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RU2009146027A - METHOD FOR HYDRAULIC CLEANING OF HYDROCARBON OIL PRODUCTS - Google Patents

METHOD FOR HYDRAULIC CLEANING OF HYDROCARBON OIL PRODUCTS Download PDF

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RU2009146027A
RU2009146027A RU2009146027/04A RU2009146027A RU2009146027A RU 2009146027 A RU2009146027 A RU 2009146027A RU 2009146027/04 A RU2009146027/04 A RU 2009146027/04A RU 2009146027 A RU2009146027 A RU 2009146027A RU 2009146027 A RU2009146027 A RU 2009146027A
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oil
hydrotreating
hydrocarbon oil
hydrogen
oil product
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RU2009146027/04A
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Russian (ru)
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Дзунси МАЦУИ (JP)
Дзунси МАЦУИ
Дзун МАСЕ (JP)
Дзун МАСЕ
Хироси ИИДА (JP)
Хироси ИИДА
Нобуюки ОХТА (JP)
Нобуюки ОХТА
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Идемицу Козан Ко., Лтд. (JP)
Идемицу Козан Ко., Лтд.
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Publication of RU2009146027A publication Critical patent/RU2009146027A/en

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    • C—CHEMISTRY; METALLURGY
    • C10—PETROLEUM, GAS OR COKE INDUSTRIES; TECHNICAL GASES CONTAINING CARBON MONOXIDE; FUELS; LUBRICANTS; PEAT
    • C10G—CRACKING HYDROCARBON OILS; PRODUCTION OF LIQUID HYDROCARBON MIXTURES, e.g. BY DESTRUCTIVE HYDROGENATION, OLIGOMERISATION, POLYMERISATION; RECOVERY OF HYDROCARBON OILS FROM OIL-SHALE, OIL-SAND, OR GASES; REFINING MIXTURES MAINLY CONSISTING OF HYDROCARBONS; REFORMING OF NAPHTHA; MINERAL WAXES
    • C10G45/00—Refining of hydrocarbon oils using hydrogen or hydrogen-generating compounds
    • C10G45/02—Refining of hydrocarbon oils using hydrogen or hydrogen-generating compounds to eliminate hetero atoms without changing the skeleton of the hydrocarbon involved and without cracking into lower boiling hydrocarbons; Hydrofinishing
    • C—CHEMISTRY; METALLURGY
    • C10—PETROLEUM, GAS OR COKE INDUSTRIES; TECHNICAL GASES CONTAINING CARBON MONOXIDE; FUELS; LUBRICANTS; PEAT
    • C10G—CRACKING HYDROCARBON OILS; PRODUCTION OF LIQUID HYDROCARBON MIXTURES, e.g. BY DESTRUCTIVE HYDROGENATION, OLIGOMERISATION, POLYMERISATION; RECOVERY OF HYDROCARBON OILS FROM OIL-SHALE, OIL-SAND, OR GASES; REFINING MIXTURES MAINLY CONSISTING OF HYDROCARBONS; REFORMING OF NAPHTHA; MINERAL WAXES
    • C10G45/00—Refining of hydrocarbon oils using hydrogen or hydrogen-generating compounds
    • C10G45/02—Refining of hydrocarbon oils using hydrogen or hydrogen-generating compounds to eliminate hetero atoms without changing the skeleton of the hydrocarbon involved and without cracking into lower boiling hydrocarbons; Hydrofinishing
    • C10G45/22—Refining of hydrocarbon oils using hydrogen or hydrogen-generating compounds to eliminate hetero atoms without changing the skeleton of the hydrocarbon involved and without cracking into lower boiling hydrocarbons; Hydrofinishing with hydrogen dissolved or suspended in the oil
