[go: up one dir, main page]

SE511531C2 - Förfarande för framställning av aminoetyletanolamin och/eller hydroxietylpiperazin - Google Patents

Förfarande för framställning av aminoetyletanolamin och/eller hydroxietylpiperazin

Info

Publication number
SE511531C2
SE511531C2 SE9500444A SE9500444A SE511531C2 SE 511531 C2 SE511531 C2 SE 511531C2 SE 9500444 A SE9500444 A SE 9500444A SE 9500444 A SE9500444 A SE 9500444A SE 511531 C2 SE511531 C2 SE 511531C2
Authority
SE
Sweden
Prior art keywords
weight
ethylenediamine
product stream
ethoxylation
piperazine
Prior art date
Application number
SE9500444A
Other languages
English (en)
Swedish (sv)
Other versions
SE9500444D0 (sv
SE9500444L (sv
Inventor
Juhan Koell
Magnus Franck
Original Assignee
Akzo Nobel Nv
Priority date (The priority date is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the date listed.)
Filing date
Publication date
Application filed by Akzo Nobel Nv filed Critical Akzo Nobel Nv
Priority to SE9500444A priority Critical patent/SE511531C2/sv
Publication of SE9500444D0 publication Critical patent/SE9500444D0/xx
Priority to HU9702428A priority patent/HU218150B/hu
Priority to JP52392496A priority patent/JP3974939B2/ja
Priority to AU45376/96A priority patent/AU699182B2/en
Priority to US08/875,871 priority patent/US6013801A/en
Priority to BR9607023A priority patent/BR9607023A/pt
Priority to KR1019970705383A priority patent/KR100379669B1/ko
Priority to RU97114881/04A priority patent/RU2159226C2/ru
Priority to GEAP19963839A priority patent/GEP19991727B/en
Priority to CZ19972312A priority patent/CZ291435B6/cs
Priority to PCT/EP1996/000207 priority patent/WO1996024576A1/en
Priority to DK96901303T priority patent/DK0821664T3/da
Priority to KR1019970705383A priority patent/KR19980701986A/ko
Priority to AT96901303T priority patent/ATE191453T1/de
Priority to CNB961918551A priority patent/CN1133618C/zh
Priority to PT96901303T priority patent/PT821664E/pt
Priority to EP96901303A priority patent/EP0821664B1/en
Priority to CA002208439A priority patent/CA2208439C/en
Priority to DE69607604T priority patent/DE69607604T2/de
Priority to ES96901303T priority patent/ES2146866T3/es
Priority to PL96321187A priority patent/PL183057B1/pl
Priority to EE9700170A priority patent/EE03391B1/xx
Priority to MX9705702A priority patent/MX197570B/es
Priority to TW085100328A priority patent/TW389756B/zh
Priority to ZA96351A priority patent/ZA96351B/xx
Priority to MYPI96000426A priority patent/MY112955A/en
Priority to ARP960101305A priority patent/AR000886A1/es
Publication of SE9500444L publication Critical patent/SE9500444L/xx
Priority to UA97063429A priority patent/UA51638C2/uk
Priority to BG101668A priority patent/BG61943B1/bg
Priority to NO973509A priority patent/NO306776B1/no
Priority to FI973254A priority patent/FI973254A0/fi
Publication of SE511531C2 publication Critical patent/SE511531C2/sv
Priority to GR20000401096T priority patent/GR3033408T3/el

