NO753867L - - Google Patents

Info

Publication number: NO753867L
Authority: NO; Norway
Prior art keywords: electrolyte; electrolysis; electrolytic; particles; temperature
Prior art date: 1974-11-18

Application number

NO753867A

Other languages

English (en)

Norwegian (no)

Inventor

S-I Tokumoto

E Tanaka

K Ogisu

H Kawai

Original Assignee

Sony Corp

Priority date (The priority date is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the date listed.)

1974-11-18

Filing date

1975-11-18

Publication date

1976-05-19

1975-11-18 Application filed by Sony Corp filed Critical Sony Corp

1976-05-19 Publication of NO753867L publication Critical patent/NO753867L/no

Links

239000003792 electrolyte Substances 0.000 claims description 183
239000002245 particle Substances 0.000 claims description 79
238000005868 electrolysis reaction Methods 0.000 claims description 69
229910052751 metal Inorganic materials 0.000 claims description 57
239000002184 metal Substances 0.000 claims description 57
238000001556 precipitation Methods 0.000 claims description 55
239000007787 solid Substances 0.000 claims description 42
230000008021 deposition Effects 0.000 claims description 40
150000003839 salts Chemical class 0.000 claims description 39
238000000034 method Methods 0.000 claims description 34
229910045601 alloy Inorganic materials 0.000 claims description 22
239000000956 alloy Substances 0.000 claims description 22
230000008569 process Effects 0.000 claims description 17
TWRXJAOTZQYOKJ-UHFFFAOYSA-L Magnesium chloride Chemical compound [Mg+2].[Cl-].[Cl-] TWRXJAOTZQYOKJ-UHFFFAOYSA-L 0.000 claims description 16
239000011343 solid material Substances 0.000 claims description 12
ZWYDDDAMNQQZHD-UHFFFAOYSA-L titanium(ii) chloride Chemical compound [Cl-].[Cl-].[Ti+2] ZWYDDDAMNQQZHD-UHFFFAOYSA-L 0.000 claims description 12
229910010068 TiCl2 Inorganic materials 0.000 claims description 11
239000011346 highly viscous material Substances 0.000 claims description 9
229910001629 magnesium chloride Inorganic materials 0.000 claims description 8
238000002844 melting Methods 0.000 claims description 8
230000008018 melting Effects 0.000 claims description 8
FAPWRFPIFSIZLT-UHFFFAOYSA-M Sodium chloride Chemical compound [Na+].[Cl-] FAPWRFPIFSIZLT-UHFFFAOYSA-M 0.000 claims description 6
229910010062 TiCl3 Inorganic materials 0.000 claims description 6
230000015572 biosynthetic process Effects 0.000 claims description 6
YONPGGFAJWQGJC-UHFFFAOYSA-K titanium(iii) chloride Chemical compound Cl[Ti](Cl)Cl YONPGGFAJWQGJC-UHFFFAOYSA-K 0.000 claims description 6
239000011780 sodium chloride Substances 0.000 claims description 3
229910004298 SiO 2 Inorganic materials 0.000 claims description 2
229910001626 barium chloride Inorganic materials 0.000 claims description 2
WDIHJSXYQDMJHN-UHFFFAOYSA-L barium chloride Chemical compound [Cl-].[Cl-].[Ba+2] WDIHJSXYQDMJHN-UHFFFAOYSA-L 0.000 claims description 2
UXVMQQNJUSDDNG-UHFFFAOYSA-L Calcium chloride Chemical compound [Cl-].[Cl-].[Ca+2] UXVMQQNJUSDDNG-UHFFFAOYSA-L 0.000 claims 1
239000001110 calcium chloride Substances 0.000 claims 1
229910001628 calcium chloride Inorganic materials 0.000 claims 1
235000011148 calcium chloride Nutrition 0.000 claims 1
150000003841 chloride salts Chemical class 0.000 claims 1
239000000203 mixture Substances 0.000 description 23
239000010936 titanium Substances 0.000 description 19
238000003756 stirring Methods 0.000 description 17
239000002994 raw material Substances 0.000 description 16
229910052719 titanium Inorganic materials 0.000 description 16
RTAQQCXQSZGOHL-UHFFFAOYSA-N Titanium Chemical compound [Ti] RTAQQCXQSZGOHL-UHFFFAOYSA-N 0.000 description 14
230000000694 effects Effects 0.000 description 11
239000000463 material Substances 0.000 description 11
150000001875 compounds Chemical class 0.000 description 9
238000013019 agitation Methods 0.000 description 8
239000013078 crystal Substances 0.000 description 8
238000007323 disproportionation reaction Methods 0.000 description 8
239000000243 solution Substances 0.000 description 8
OKTJSMMVPCPJKN-UHFFFAOYSA-N Carbon Chemical compound [C] OKTJSMMVPCPJKN-UHFFFAOYSA-N 0.000 description 7
238000004458 analytical method Methods 0.000 description 7
229910052799 carbon Inorganic materials 0.000 description 7
238000006243 chemical reaction Methods 0.000 description 7
238000005137 deposition process Methods 0.000 description 7