    • C—CHEMISTRY; METALLURGY
    • C10—PETROLEUM, GAS OR COKE INDUSTRIES; TECHNICAL GASES CONTAINING CARBON MONOXIDE; FUELS; LUBRICANTS; PEAT
    • C10G—CRACKING HYDROCARBON OILS; PRODUCTION OF LIQUID HYDROCARBON MIXTURES, e.g. BY DESTRUCTIVE HYDROGENATION, OLIGOMERISATION, POLYMERISATION; RECOVERY OF HYDROCARBON OILS FROM OIL-SHALE, OIL-SAND, OR GASES; REFINING MIXTURES MAINLY CONSISTING OF HYDROCARBONS; REFORMING OF NAPHTHA; MINERAL WAXES
    • C10G45/00—Refining of hydrocarbon oils using hydrogen or hydrogen-generating compounds
    • C10G45/44—Hydrogenation of the aromatic hydrocarbons
    • C—CHEMISTRY; METALLURGY
    • C10—PETROLEUM, GAS OR COKE INDUSTRIES; TECHNICAL GASES CONTAINING CARBON MONOXIDE; FUELS; LUBRICANTS; PEAT
    • C10G—CRACKING HYDROCARBON OILS; PRODUCTION OF LIQUID HYDROCARBON MIXTURES, e.g. BY DESTRUCTIVE HYDROGENATION, OLIGOMERISATION, POLYMERISATION; RECOVERY OF HYDROCARBON OILS FROM OIL-SHALE, OIL-SAND, OR GASES; REFINING MIXTURES MAINLY CONSISTING OF HYDROCARBONS; REFORMING OF NAPHTHA; MINERAL WAXES
    • C10G47/00—Cracking of hydrocarbon oils, in the presence of hydrogen or hydrogen- generating compounds, to obtain lower boiling fractions
    • C—CHEMISTRY; METALLURGY
    • C10—PETROLEUM, GAS OR COKE INDUSTRIES; TECHNICAL GASES CONTAINING CARBON MONOXIDE; FUELS; LUBRICANTS; PEAT
    • C10G—CRACKING HYDROCARBON OILS; PRODUCTION OF LIQUID HYDROCARBON MIXTURES, e.g. BY DESTRUCTIVE HYDROGENATION, OLIGOMERISATION, POLYMERISATION; RECOVERY OF HYDROCARBON OILS FROM OIL-SHALE, OIL-SAND, OR GASES; REFINING MIXTURES MAINLY CONSISTING OF HYDROCARBONS; REFORMING OF NAPHTHA; MINERAL WAXES
    • C10G2300/00—Aspects relating to hydrocarbon processing covered by groups C10G1/00 - C10G99/00
    • C10G2300/10—Feedstock materials
    • C10G2300/1033—Oil well production fluids
    • C—CHEMISTRY; METALLURGY
    • C10—PETROLEUM, GAS OR COKE INDUSTRIES; TECHNICAL GASES CONTAINING CARBON MONOXIDE; FUELS; LUBRICANTS; PEAT
    • C10G—CRACKING HYDROCARBON OILS; PRODUCTION OF LIQUID HYDROCARBON MIXTURES, e.g. BY DESTRUCTIVE HYDROGENATION, OLIGOMERISATION, POLYMERISATION; RECOVERY OF HYDROCARBON OILS FROM OIL-SHALE, OIL-SAND, OR GASES; REFINING MIXTURES MAINLY CONSISTING OF HYDROCARBONS; REFORMING OF NAPHTHA; MINERAL WAXES
    • C10G2300/00—Aspects relating to hydrocarbon processing covered by groups C10G1/00 - C10G99/00
    • C10G2300/10—Feedstock materials
    • C10G2300/1037—Hydrocarbon fractions
    • C10G2300/1048—Middle distillates
    • C10G2300/1051—Kerosene having a boiling range of about 180 - 230 °C
    • C—CHEMISTRY; METALLURGY
    • C10—PETROLEUM, GAS OR COKE INDUSTRIES; TECHNICAL GASES CONTAINING CARBON MONOXIDE; FUELS; LUBRICANTS; PEAT
    • C10G—CRACKING HYDROCARBON OILS; PRODUCTION OF LIQUID HYDROCARBON MIXTURES, e.g. BY DESTRUCTIVE HYDROGENATION, OLIGOMERISATION, POLYMERISATION; RECOVERY OF HYDROCARBON OILS FROM OIL-SHALE, OIL-SAND, OR GASES; REFINING MIXTURES MAINLY CONSISTING OF HYDROCARBONS; REFORMING OF NAPHTHA; MINERAL WAXES