Links

Classifications

    • C—CHEMISTRY; METALLURGY
    • C07—ORGANIC CHEMISTRY
    • C07C—ACYCLIC OR CARBOCYCLIC COMPOUNDS
    • C07C213/00—Preparation of compounds containing amino and hydroxy, amino and etherified hydroxy or amino and esterified hydroxy groups bound to the same carbon skeleton
    • C07C213/04—Preparation of compounds containing amino and hydroxy, amino and etherified hydroxy or amino and esterified hydroxy groups bound to the same carbon skeleton by reaction of ammonia or amines with olefin oxides or halohydrins
    • C—CHEMISTRY; METALLURGY
    • C07—ORGANIC CHEMISTRY
    • C07C—ACYCLIC OR CARBOCYCLIC COMPOUNDS
    • C07C215/00—Compounds containing amino and hydroxy groups bound to the same carbon skeleton
    • C07C215/02—Compounds containing amino and hydroxy groups bound to the same carbon skeleton having hydroxy groups and amino groups bound to acyclic carbon atoms of the same carbon skeleton
    • C07C215/04—Compounds containing amino and hydroxy groups bound to the same carbon skeleton having hydroxy groups and amino groups bound to acyclic carbon atoms of the same carbon skeleton the carbon skeleton being saturated
    • C07C215/06—Compounds containing amino and hydroxy groups bound to the same carbon skeleton having hydroxy groups and amino groups bound to acyclic carbon atoms of the same carbon skeleton the carbon skeleton being saturated and acyclic
    • C07C215/14—Compounds containing amino and hydroxy groups bound to the same carbon skeleton having hydroxy groups and amino groups bound to acyclic carbon atoms of the same carbon skeleton the carbon skeleton being saturated and acyclic the nitrogen atom of the amino group being further bound to hydrocarbon groups substituted by amino groups
    • C—CHEMISTRY; METALLURGY
    • C07—ORGANIC CHEMISTRY
    • C07D—HETEROCYCLIC COMPOUNDS
    • C07D295/00—Heterocyclic compounds containing polymethylene-imine rings with at least five ring members, 3-azabicyclo [3.2.2] nonane, piperazine, morpholine or thiomorpholine rings, having only hydrogen atoms directly attached to the ring carbon atoms
    • C07D295/04—Heterocyclic compounds containing polymethylene-imine rings with at least five ring members, 3-azabicyclo [3.2.2] nonane, piperazine, morpholine or thiomorpholine rings, having only hydrogen atoms directly attached to the ring carbon atoms with substituted hydrocarbon radicals attached to ring nitrogen atoms
    • C07D295/08—Heterocyclic compounds containing polymethylene-imine rings with at least five ring members, 3-azabicyclo [3.2.2] nonane, piperazine, morpholine or thiomorpholine rings, having only hydrogen atoms directly attached to the ring carbon atoms with substituted hydrocarbon radicals attached to ring nitrogen atoms substituted by singly bound oxygen or sulfur atoms
    • C07D295/084—Heterocyclic compounds containing polymethylene-imine rings with at least five ring members, 3-azabicyclo [3.2.2] nonane, piperazine, morpholine or thiomorpholine rings, having only hydrogen atoms directly attached to the ring carbon atoms with substituted hydrocarbon radicals attached to ring nitrogen atoms substituted by singly bound oxygen or sulfur atoms with the ring nitrogen atoms and the oxygen or sulfur atoms attached to the same carbon chain, which is not interrupted by carbocyclic rings
    • C07D295/088—Heterocyclic compounds containing polymethylene-imine rings with at least five ring members, 3-azabicyclo [3.2.2] nonane, piperazine, morpholine or thiomorpholine rings, having only hydrogen atoms directly attached to the ring carbon atoms with substituted hydrocarbon radicals attached to ring nitrogen atoms substituted by singly bound oxygen or sulfur atoms with the ring nitrogen atoms and the oxygen or sulfur atoms attached to the same carbon chain, which is not interrupted by carbocyclic rings to an acyclic saturated chain

Landscapes

  • Chemical & Material Sciences (AREA)
  • Organic Chemistry (AREA)
  • Chemical Kinetics & Catalysis (AREA)
  • Organic Low-Molecular-Weight Compounds And Preparation Thereof (AREA)
  • Low-Molecular Organic Synthesis Reactions Using Catalysts (AREA)
SE9500444A 1995-02-08 1995-02-08 Förfarande för framställning av aminoetyletanolamin och/eller hydroxietylpiperazin SE511531C2 (sv)

Priority Applications (32)