VEXZGXHMUGYJMC-UHFFFAOYSA-N Hydrochloric acid Chemical compound Cl VEXZGXHMUGYJMC-UHFFFAOYSA-N 0.000 description 6
239000006185 dispersion Substances 0.000 description 6
150000003608 titanium Chemical class 0.000 description 6
IJGRMHOSHXDMSA-UHFFFAOYSA-N Atomic nitrogen Chemical compound N#N IJGRMHOSHXDMSA-UHFFFAOYSA-N 0.000 description 4
UFHFLCQGNIYNRP-UHFFFAOYSA-N Hydrogen Chemical compound [H][H] UFHFLCQGNIYNRP-UHFFFAOYSA-N 0.000 description 4
239000007864 aqueous solution Substances 0.000 description 4
238000002425 crystallisation Methods 0.000 description 4
230000008025 crystallization Effects 0.000 description 4
230000007423 decrease Effects 0.000 description 4
210000001787 dendrite Anatomy 0.000 description 4
230000001105 regulatory effect Effects 0.000 description 4
239000010935 stainless steel Substances 0.000 description 4
229910001220 stainless steel Inorganic materials 0.000 description 4
230000009471 action Effects 0.000 description 3
238000001816 cooling Methods 0.000 description 3
239000011888 foil Substances 0.000 description 3
239000007791 liquid phase Substances 0.000 description 3
239000011777 magnesium Substances 0.000 description 3
238000010907 mechanical stirring Methods 0.000 description 3
150000002739 metals Chemical class 0.000 description 3
239000012071 phase Substances 0.000 description 3
238000010587 phase diagram Methods 0.000 description 3
229910052573 porcelain Inorganic materials 0.000 description 3
239000002244 precipitate Substances 0.000 description 3
230000009467 reduction Effects 0.000 description 3
150000003609 titanium compounds Chemical class 0.000 description 3
-1 titanium salt Chemical class 0.000 description 3
RYGMFSIKBFXOCR-UHFFFAOYSA-N Copper Chemical group [Cu] RYGMFSIKBFXOCR-UHFFFAOYSA-N 0.000 description 2
FYYHWMGAXLPEAU-UHFFFAOYSA-N Magnesium Chemical compound [Mg] FYYHWMGAXLPEAU-UHFFFAOYSA-N 0.000 description 2
PWHULOQIROXLJO-UHFFFAOYSA-N Manganese Chemical compound [Mn] PWHULOQIROXLJO-UHFFFAOYSA-N 0.000 description 2
ZOKXTWBITQBERF-UHFFFAOYSA-N Molybdenum Chemical compound [Mo] ZOKXTWBITQBERF-UHFFFAOYSA-N 0.000 description 2
230000018199 S phase Effects 0.000 description 2
QAOWNCQODCNURD-UHFFFAOYSA-N Sulfuric acid Chemical compound OS(O)(=O)=O QAOWNCQODCNURD-UHFFFAOYSA-N 0.000 description 2
239000012300 argon atmosphere Substances 0.000 description 2
QVGXLLKOCUKJST-UHFFFAOYSA-N atomic oxygen Chemical compound [O] QVGXLLKOCUKJST-UHFFFAOYSA-N 0.000 description 2
159000000009 barium salts Chemical class 0.000 description 2
238000004090 dissolution Methods 0.000 description 2
238000009826 distribution Methods 0.000 description 2
KWGKDLIKAYFUFQ-UHFFFAOYSA-M lithium chloride Chemical compound [Li+].[Cl-] KWGKDLIKAYFUFQ-UHFFFAOYSA-M 0.000 description 2
229910052749 magnesium Inorganic materials 0.000 description 2
229910052748 manganese Inorganic materials 0.000 description 2
239000011572 manganese Substances 0.000 description 2
238000004519 manufacturing process Methods 0.000 description 2
239000012528 membrane Substances 0.000 description 2
229910052750 molybdenum Inorganic materials 0.000 description 2
239000011733 molybdenum Substances 0.000 description 2
229910052757 nitrogen Inorganic materials 0.000 description 2
230000010355 oscillation Effects 0.000 description 2
239000001301 oxygen Substances 0.000 description 2
229910052760 oxygen Inorganic materials 0.000 description 2
238000005498 polishing Methods 0.000 description 2
239000000843 powder Substances 0.000 description 2
239000000047 product Substances 0.000 description 2
XJDNKRIXUMDJCW-UHFFFAOYSA-J titanium tetrachloride Chemical compound Cl[Ti](Cl)(Cl)Cl XJDNKRIXUMDJCW-UHFFFAOYSA-J 0.000 description 2
229910000497 Amalgam Inorganic materials 0.000 description 1
229910052582 BN Inorganic materials 0.000 description 1
ZOXJGFHDIHLPTG-UHFFFAOYSA-N Boron Chemical compound [B] ZOXJGFHDIHLPTG-UHFFFAOYSA-N 0.000 description 1
PZNSFCLAULLKQX-UHFFFAOYSA-N Boron nitride Chemical compound N#B PZNSFCLAULLKQX-UHFFFAOYSA-N 0.000 description 1
CPELXLSAUQHCOX-UHFFFAOYSA-M Bromide Chemical compound [Br-] CPELXLSAUQHCOX-UHFFFAOYSA-M 0.000 description 1
VEXZGXHMUGYJMC-UHFFFAOYSA-M Chloride anion Chemical compound [Cl-] VEXZGXHMUGYJMC-UHFFFAOYSA-M 0.000 description 1
KRHYYFGTRYWZRS-UHFFFAOYSA-M Fluoride anion Chemical compound [F-] KRHYYFGTRYWZRS-UHFFFAOYSA-M 0.000 description 1
229910000914 Mn alloy Inorganic materials 0.000 description 1
