 1,2-oxazole or hydrogenated 1,2-oxazole rings not condensed with other rings having one double bond between ring members or between a ring member and a non-ring member
    • C—CHEMISTRY; METALLURGY
    • C07—ORGANIC CHEMISTRY
    • C07D—HETEROCYCLIC COMPOUNDS
    • C07D413/00—Heterocyclic compounds containing two or more hetero rings, at least one ring having nitrogen and oxygen atoms as the only ring hetero atoms
    • C07D413/02—Heterocyclic compounds containing two or more hetero rings, at least one ring having nitrogen and oxygen atoms as the only ring hetero atoms containing two hetero rings
    • C07D413/10—Heterocyclic compounds containing two or more hetero rings, at least one ring having nitrogen and oxygen atoms as the only ring hetero atoms containing two hetero rings linked by a carbon chain containing aromatic rings

Landscapes

  • Chemical & Material Sciences (AREA)
  • Organic Chemistry (AREA)
  • Chemical Kinetics & Catalysis (AREA)
  • Heterocyclic Carbon Compounds Containing A Hetero Ring Having Nitrogen And Oxygen As The Only Ring Hetero Atoms (AREA)
  • Organic Low-Molecular-Weight Compounds And Preparation Thereof (AREA)
  • Pharmaceuticals Containing Other Organic And Inorganic Compounds (AREA)
  • Low-Molecular Organic Synthesis Reactions Using Catalysts (AREA)
  • Plural Heterocyclic Compounds (AREA)
  • Agricultural Chemicals And Associated Chemicals (AREA)
SI9931067T 1998-05-11 1999-05-04 Postopek za pripravo izoksazolin il acil benzolov SI1852424T1 (sl)

Applications Claiming Priority (3)

Application Number Priority Date Filing Date Title
DE19820722A DE19820722C1 (de) 1998-05-11 1998-05-11 Verfahren zur Herstellung von Benzoylpyrazolen
DE19852095A DE19852095A1 (de) 1998-11-12 1998-11-12 Verfahren zur Herstellung von 2-Alkyl-3-(4,5-dihydroisoxazol-3-yl)-acylbenzolen
EP07104691A EP1852424B1 (de) 1998-05-11 1999-05-04 Verfahren zur Herstellung von Isoxazolin-3-YL-Acylbenzolen

Publications (1)

Publication Number Publication Date
SI1852424T1 true SI1852424T1 (sl) 2012-05-31

Family

ID=26046070

Family Applications (2)

Application Number Title Priority Date Filing Date
SI9931067T SI1852424T1 (sl) 1998-05-11 1999-05-04 Postopek za pripravo izoksazolin il acil benzolov
SI9930975T SI1077955T1 (sl) 1998-05-11 1999-05-04 Postopek za proizvodnjo izoksazolin-3il-acil benzena

Family Applications After (1)

Application Number Title Priority Date Filing Date
SI9930975T SI1077955T1 (sl) 1998-05-11 1999-05-04 Postopek za proizvodnjo izoksazolin-3il-acil benzena

Country Status (24)

Country Link
US (6) US6525204B1 (sl)
EP (4) EP1852424B1 (sl)
JP (2) JP4786032B2 (sl)
KR (1) KR100604302B1 (sl)
CN (3) CN101113137B (sl)
AT (2) ATE365724T1 (sl)
AU (1) AU772781B2 (sl)
BR (1) BR9910326B1 (sl)
CA (3) CA2652071C (sl)
CZ (2) CZ304938B6 (sl)
DE (1) DE59914392D1 (sl)
DK (2) DK1852424T3 (sl)
EA (3) EA010633B1 (sl)
ES (2) ES2381758T3 (sl)
HU (1) HUP0102843A3 (sl)
IL (1) IL139277A0 (sl)
NO (1) NO318079B1 (sl)
NZ (1) NZ508648A (sl)
PL (2) PL219088B1 (sl)
PT (2) PT1852424E (sl)
SI (2) SI1852424T1 (sl)
SK (4) SK287758B6 (sl)
TR (1) TR200003332T2 (sl)
WO (1) WO1999058509A1 (sl)