Application Number Priority Date Filing Date Title
SE9500444A SE511531C2 (sv) 1995-02-08 1995-02-08 Förfarande för framställning av aminoetyletanolamin och/eller hydroxietylpiperazin
MX9705702A MX197570B (es) 1995-02-08 1996-01-11 Metodo para producir aminoetiletanolamina y/o hidroxietilpiperazina.
EP96901303A EP0821664B1 (en) 1995-02-08 1996-01-11 Method for producing aminoethylethanolamine and/or hydroxyethyl piperazine
CA002208439A CA2208439C (en) 1995-02-08 1996-01-11 Method for producing aminoethylethanolamine and/or hydroxyethyl piperazine
AU45376/96A AU699182B2 (en) 1995-02-08 1996-01-11 Method for producing aminoethylethanolamine and/or hydroxyethyl piperazine
US08/875,871 US6013801A (en) 1995-02-08 1996-01-11 Method for producing aminoethylethanolamine and/or hydroxyethyl piperazine
BR9607023A BR9607023A (pt) 1995-02-08 1996-01-11 Método para produção de aminoetilenolamina e/ou hidroxietil piperazina
KR1019970705383A KR100379669B1 (ko) 1995-02-08 1996-01-11 아미노에틸에탄올아민및/또는히드록시에틸피페라진을제조하는방법
RU97114881/04A RU2159226C2 (ru) 1995-02-08 1996-01-11 Способ получения аминоэтилэтаноламина и/или гидроксиэтилпиперазина
GEAP19963839A GEP19991727B (en) 1995-02-08 1996-01-11 Method for producing aminoethylethanolamine and/or hydroxyethyl piperazine
CZ19972312A CZ291435B6 (cs) 1995-02-08 1996-01-11 Způsob výroby aminoethylethanolaminu a/nebo hydroxyethylpiperazinu
PCT/EP1996/000207 WO1996024576A1 (en) 1995-02-08 1996-01-11 Method for producing aminoethylethanolamine and/or hydroxyethyl piperazine
DK96901303T DK0821664T3 (da) 1995-02-08 1996-01-11 Fremgangsmåde til fremstilling af aminoethylethanolamin og/eller hydroxyethylenpiperazin
KR1019970705383A KR19980701986A (ko) 1995-02-08 1996-01-11 아미노에틸에탄올아민 및/또는 히드록시에틸 피페라진을 제조하는 방법
AT96901303T ATE191453T1 (de) 1995-02-08 1996-01-11 Verfahren zur herstellung von aminoethylethanolamin und/oder hydroxyethylpiperazin
CNB961918551A CN1133618C (zh) 1995-02-08 1996-01-11 生产氨基乙基醇胺和/或羟乙基哌嗪的方法
PT96901303T PT821664E (pt) 1995-02-08 1996-01-11 Processo de producao de aminoetiletanolamina e/ou hidroxietil-piperazina
HU9702428A HU218150B (hu) 1995-02-08 1996-01-11 Eljárás amino-etil-etanol-amin és/vagy hidroxi-etil-piperazin előállítására
ES96901303T ES2146866T3 (es) 1995-02-08 1996-01-11 Metodo para producir aminoetiletanolamina y/o hidroxietilpiperazina.
JP52392496A JP3974939B2 (ja) 1995-02-08 1996-01-11 アミノエチルエタノールアミンおよび／またはヒドロキシエチルピペラジンを製造するための方法
DE69607604T DE69607604T2 (de) 1995-02-08 1996-01-11 Verfahren zur herstellung von aminoethylethanolamin und/oder hydroxyethylpiperazin
PL96321187A PL183057B1 (pl) 1995-02-08 1996-01-11 Sposób wytwarzania aminoetyloetanoloaminy i/lub hydroksyetylopiperazyny
EE9700170A EE03391B1 (et) 1995-02-08 1996-01-11 Aminoetüületanoolamiini ja/või hüdroksüetüülpiperasiini saamise meetod
TW085100328A TW389756B (en) 1995-02-08 1996-01-12 Method for producing aminoethylethanolamine and/or hydroxyethyl piperazine
ZA96351A ZA96351B (en) 1995-02-08 1996-01-17 Method for producing aminoethylethanolamine and/or hydroxyethyl piperazine
MYPI96000426A MY112955A (en) 1995-02-08 1996-02-06 Method for producing aminoethylethanolamine and/or hydroxyethyl piperazine
ARP960101305A AR000886A1 (es) 1995-02-08 1996-02-07 Metodo para producir aminoetiletanolamina y/o n-hidroxietil piperazina
UA97063429A UA51638C2 (uk) 1995-02-08 1996-11-01 Спосіб одержання аміноетилетаноламіну та/або гідроксіетилпіперазину
BG101668A BG61943B1 (bg) 1995-02-08 1997-06-25 Метод за производство на аминоетилетаноламин и/или нахидроксиетилпиперазин
NO973509A NO306776B1 (no) 1995-02-08 1997-07-30 Fremgangsmåte ved fremstilling av aminoetyletanolamin og/eller hydroksyetylpiperazin
FI973254A FI973254A0 (fi) 1995-02-08 1997-08-07 Menetelmä aminoetyylietanoliamiinin ja/tai hydroksietyylipiperatsiinin valmistamiseksi
GR20000401096T GR3033408T3 (en) 1995-02-08 2000-05-12 Method for producing aminoethylethanolamine and/or hydroxyethyl piperazine