    • C10G2300/00—Aspects relating to hydrocarbon processing covered by groups C10G1/00 - C10G99/00
    • C10G2300/10—Feedstock materials
    • C10G2300/1037—Hydrocarbon fractions
    • C10G2300/1048—Middle distillates
    • C10G2300/1059—Gasoil having a boiling range of about 330 - 427 °C
    • C—CHEMISTRY; METALLURGY
    • C10—PETROLEUM, GAS OR COKE INDUSTRIES; TECHNICAL GASES CONTAINING CARBON MONOXIDE; FUELS; LUBRICANTS; PEAT
    • C10G—CRACKING HYDROCARBON OILS; PRODUCTION OF LIQUID HYDROCARBON MIXTURES, e.g. BY DESTRUCTIVE HYDROGENATION, OLIGOMERISATION, POLYMERISATION; RECOVERY OF HYDROCARBON OILS FROM OIL-SHALE, OIL-SAND, OR GASES; REFINING MIXTURES MAINLY CONSISTING OF HYDROCARBONS; REFORMING OF NAPHTHA; MINERAL WAXES
    • C10G2300/00—Aspects relating to hydrocarbon processing covered by groups C10G1/00 - C10G99/00
    • C10G2300/10—Feedstock materials
    • C10G2300/107—Atmospheric residues having a boiling point of at least about 538 °C
    • C—CHEMISTRY; METALLURGY
    • C10—PETROLEUM, GAS OR COKE INDUSTRIES; TECHNICAL GASES CONTAINING CARBON MONOXIDE; FUELS; LUBRICANTS; PEAT
    • C10G—CRACKING HYDROCARBON OILS; PRODUCTION OF LIQUID HYDROCARBON MIXTURES, e.g. BY DESTRUCTIVE HYDROGENATION, OLIGOMERISATION, POLYMERISATION; RECOVERY OF HYDROCARBON OILS FROM OIL-SHALE, OIL-SAND, OR GASES; REFINING MIXTURES MAINLY CONSISTING OF HYDROCARBONS; REFORMING OF NAPHTHA; MINERAL WAXES
    • C10G2300/00—Aspects relating to hydrocarbon processing covered by groups C10G1/00 - C10G99/00
    • C10G2300/10—Feedstock materials
    • C10G2300/1074—Vacuum distillates
    • C—CHEMISTRY; METALLURGY
    • C10—PETROLEUM, GAS OR COKE INDUSTRIES; TECHNICAL GASES CONTAINING CARBON MONOXIDE; FUELS; LUBRICANTS; PEAT
    • C10G—CRACKING HYDROCARBON OILS; PRODUCTION OF LIQUID HYDROCARBON MIXTURES, e.g. BY DESTRUCTIVE HYDROGENATION, OLIGOMERISATION, POLYMERISATION; RECOVERY OF HYDROCARBON OILS FROM OIL-SHALE, OIL-SAND, OR GASES; REFINING MIXTURES MAINLY CONSISTING OF HYDROCARBONS; REFORMING OF NAPHTHA; MINERAL WAXES
    • C10G2300/00—Aspects relating to hydrocarbon processing covered by groups C10G1/00 - C10G99/00
    • C10G2300/10—Feedstock materials
    • C10G2300/1077—Vacuum residues
    • C—CHEMISTRY; METALLURGY
    • C10—PETROLEUM, GAS OR COKE INDUSTRIES; TECHNICAL GASES CONTAINING CARBON MONOXIDE; FUELS; LUBRICANTS; PEAT
    • C10G—CRACKING HYDROCARBON OILS; PRODUCTION OF LIQUID HYDROCARBON MIXTURES, e.g. BY DESTRUCTIVE HYDROGENATION, OLIGOMERISATION, POLYMERISATION; RECOVERY OF HYDROCARBON OILS FROM OIL-SHALE, OIL-SAND, OR GASES; REFINING MIXTURES MAINLY CONSISTING OF HYDROCARBONS; REFORMING OF NAPHTHA; MINERAL WAXES
    • C10G2300/00—Aspects relating to hydrocarbon processing covered by groups C10G1/00 - C10G99/00
    • C10G2300/40—Characteristics of the process deviating from typical ways of processing
    • C10G2300/4018—Spatial velocity, e.g. LHSV, WHSV