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EE05455B1 (et) * 1997-01-17 2011-08-15 Basf Aktiengesellschaft 3-heterotskll-asendatud bensolderivaadid ja neid sisaldavad vahendid, nende saamise meetodid ning nende kasutamine herbitsiididena
DE19852095A1 (de) 1998-11-12 2000-05-18 Basf Ag Verfahren zur Herstellung von 2-Alkyl-3-(4,5-dihydroisoxazol-3-yl)-acylbenzolen
SI1852424T1 (sl) * 1998-05-11 2012-05-31 Basf Se Postopek za pripravo izoksazolin il acil benzolov
WO2000029395A1 (de) 1998-11-18 2000-05-25 Basf Aktiengesellschaft Verfahren zur herstellung von 2-alkyl- 3-(4,5- dihydroisoxazol- 3-yl)-halogenbenzolen
US6388135B1 (en) 2000-06-30 2002-05-14 Basf Aktiengesellschaft Preparation of 4-bromoaniline derivatives
NZ523825A (en) * 2000-06-30 2004-06-25 Basf Ag Method for producing 4-bromine-aniline derivatives
NZ524049A (en) * 2000-07-17 2004-09-24 Basf Ag Process for the preparation of 4-thioalkylbromobenzene derivatives
DE10127328A1 (de) 2001-06-06 2002-12-19 Bayer Cropscience Gmbh Herbizide Mittel enthaltend Benzoylpyrazole und Safener
DE10157545A1 (de) 2001-11-23 2003-06-12 Bayer Cropscience Gmbh Herbizide Mittel enthaltend Benzoylpyrazole und Safener
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PT2173742E (pt) 2007-07-06 2012-01-13 Basf Se Forma cristalina da [3-(4,5-dihidro-3-isoxazolil)-2-metil- 4-(metilsulfonil)-fenil]-(5-hidroxi-1-metil-1h- -pirazol-4-il)-metanona
US20090215625A1 (en) * 2008-01-07 2009-08-27 Auburn University Combinations of Herbicides and Safeners
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DE102011080007A1 (de) 2011-07-28 2012-09-13 Bayer Cropscience Ag Verwendung von Saatgutbehandlungs-Wirkstoffen aus den Gruppen der Conazole- und Triazol-Fungizide als Safener
DE102011080020A1 (de) 2011-07-28 2012-09-13 Bayer Cropscience Ag Verwendung von Saatgutbehandlungs-Wirkstoffen aus der Gruppe der Dicarboximid-Fungizide als Safener
DE102011080010A1 (de) 2011-07-28 2012-10-25 Bayer Cropscience Ag Verwendung von Saatgutbehandlungs-Wirkstoffen aus den Gruppen der Anilid- und Thiazol-Fungizide als Safener
DE102011079997A1 (de) 2011-07-28 2012-09-13 Bayer Corpscience Ag Verwendung von Saatgutbehandlungs-Wirkstoffen aus der Gruppe der Pyrazol-Insektizide als Safener
CN102584735A (zh) * 2011-12-13 2012-07-18 大连理工大学 一种异噁唑类化合物的制备方法
AU2013333916B2 (en) 2012-10-19 2017-05-25 Bayer Cropscience Ag Active compound combinations comprising carboxamide derivatives
CN103467300B (zh) * 2013-08-19 2016-02-24 浙江工业大学 一种邻硝基苯甲醛类化合物的合成方法
CN105481787B (zh) * 2015-11-30 2018-04-20 湖南海利化工股份有限公司 3‑(2‑甲基‑6‑硝基苯基)‑4,5‑二氢异噁唑的制备方法
CN106928159A (zh) * 2017-03-01 2017-07-07 安徽丰乐农化有限责任公司 3‑(3‑溴‑2‑甲基‑6‑甲基磺酰基苯基)‑4,5‑二氢化异恶唑的提纯方法
CN107011278B (zh) * 2017-04-06 2019-03-22 湘潭大学 3,4,5-,三取代-4,5-二氢异噁唑、衍生物及其合成方法及用途
CN107162944B (zh) * 2017-04-27 2019-02-26 湖南化工研究院有限公司 2,3-二甲基苯甲硫醚的制备方法
CN107325091B (zh) * 2017-07-13 2019-09-20 湖南海利化工股份有限公司 一种苯吡唑草酮的制备方法
CN107652246B (zh) * 2017-09-25 2020-08-25 江苏乾元生物科技有限公司 一种3-[3-溴-2-甲基-6-(甲基磺酰基)苯基]-4,5-二氢化异噁唑的制备方法
CN108863969B (zh) * 2018-06-30 2022-05-24 华南理工大学 一种4-烯丙基-3,5-二取代异噁唑的合成方法
AU2019330847A1 (en) 2018-08-27 2021-03-18 Basf Se Aqueous compositions of topramezone
CN108947923A (zh) * 2018-08-28 2018-12-07 常州大学 一种3-(2-甲基-6-甲硫基)苯基-4,5-二氢异恶唑的制备方法
WO2020069876A1 (en) 2018-10-03 2020-04-09 Basf Se Microemulsion compositions of topramezone
CN109438380B (zh) * 2018-11-19 2022-04-22 华南理工大学 一种合成4-(n,n-二烷基-2-丙炔-1-氨基)异恶唑的方法
WO2020152200A1 (en) 2019-01-25 2020-07-30 Basf Se Process for preparation of heteroarylketones
CN110183392B (zh) * 2019-06-14 2023-03-28 河北医科大学 一种3-取代苯基-4，5-二氢异噁唑衍生物的制备方法及其用途和中间体
CN112552178B (zh) * 2019-09-25 2023-07-18 江西天宇化工有限公司 一种苯甲硫醚类化合物合成中的副产物的回收利用方法
CN112694427B (zh) * 2019-10-23 2022-11-18 江西天宇化工有限公司 一种制备2,3-二甲基苯甲硫醚的方法
CN114644622B (zh) * 2020-12-17 2022-10-18 山东省联合农药工业有限公司 一种含异噁唑啉的吡啶联苯类化合物及其制备方法与用途
CN114797738B (zh) * 2022-04-30 2024-04-02 兰升生物科技集团股份有限公司 改进的管式反应器、使用该管式反应器的生产设备及使用它们制备磺酰基化合物的方法
CN115128202A (zh) * 2022-07-28 2022-09-30 京博农化科技有限公司 一种苯唑草酮中间体的含量测定方法
CN115784925B (zh) * 2022-10-31 2024-07-02 江苏七洲绿色科技研究院有限公司 一种2-甲基-6-硝基苯甲醛肟连续化制备方法
CN116178295A (zh) * 2023-01-28 2023-05-30 山东亿盛实业股份有限公司 一种苯唑草酮代谢物t283的制备方法
CN118788251B (zh) * 2024-09-13 2025-02-07 苏州开元民生科技股份有限公司 一种制备3-[3-溴-2-甲基-6-（甲基磺酰基）苯基]-4,5-二氢化异噁唑的方法

