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MY120567A - Method for producing acrylic acid and acrylic acid esters. - Google Patents

Method for producing acrylic acid and acrylic acid esters.

Info

Publication number
MY120567A
MY120567A MYPI99001164A MYPI9901164A MY120567A MY 120567 A MY120567 A MY 120567A MY PI99001164 A MYPI99001164 A MY PI99001164A MY PI9901164 A MYPI9901164 A MY PI9901164A MY 120567 A MY120567 A MY 120567A
Authority
MY
Malaysia
Prior art keywords
acrylic acid
give
mixture
esters
acrylates
Prior art date
Application number
MYPI99001164A
Inventor
Gerhard Dr Bolz
Gerhard Dr Nestler
Jurgen Dr Schroder
Original Assignee
Basf Ag
Priority date (The priority date is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the date listed.)
Filing date
Publication date
Application filed by Basf Ag filed Critical Basf Ag
Publication of MY120567A publication Critical patent/MY120567A/en

Links

Classifications

    • C—CHEMISTRY; METALLURGY
    • C07—ORGANIC CHEMISTRY
    • C07C—ACYCLIC OR CARBOCYCLIC COMPOUNDS
    • C07C51/00—Preparation of carboxylic acids or their salts, halides or anhydrides
    • C07C51/42—Separation; Purification; Stabilisation; Use of additives
    • C07C51/43—Separation; Purification; Stabilisation; Use of additives by change of the physical state, e.g. crystallisation
    • C07C51/44—Separation; Purification; Stabilisation; Use of additives by change of the physical state, e.g. crystallisation by distillation
    • C—CHEMISTRY; METALLURGY
    • C07—ORGANIC CHEMISTRY
    • C07C—ACYCLIC OR CARBOCYCLIC COMPOUNDS
    • C07C67/00—Preparation of carboxylic acid esters
    • C07C67/08—Preparation of carboxylic acid esters by reacting carboxylic acids or symmetrical anhydrides with the hydroxy or O-metal group of organic compounds

Landscapes

  • Chemical & Material Sciences (AREA)
  • Organic Chemistry (AREA)
  • Crystallography & Structural Chemistry (AREA)
  • Engineering & Computer Science (AREA)
  • Oil, Petroleum & Natural Gas (AREA)
  • Organic Low-Molecular-Weight Compounds And Preparation Thereof (AREA)

Abstract

A PROCESS FOR PREPARING ACRYLIC ACID AND/OR AN ACRYLATE COMPRISING THE FOLLOWING STAGE A AND, IF DESIRED, B AND, IF DESIRED, C: A: COOLING A GASEOUS REACTION MIXTURE WHICH COMPRISES ACRYLIC ACID AND IS OBTAINED IN THE GAS-PHASE OXIDATION TO PREPARE ACRYLIC ACID, USING AN ACRYLIC ACID CONTAINING NOT MORE THAN 5% BY WEIGHT OF WATER, TO GIVE A GASEOUS MIXTURE COMPRISING (METH)ACRYLIC ACID; B: SEPARATING THE GASEOUS MIXTURE COMPRISING ACRYLIC ACID TO GIVE A LOW-BOILING FRACTION AND A BOTTOM PRODUCT WHICH COMPRISES CRUDE ACRYLIC ACID, AND C: ESTERIFYING THE CRUDE ACRYLIC ACID OBTAINED IN STAGE B BY MEANS OF ONE OR MORE ALKANOLS, TO GIVE AN ESTERIFICATION MIXTURE COMPRISING ONE OR MORE ACRYLATES, ONE OR MORE ACETIC ESTERS, ONE OR MORE MALEIC ESTERS, AND OLIGOMERIC AND POLYMERIC ACRYLATES.
MYPI99001164A 1998-03-31 1999-03-26 Method for producing acrylic acid and acrylic acid esters. MY120567A (en)

Applications Claiming Priority (1)

Application Number Priority Date Filing Date Title
DE19814421A DE19814421A1 (en) 1998-03-31 1998-03-31 Process for the production of acrylic acid and acrylic acid esters

Publications (1)

Publication Number Publication Date
MY120567A true MY120567A (en) 2005-11-30

Family

ID=7863128

Family Applications (1)

Application Number Title Priority Date Filing Date
MYPI99001164A MY120567A (en) 1998-03-31 1999-03-26 Method for producing acrylic acid and acrylic acid esters.