BQCADISMDOOEFD-UHFFFAOYSA-N Silver Chemical compound [Ag] BQCADISMDOOEFD-UHFFFAOYSA-N 0.000 description 1
UCKMPCXJQFINFW-UHFFFAOYSA-N Sulphide Chemical compound [S-2] UCKMPCXJQFINFW-UHFFFAOYSA-N 0.000 description 1
229910001069 Ti alloy Inorganic materials 0.000 description 1
229910052770 Uranium Inorganic materials 0.000 description 1
238000002441 X-ray diffraction Methods 0.000 description 1
238000004125 X-ray microanalysis Methods 0.000 description 1
HCHKCACWOHOZIP-UHFFFAOYSA-N Zinc Chemical compound [Zn] HCHKCACWOHOZIP-UHFFFAOYSA-N 0.000 description 1
QCWXUUIWCKQGHC-UHFFFAOYSA-N Zirconium Chemical compound [Zr] QCWXUUIWCKQGHC-UHFFFAOYSA-N 0.000 description 1
238000009825 accumulation Methods 0.000 description 1
239000002253 acid Substances 0.000 description 1
229910001514 alkali metal chloride Inorganic materials 0.000 description 1
150000001340 alkali metals Chemical class 0.000 description 1
229910001617 alkaline earth metal chloride Inorganic materials 0.000 description 1
238000005275 alloying Methods 0.000 description 1
239000004411 aluminium Substances 0.000 description 1
229910052782 aluminium Inorganic materials 0.000 description 1
XAGFODPZIPBFFR-UHFFFAOYSA-N aluminium Chemical compound [Al] XAGFODPZIPBFFR-UHFFFAOYSA-N 0.000 description 1
230000002547 anomalous effect Effects 0.000 description 1
229910052796 boron Inorganic materials 0.000 description 1
230000015556 catabolic process Effects 0.000 description 1
210000004027 cell Anatomy 0.000 description 1
230000008859 change Effects 0.000 description 1
238000010276 construction Methods 0.000 description 1
238000011109 contamination Methods 0.000 description 1
229910052802 copper Inorganic materials 0.000 description 1
239000010949 copper Substances 0.000 description 1
230000001419 dependent effect Effects 0.000 description 1
238000006073 displacement reaction Methods 0.000 description 1
239000002659 electrodeposit Substances 0.000 description 1
239000004744 fabric Substances 0.000 description 1
238000005243 fluidization Methods 0.000 description 1
239000007789 gas Substances 0.000 description 1
239000011521 glass Substances 0.000 description 1
238000010438 heat treatment Methods 0.000 description 1
230000003993 interaction Effects 0.000 description 1
239000007788 liquid Substances 0.000 description 1
230000007246 mechanism Effects 0.000 description 1
239000000155 melt Substances 0.000 description 1
229910021645 metal ion Inorganic materials 0.000 description 1
239000013528 metallic particle Substances 0.000 description 1
229910052758 niobium Inorganic materials 0.000 description 1
239000010955 niobium Substances 0.000 description 1
GUCVJGMIXFAOAE-UHFFFAOYSA-N niobium atom Chemical compound [Nb] GUCVJGMIXFAOAE-UHFFFAOYSA-N 0.000 description 1
150000004767 nitrides Chemical class 0.000 description 1
230000000704 physical effect Effects 0.000 description 1
239000010453 quartz Substances 0.000 description 1
230000000284 resting effect Effects 0.000 description 1
238000005070 sampling Methods 0.000 description 1
238000000926 separation method Methods 0.000 description 1
VYPSYNLAJGMNEJ-UHFFFAOYSA-N silicon dioxide Inorganic materials O=[Si]=O VYPSYNLAJGMNEJ-UHFFFAOYSA-N 0.000 description 1
229910052709 silver Inorganic materials 0.000 description 1
239000004332 silver Substances 0.000 description 1
159000000000 sodium salts Chemical class 0.000 description 1
239000007790 solid phase Substances 0.000 description 1
239000012086 standard solution Substances 0.000 description 1
239000004575 stone Substances 0.000 description 1
229910052715 tantalum Inorganic materials 0.000 description 1
GUVRBAGPIYLISA-UHFFFAOYSA-N tantalum atom Chemical compound [Ta] GUVRBAGPIYLISA-UHFFFAOYSA-N 0.000 description 1
238000004448 titration Methods 0.000 description 1
DNYWZCXLKNTFFI-UHFFFAOYSA-N uranium Chemical compound [U][U][U][U][U][U][U][U][U][U][U][U][U][U][U][U][U][U][U][U][U][U][U][U][U][U][U][U][U][U][U][U][U][U][U][U][U][U][U][U][U][U][U][U][U][U][U][U][U][U][U][U][U][U][U][U][U][U][U][U][U][U][U][U][U][U][U][U][U][U][U][U][U][U][U][U][U][U][U][U][U][U][U][U][U][U][U][U][U][U][U][U][U][U][U][U][U][U][U][U][U][U][U][U][U][U][U][U][U][U][U][U][U][U] DNYWZCXLKNTFFI-UHFFFAOYSA-N 0.000 description 1
229910052725 zinc Inorganic materials 0.000 description 1
239000011701 zinc Substances 0.000 description 1
229910052726 zirconium Inorganic materials 0.000 description 1