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  • Chemical & Material Sciences (AREA)
  • Oil, Petroleum & Natural Gas (AREA)
  • Engineering & Computer Science (AREA)
  • Chemical Kinetics & Catalysis (AREA)
  • General Chemical & Material Sciences (AREA)
  • Organic Chemistry (AREA)
  • Production Of Liquid Hydrocarbon Mixture For Refining Petroleum (AREA)

Abstract

1. Способ гидроочистки углеводородного нефтепродукта, отличающийся тем, что он включает использование смеси тяжелой нефтяной фракции и углеводородного нефтепродукта, повышающего концентрацию растворенного водорода; перемешивание смеси фракций, которая подвергается гидроочистке, с водородом; и пропускание полученной смеси через реактор для проведения гидроочистки. ! 2. Способ гидроочистки углеводородного нефтепродукта по п.1, где смесь тяжелой нефтяной фракции и углеводородного нефтепродукта, увеличивающего концентрацию растворенного водорода, имеет концентрацию растворенного водорода, в 1,1 раз или более превышающую самую высокую возможную концентрацию водорода в тяжелой нефтяной фракции. !3. Способ гидроочистки углеводородного нефтепродукта по п.1, где тяжелая нефтяная фракция представляет собой одну или несколько фракций, выбранных из остаточной фракции вакуумной перегонки, газойля вакуумной перегонки, остаточной фракции перегонки при атмосферном давлении, отбензиненной нефти, сырой нефти, деасфальтезированной нефти, углемазутной нефти, нефти, выделенной из нефтяных песков, и нефти, полученной из нефтяного сланца. ! 4. Способ гидроочистки углеводородного нефтепродукта по п.1, где углеводородный нефтепродукт, повышающий концентрацию растворенного водорода, в условиях реактора содержится в жидкой фазе полностью или частично. ! 5. Способ гидроочистки углеводородного нефтепродукта по п. 1, где эффект повышения концентрации растворенного водорода оценивают на основе равновесия водорода между газовой и жидкой фазой в реакторе. ! 6. Способ гидроочистки углеводородного нефтепродукта по п.1, где в реакто� 1. A method for hydrotreating a hydrocarbon oil product, characterized in that it includes the use of a mixture of a heavy oil fraction and a hydrocarbon oil product, which increases the concentration of dissolved hydrogen; mixing the mixture of fractions, which is being hydrotreated, with hydrogen; and passing the resulting mixture through a hydrotreating reactor. ! 2. The method for hydrotreating a hydrocarbon oil product according to claim 1, wherein the mixture of a heavy oil fraction and a hydrocarbon oil product increasing the concentration of dissolved hydrogen has a dissolved hydrogen concentration 1.1 times or more higher than the highest possible concentration of hydrogen in the heavy oil fraction. ! 3. The method for hydrotreating a hydrocarbon oil product according to claim 1, where the heavy oil fraction is one or more fractions selected from the residual fraction of vacuum distillation, vacuum gas oil, residual fraction of distillation at atmospheric pressure, stripped oil, crude oil, deasphalted oil, coal-fuel oil, oil extracted from oil sands; and oil obtained from oil shale. ! 4. The method of hydrotreating a hydrocarbon oil product according to claim 1, where the hydrocarbon oil product, which increases the concentration of dissolved hydrogen, is contained in the liquid phase in full or in part in the reactor conditions. ! 5. A method for hydrotreating a hydrocarbon oil product according to claim 1, where the effect of increasing the concentration of dissolved hydrogen is estimated based on the equilibrium of hydrogen between the gas and liquid phases in the reactor. ! 6. A method for hydrotreating a hydrocarbon oil product according to claim 1, where the reactor

Claims (10)