Country Status (7)

Country Link
EP (1) EP1068174B1 (en)
JP (1) JP5021116B2 (en)
CN (1) CN1137079C (en)
BR (1) BR9909312B1 (en)
DE (2) DE19814421A1 (en)
MY (1) MY120567A (en)
WO (1) WO1999050222A1 (en)

Families Citing this family (19)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
DE19851983A1 (en) 1998-11-11 2000-05-18 Basf Ag Process for the continuous production of alkyl esters of (meth) acrylic acid
MY122671A (en) 1999-03-06 2006-04-29 Basf Ag Fractional condensation of a product gas mixture containing acrylic acid
US6498272B1 (en) 1999-03-06 2002-12-24 Basf Aktiengesellschaft Method for producing acrylic acid
JP3885486B2 (en) * 2000-11-16 2007-02-21 東亞合成株式会社 Polymerization inhibitor composition for vinyl monomer and method for producing high purity (meth) acrylic acid
DE10063161A1 (en) * 2000-12-18 2002-06-20 Basf Ag Process for quenching a hot gas mixture containing (meth) acrylic acid
US7592483B2 (en) 2004-07-01 2009-09-22 Basf Aktiengesellschaft Preparation of acrolein or acrylic acid or a mixture thereof by heterogeneously catalyzed partial gas phase oxidation of propylene
JP4732366B2 (en) 2004-08-02 2011-07-27 エルジー・ケム・リミテッド Method for producing (meth) acrylic acid
US7705181B2 (en) 2005-03-01 2010-04-27 Basf Akiengesellschaft Process for removing methacrylic acid from liquid phase comprising acrylic acid as a main constituent and target product, and methacrylic acid as a secondary component
JP2007191435A (en) * 2006-01-19 2007-08-02 Nippon Shokubai Co Ltd Method for producing (meth)acrylic acid
KR101424522B1 (en) 2006-09-15 2014-08-13 알케마 인코포레이티드 Process for producing acrylic acid
DE102008040799A1 (en) 2008-07-28 2008-12-11 Basf Se Separating a three carbon precursor compound of acrylic acid as main component containing acrylic acid and as byproduct containing glyoxal, in a product mixture of a heterogeneously catalyzed partial gas phase oxidation
DE102008041573A1 (en) 2008-08-26 2010-03-04 Basf Se Separating acrylic acid and glyoxal from gaseous product mixture of gas phase oxidation of a three carbon-precursor compound of acrylic acid comprises producing a liquid phase containing acrylic acid and glyoxal, and separating glyoxal
KR101861855B1 (en) 2008-07-28 2018-05-28 바스프 에스이 Method for separating acrylic acid, contained as the main constituent, and glyoxal, contained as a by-product, from a gaseous product mixture of a c3 precursor compound of acrylic acid
JP5169899B2 (en) * 2009-02-19 2013-03-27 東亞合成株式会社 Method for producing alkyl acrylate ester
DE102010042216A1 (en) 2010-10-08 2011-06-09 Basf Se Inhibiting the unwanted radical polymerization of acrylic acid present in a liquid phase, comprises adding a chemical compound of copper to the liquid phase, and the liquid phase additionally contains propionic acid and glyoxal
WO2015197425A1 (en) * 2014-06-23 2015-12-30 Basf Se Device for dispensing drops of a monomer solution into a reactor
JP6497454B2 (en) * 2018-01-12 2019-04-10 三菱ケミカル株式会社 Method for producing butyl acrylate
EP3826987A1 (en) 2018-07-26 2021-06-02 Basf Se Method for inhibiting unwanted radical polymerisation of acrylic acid present in a liquid phase p
JP2023519280A (en) 2020-03-26 2023-05-10 ベーアーエスエフ・エスエー Method for Suppressing Undesired Free Radical Polymerization of Acrylic Acid Present in Liquid Phase P

Family Cites Families (4)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
US3405172A (en) * 1962-12-19 1968-10-08 Distillers Co Yeast Ltd Preparation of acrylic acid with the prevention of formation of acrylic polymers
JPS57144237A (en) * 1981-03-04 1982-09-06 Japan Synthetic Rubber Co Ltd Preparation of methacrylic acid
US4554054A (en) * 1983-12-09 1985-11-19 Rohm And Haas Company Methacrylic acid separation
CA1316545C (en) * 1987-06-27 1993-04-20 Morimasa Kuragano Quenching process of reaction product gas containing methacrylic acid and treatment method of quenched liquid

Also Published As

Publication number Publication date
JP5021116B2 (en) 2012-09-05
JP2002509905A (en) 2002-04-02
DE59905752D1 (en) 2003-07-03
CN1296470A (en) 2001-05-23
DE19814421A1 (en) 1999-10-07
WO1999050222A1 (en) 1999-10-07
BR9909312B1 (en) 2011-05-31
CN1137079C (en) 2004-02-04
EP1068174B1 (en) 2003-05-28
EP1068174A1 (en) 2001-01-17
BR9909312A (en) 2000-11-21

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