Classifications

- C—CHEMISTRY; METALLURGY
- C25—ELECTROLYTIC OR ELECTROPHORETIC PROCESSES; APPARATUS THEREFOR
- C25D—PROCESSES FOR THE ELECTROLYTIC OR ELECTROPHORETIC PRODUCTION OF COATINGS; ELECTROFORMING; APPARATUS THEREFOR
- C25D3/00—Electroplating: Baths therefor
- C25D3/66—Electroplating: Baths therefor from melts

Landscapes

Chemical & Material Sciences (AREA)
Engineering & Computer Science (AREA)
Chemical Kinetics & Catalysis (AREA)
Electrochemistry (AREA)
Materials Engineering (AREA)
Metallurgy (AREA)
Organic Chemistry (AREA)
Electrolytic Production Of Metals (AREA)
Electroplating Methods And Accessories (AREA)
Silicon Compounds (AREA)

NO753867A 1974-11-18 1975-11-18 NO753867L (it)

Applications Claiming Priority (1)

Application Number	Priority Date	Filing Date	Title
JP13196074A JPS5636238B2 (it)	1974-11-18	1974-11-18

Publications (1)

Publication Number	Publication Date
NO753867L true NO753867L (it)	1976-05-19

Family

ID=15070228

Family Applications (1)

Application Number	Title	Priority Date	Filing Date
NO753867A NO753867L (it)	1974-11-18	1975-11-18

Country Status (9)