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Also Published As

Publication number Publication date
BR9910326A (pt) 2001-01-30
EA200001135A1 (ru) 2001-06-25
NO318079B1 (no) 2005-01-31
SK16872000A3 (sk) 2001-06-11
ES2288021T3 (es) 2007-12-16
US8124810B2 (en) 2012-02-28
US20030018200A1 (en) 2003-01-23
JP4786032B2 (ja) 2011-10-05
HUP0102843A3 (en) 2004-03-01
EP1077955B1 (de) 2007-06-27
KR20010043497A (ko) 2001-05-25
CZ20004167A3 (cs) 2001-07-11
EP1077955A1 (de) 2001-02-28
DK1077955T3 (da) 2007-10-08
EP2325176A1 (de) 2011-05-25
US8049017B2 (en) 2011-11-01
EA007095B1 (ru) 2006-06-30
PL344332A1 (en) 2001-11-05
SK287476B6 (sk) 2010-11-08
DE59914392D1 (de) 2007-08-09
JP2010215642A (ja) 2010-09-30
CA2331816A1 (en) 1999-11-18
EP2298749B1 (de) 2014-12-24
US6608209B2 (en) 2003-08-19
EA010633B1 (ru) 2008-10-30
PT1077955E (pt) 2007-08-01
ATE365724T1 (de) 2007-07-15
EA009301B1 (ru) 2007-12-28
CN1139578C (zh) 2004-02-25
IL139277A0 (en) 2001-11-25
CZ304938B6 (cs) 2015-01-28
AU3930599A (en) 1999-11-29
SK287758B6 (sk) 2011-09-05
NZ508648A (en) 2003-09-26
CN1300284A (zh) 2001-06-20
CN1495158A (zh) 2004-05-12
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US20030216580A1 (en) 2003-11-20
TR200003332T2 (tr) 2001-02-21
EP1852424B1 (de) 2012-04-04
EP2298749A1 (de) 2011-03-23
EA200500510A1 (ru) 2005-08-25
US7309802B2 (en) 2007-12-18
PL209931B1 (pl) 2011-11-30
EA200500509A1 (ru) 2005-08-25
HUP0102843A2 (hu) 2002-03-28
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KR100604302B1 (ko) 2006-07-28
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SI1077955T1 (sl) 2007-10-31
US20100105920A1 (en) 2010-04-29
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US20070161800A1 (en) 2007-07-12
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AU772781B2 (en) 2004-05-06
EP1852424A3 (de) 2008-03-05
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PL219088B1 (pl) 2015-03-31
DK1852424T3 (da) 2012-07-23
EP1852424A2 (de) 2007-11-07
CA2652071C (en) 2012-01-17
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SK287967B6 (sk) 2012-07-03
US7663001B2 (en) 2010-02-16
CN1255377C (zh) 2006-05-10
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