1. Способ гидроочистки углеводородного нефтепродукта, отличающийся тем, что он включает использование смеси тяжелой нефтяной фракции и углеводородного нефтепродукта, повышающего концентрацию растворенного водорода; перемешивание смеси фракций, которая подвергается гидроочистке, с водородом; и пропускание полученной смеси через реактор для проведения гидроочистки.1. The method of hydrotreating a hydrocarbon oil product, characterized in that it involves the use of a mixture of a heavy oil fraction and a hydrocarbon oil product that increases the concentration of dissolved hydrogen; mixing the mixture of fractions that is hydrotreated with hydrogen; and passing the resulting mixture through a hydrotreatment reactor. 2. Способ гидроочистки углеводородного нефтепродукта по п.1, где смесь тяжелой нефтяной фракции и углеводородного нефтепродукта, увеличивающего концентрацию растворенного водорода, имеет концентрацию растворенного водорода, в 1,1 раз или более превышающую самую высокую возможную концентрацию водорода в тяжелой нефтяной фракции.2. The method of hydrotreating a hydrocarbon oil product according to claim 1, where the mixture of a heavy oil fraction and a hydrocarbon oil product that increases the concentration of dissolved hydrogen has a concentration of dissolved hydrogen 1.1 times or more higher than the highest possible concentration of hydrogen in the heavy oil fraction. 3. Способ гидроочистки углеводородного нефтепродукта по п.1, где тяжелая нефтяная фракция представляет собой одну или несколько фракций, выбранных из остаточной фракции вакуумной перегонки, газойля вакуумной перегонки, остаточной фракции перегонки при атмосферном давлении, отбензиненной нефти, сырой нефти, деасфальтезированной нефти, углемазутной нефти, нефти, выделенной из нефтяных песков, и нефти, полученной из нефтяного сланца.3. The method of hydrotreating a hydrocarbon oil product according to claim 1, where the heavy oil fraction is one or more fractions selected from the residual fraction of vacuum distillation, gas oil vacuum distillation, the residual fraction of distillation at atmospheric pressure, stripped oil, crude oil, deasphalted oil, coal oil oil, oil extracted from oil sands, and oil obtained from oil shale. 4. Способ гидроочистки углеводородного нефтепродукта по п.1, где углеводородный нефтепродукт, повышающий концентрацию растворенного водорода, в условиях реактора содержится в жидкой фазе полностью или частично.4. The method of hydrotreating a hydrocarbon oil product according to claim 1, where the hydrocarbon oil product that increases the concentration of dissolved hydrogen in the reactor is contained in the liquid phase in whole or in part. 5. Способ гидроочистки углеводородного нефтепродукта по п. 1, где эффект повышения концентрации растворенного водорода оценивают на основе равновесия водорода между газовой и жидкой фазой в реакторе.5. The method of hydrotreating a hydrocarbon oil product according to claim 1, where the effect of increasing the concentration of dissolved hydrogen is evaluated based on the equilibrium of hydrogen between the gas and liquid phases in the reactor. 6. Способ гидроочистки углеводородного нефтепродукта по п.1, где в реактор дополнительно вводят углеводородный нефтепродукт, повышающий концентрацию растворенного водорода, в качестве закалочного масла.6. The method of hydrotreating a hydrocarbon oil product according to claim 1, where an additional hydrocarbon oil product is added to the reactor, which increases the concentration of dissolved hydrogen, as quenching oil. 7. Способ гидроочистки углеводородного нефтепродукта по п.1, где углеводородный нефтепродукт, повышающий концентрацию растворенного водорода, представляет собой одну или несколько фракций, выбранных из керосиновой фракции прямой перегонки, фракции легкого газойля прямой перегонки, фракции тяжелого газойля прямой перегонки, крекированной нефти, полученной из установки FCC, и нефти термического крекинга, полученной из установки для коксования.7. The method of hydrotreating a hydrocarbon oil product according to claim 1, where the hydrocarbon oil product that increases the concentration of dissolved hydrogen is one or more fractions selected from a kerosene fraction of direct distillation, a fraction of light gas oil of direct distillation, a fraction of heavy gas oil of direct distillation, cracked oil obtained from the FCC unit, and thermal cracking oil obtained from the coking unit. 8. Способ гидроочистки углеводородного нефтепродукта по п.1, где гидроочистка включает одну или несколько стадий, выбранных из стадии гидродеметаллизации, стадии гидрообессеривания, стадии гидрокрекинга, стадии гидродеазотирования и стадии гидродеароматизации.8. The method of hydrotreating a hydrocarbon oil product according to claim 1, where hydrotreating includes one or more stages selected from a hydrodemetallization step, a hydrodesulfurization step, a hydrocracking step, a hydrodeazotization step, and a hydrodearomatization step. 9. Способ гидроочистки углеводородного нефтепродукта по п.1, где гидроочистку осуществляют в следующих условиях: температуре реакции от 300 до 450°С, парциальном давлении водорода от 5,1 до 25,3 МПа(Г), отношении водород/углеводородный нефтепродукт от 200 до 2000 Нм3/кл и LHSV от 0,05 до 10 ч-1.9. The method of hydrotreating a hydrocarbon oil product according to claim 1, where hydrotreating is carried out under the following conditions: reaction temperature from 300 to 450 ° C, a partial pressure of hydrogen from 5.1 to 25.3 MPa (G), the ratio of hydrogen / hydrocarbon oil from 200 up to 2000 Nm 3 / cell and LHSV from 0.05 to 10 h -1 . 10. Способ гидроочистки углеводородного нефтепродукта по п.1, где гидроочистку осуществляют в следующих условиях: температуре реакции от 330 до 430°С, парциальном давлении водорода от 10,1 до 20,3 МПа (Г), отношении водород/углеводородный нефтепродукт от 500 до 1000 Нм3/кл и LHSV от 0,1 до 1,0 ч-1. 10. The method of hydrotreating a hydrocarbon oil product according to claim 1, where hydrotreating is carried out under the following conditions: reaction temperature from 330 to 430 ° C, a partial pressure of hydrogen from 10.1 to 20.3 MPa (G), the ratio of hydrogen / hydrocarbon oil from 500 up to 1000 Nm 3 / cell and LHSV from 0.1 to 1.0 h -1 .
RU2009146027/04A 2007-07-24 2008-06-26 METHOD FOR HYDRAULIC CLEANING OF HYDROCARBON OIL PRODUCTS RU2009146027A (en)

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US20140221713A1 (en) * 2013-02-04 2014-08-07 Lummus Technology Inc. Residue hydrocracking processing

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TW200920835A (en) 2009-05-16
EP2169031A1 (en) 2010-03-31

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