Applications Claiming Priority (1)

Application Number Priority Date Filing Date Title
SE9500444A SE511531C2 (sv) 1995-02-08 1995-02-08 Förfarande för framställning av aminoetyletanolamin och/eller hydroxietylpiperazin

Publications (3)

Publication Number Publication Date
SE9500444D0 SE9500444D0 (sv) 1995-02-08
SE9500444L SE9500444L (sv) 1996-08-09
SE511531C2 true SE511531C2 (sv) 1999-10-11

Family

ID=20397122

Family Applications (1)

Application Number Title Priority Date Filing Date
SE9500444A SE511531C2 (sv) 1995-02-08 1995-02-08 Förfarande för framställning av aminoetyletanolamin och/eller hydroxietylpiperazin

Country Status (31)

Country Link
US (1) US6013801A (bg)
EP (1) EP0821664B1 (bg)
JP (1) JP3974939B2 (bg)
KR (2) KR19980701986A (bg)
CN (1) CN1133618C (bg)
AR (1) AR000886A1 (bg)
AT (1) ATE191453T1 (bg)
AU (1) AU699182B2 (bg)
BG (1) BG61943B1 (bg)
BR (1) BR9607023A (bg)
CA (1) CA2208439C (bg)
CZ (1) CZ291435B6 (bg)
DE (1) DE69607604T2 (bg)
DK (1) DK0821664T3 (bg)
EE (1) EE03391B1 (bg)
ES (1) ES2146866T3 (bg)
FI (1) FI973254A0 (bg)
GE (1) GEP19991727B (bg)
GR (1) GR3033408T3 (bg)
HU (1) HU218150B (bg)
MX (1) MX197570B (bg)
MY (1) MY112955A (bg)
NO (1) NO306776B1 (bg)
PL (1) PL183057B1 (bg)
PT (1) PT821664E (bg)
RU (1) RU2159226C2 (bg)
SE (1) SE511531C2 (bg)
TW (1) TW389756B (bg)
UA (1) UA51638C2 (bg)
WO (1) WO1996024576A1 (bg)
ZA (1) ZA96351B (bg)