Country	Link
JP (1)	JPS5636238B2 (it)
AU (1)	AU506646B2 (it)
CA (1)	CA1073400A (it)
DE (1)	DE2551727C3 (it)
FR (1)	FR2291294A1 (it)
GB (1)	GB1504356A (it)
IT (1)	IT1064458B (it)
NO (1)	NO753867L (it)
SE (1)	SE414196B (it)

Families Citing this family (5)

* Cited by examiner, † Cited by third party
Publication number	Priority date	Publication date	Assignee	Title
JPS5817269B2 (ja) *	1976-12-17	1983-04-06	ソニー株式会社	チタン又はチタン合金の電着法
JP4711724B2 (ja) *	2005-04-19	2011-06-29	学校法人同志社	溶融塩めっき用電解浴及び該電解浴を用いた溶融塩めっき方法
JP2012031471A (ja) *	2010-07-30	2012-02-16	Yoshiji Ichihara	電気めっき方法及びめっき部材の製造方法
CN107460502A (zh) *	2017-09-21	2017-12-12	北京工业大学	一种添加固相微粒的熔盐电沉积制备合金的方法
JP6875711B2 (ja) *	2020-03-23	2021-05-26	日本製鉄株式会社	溶融塩電解による金属チタン箔の製造方法

1974
- 1974-11-18 JP JP13196074A patent/JPS5636238B2/ja not_active Expired
1975
- 1975-11-12 AU AU86554/75A patent/AU506646B2/en not_active Ceased
- 1975-11-14 GB GB47121/75A patent/GB1504356A/en not_active Expired
- 1975-11-18 DE DE2551727A patent/DE2551727C3/de not_active Expired
- 1975-11-18 IT IT29407/75A patent/IT1064458B/it active
- 1975-11-18 SE SE7512932A patent/SE414196B/xx not_active IP Right Cessation
- 1975-11-18 FR FR7535228A patent/FR2291294A1/fr active Granted
- 1975-11-18 NO NO753867A patent/NO753867L/no unknown
- 1975-11-18 CA CA239,861A patent/CA1073400A/en not_active Expired

Also Published As

Publication number	Publication date
CA1073400A (en)	1980-03-11
FR2291294B1 (it)	1983-10-28
JPS5157605A (it)	1976-05-20
FR2291294A1 (fr)	1976-06-11
DE2551727B2 (de)	1980-04-30
GB1504356A (en)	1978-03-22
AU506646B2 (en)	1980-01-17
AU8655475A (en)	1977-05-19
DE2551727C3 (de)	1981-01-08
JPS5636238B2 (it)	1981-08-22
IT1064458B (it)	1985-02-18
SE414196B (sv)	1980-07-14
SE7512932L (sv)	1976-05-19
DE2551727A1 (de)	1976-05-26

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JP5011468B2 (ja)	2012-08-29	金属または金属合金の生成方法、電解セル、および溶融塩電解質
Pradhan et al.	2009	The effect of electrode surface modification and cathode overpotential on deposit characteristics in aluminum electrorefining using EMIC–AlCl3 ionic liquid electrolyte
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JP2863058B2 (ja)	1999-03-03	均質で純粋なインゴットに加工することのできる耐熱金属合金及び該合金の製造方法
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US2848397A (en)	1958-08-19	Electrolytic production of metallic titanium
US4016052A (en)	1977-04-05	Electrodeposition process
EP0142829B1 (en)	1991-02-06	Method of producing a high purity aluminum-lithium mother alloy
US20110100831A1 (en)	2011-05-05	Method of determining the extent of a metal oxide reduction
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NO144640B (no)	1981-06-29	Fremgangsmaate for fremstilling av et kompakt, skorpeformet beskyttelsesmaterial i en celle for smelteelektrolyse av aluminiumoksyd
US3775271A (en)	1973-11-27	Electrolytic preparation of titanium and zirconium diborides using a molten, sodium salt electrolyte
JP4198434B2 (ja)	2008-12-17	金属チタンの製錬方法
JP4756132B2 (ja)	2011-08-24	炭素質皮膜及びその製造方法
CN108642529B (zh)	2021-02-02	基于调配阳离子的亚稳态高温熔盐电解精炼高纯钛的方法
JP4198439B2 (ja)	2008-12-17	金属チタン製錬用の消耗性炭素陽極
US4108741A (en)	1978-08-22	Process for production of aluminum
RU2827173C2 (ru)	2024-09-23	Способ получения металлического титана путем восстановления диоксида титана электролизом расплавленной соли