Families Citing this family (17)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
EP1323706A1 (en) * 2001-12-28 2003-07-02 Nippon Shokubai Co., Ltd. Process for producing N-hydroxyalkyl compound, and tris(2-hydroxyethyl) isocyanurate composition
DE10335991A1 (de) * 2003-08-01 2005-02-24 Basf Ag Verfahren zur Herstellung von Ethylenaminen
BR112012021940A2 (pt) * 2010-03-18 2016-05-31 Basf Se processo para preparar aminocarboxilatos
WO2012055893A1 (de) * 2010-10-29 2012-05-03 Basf Se Verfahren zur herstellung von 1,4-bishydroxyethyl-piperazin
CN102786425B (zh) * 2011-05-19 2014-06-04 中国科学院大连化学物理研究所 生产β-羟乙基乙二胺的方法
CN102617363A (zh) * 2012-03-13 2012-08-01 河北科技大学 一种乙二胺和环氧乙烷合成羟乙基乙二胺的新工艺
JP6070088B2 (ja) * 2012-05-31 2017-02-01 東ソー株式会社 Ｎ−アルキルピペラジン類の精製方法
CN103936601B (zh) * 2013-01-23 2016-08-03 中国石油化工股份有限公司 乙醇胺生产中的氨回收方法
CN103908872B (zh) * 2014-04-04 2015-12-30 江苏蓝电环保股份有限公司 一种从工业废气中回收二氧化硫的吸收剂及回收方法
CN103908873B (zh) * 2014-04-04 2016-03-09 江苏蓝电环保股份有限公司 一种从工业废气中回收二氧化硫的方法
CN104130208B (zh) * 2014-08-04 2016-01-13 西安近代化学研究所 一种n-甲基哌嗪与n-乙基哌嗪的分离方法
ES2894854T3 (es) * 2015-07-15 2022-02-16 Dow Global Technologies Llc Proceso para la preparación de compuestos de hidroxietil piperazina
CN107089916B (zh) * 2016-06-02 2019-06-21 补天新材料技术有限公司 甲酸有机胺盐类化合物及其作为发泡剂的用途
CN106543104B (zh) * 2016-11-04 2019-02-01 山东铂源药业有限公司 一种1-(2-羟基乙基)哌嗪的合成方法
CN106866583B (zh) * 2017-01-22 2019-02-19 绍兴兴欣新材料股份有限公司 一种二(2-羟乙基)哌嗪的制备方法
EP3652144B1 (en) * 2017-07-10 2022-09-07 Nouryon Chemicals International B.V. Process for making higher ethylene amines
SG11202104260RA (en) 2018-10-30 2021-05-28 Dow Global Technologies Llc Production of hydroxyethylpiperazine

Family Cites Families (8)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
DE206670C (bg) *
US3639403A (en) * 1969-03-26 1972-02-01 Jefferson Chem Co Inc Method for the preparation of piperazine and substituted piperazines
DE2716946C2 (de) * 1977-04-16 1986-05-07 Bayer Ag, 5090 Leverkusen Verfahren zur Herstellung von monohydroxyalkylierten Aminen
US4338443A (en) * 1980-08-15 1982-07-06 Texaco Inc. Synthesis of N-(2-hydroxyethyl)piperazine
DD206670A3 (de) * 1982-03-15 1984-02-01 Leuna Werke Veb Verfahren zur herstellung von n-(beta-hydroxyethyl-)piperazin
JPS58162625A (ja) * 1982-03-23 1983-09-27 Toyo Soda Mfg Co Ltd ポリウレタン製造用触媒
DE3824304A1 (de) * 1988-07-18 1990-02-22 Henkel Kgaa Verfahren zur herstellung von anlagerungsprodukten von ethylenoxid und/oder propylenoxid an amine bzw. amide
DE4325848A1 (de) * 1993-07-31 1995-02-02 Basf Ag Verfahren zur Herstellung von N-(2-Hydroxyethyl)-piperazin

Also Published As

Publication number Publication date
DE69607604T2 (de) 2000-08-10
GEP19991727B (en) 1999-08-12
PL183057B1 (pl) 2002-05-31
RU2159226C2 (ru) 2000-11-20
KR19980701986A (ko) 1998-06-25
KR100379669B1 (ko) 2003-06-09
ATE191453T1 (de) 2000-04-15
MX9705702A (es) 1998-02-28
AU699182B2 (en) 1998-11-26
AR000886A1 (es) 1997-08-06
JPH10513456A (ja) 1998-12-22
UA51638C2 (uk) 2002-12-16
HU218150B (hu) 2000-06-28
TW389756B (en) 2000-05-11
PT821664E (pt) 2000-07-31
JP3974939B2 (ja) 2007-09-12
MX197570B (es) 2000-07-17
SE9500444D0 (sv) 1995-02-08
MY112955A (en) 2001-10-31
CN1133618C (zh) 2004-01-07
NO306776B1 (no) 1999-12-20
DK0821664T3 (da) 2000-09-04
CZ231297A3 (en) 1997-11-12
WO1996024576A1 (en) 1996-08-15
ZA96351B (en) 1996-08-01
DE69607604D1 (de) 2000-05-11
AU4537696A (en) 1996-08-27
ES2146866T3 (es) 2000-08-16
CA2208439A1 (en) 1996-08-15
GR3033408T3 (en) 2000-09-29
EP0821664A1 (en) 1998-02-04
EE9700170A (et) 1998-02-16
NO973509D0 (no) 1997-07-30
HUP9702428A2 (hu) 1998-04-28
CZ291435B6 (cs) 2003-03-12
EP0821664B1 (en) 2000-04-05
PL321187A1 (en) 1997-11-24
FI973254A (fi) 1997-08-07
CN1173862A (zh) 1998-02-18
BG61943B1 (bg) 1998-10-30
NO973509L (no) 1997-07-30
SE9500444L (sv) 1996-08-09
FI973254A0 (fi) 1997-08-07
BG101668A (bg) 1998-02-27
US6013801A (en) 2000-01-11
KR19987001986A (bg) 1998-06-25
BR9607023A (pt) 1997-11-04
CA2208439C (en) 2006-12-12
EE03391B1 (et) 2001-04-16
HUP9702428A3 (en) 1999-05-28

Similar Documents

Publication Publication Date Title
SE511531C2 (sv) Förfarande för framställning av aminoetyletanolamin och/eller hydroxietylpiperazin
MXPA97005702A (en) Method for producing aminoetiletanolamine and / or hydroxyethylpiperaz
TWI762670B (zh) 製備較高分子量伸乙基胺或其脲衍生物之方法
US20090187045A1 (en) Process for preparing monomethylhydrazine
CN101522650A (zh) 通过蒸馏连续分离含有吗啉（mo）、单氨基二甘醇（adg）、氨和水的混合物的方法
US3285920A (en) Combination process for producing piperazine and triethylenediamine
US4918247A (en) Process for the preparation of 2,2-dimethylpropanediol-1,3
CN110997640B (zh) 将亚乙基胺化合物的环状单脲转化为亚乙基胺化合物的方法
US3297700A (en) Combination process for producing piperazine and nu-aminoethylpiperazine
CN110028466B (zh) 双吗啉基二乙基醚的生产方法
CN111741949B (zh) 通过蒸馏连续分离包含吗啉(mo)、单氨基二甘醇(adg)、氨、水和甲氧基乙醇(moe)的混合物的方法
US6090988A (en) Method for recovering alkyl vinyl ether
EP0096720A1 (en) Process for the preparation of B - [(2-methylpropoxy) -methyl] -N-phenyl-N- (phenylmethyl) -1-pyrrolidineethanamine.
CN112457230A (zh) 一种乙烯亚胺的分离提纯方法
EP0625519A1 (en) Method for the production of alkylene carbonates
JP4091361B2 (ja) ジアルキルカーボネートの製造方法
WO2024002740A1 (en) Method for manufacture of ethyleneamines
CA1124748A (en) Process for production of dimethylformamide
JPH0513939B2 (bg)
WO2024002748A1 (en) Method for manufacture of ethyleneamines
CN114163332A (zh) 一种从近共沸浓度碳酸二甲酯-甲醇混合物中除去甲醇制取碳酸二甲酯的工艺
KR20210084530A (ko) 하이드록시에틸피페라진의 생산
JPS58146532A (ja) ジ第３級アミンの製法

Legal Events

Date Code Title Description
NUG Patent has lapsed