MX364711B - Recuperacion de plomo de un material oxidado mixto. - Google Patents
Recuperacion de plomo de un material oxidado mixto.Info
- Publication number
- MX364711B MX364711B MX2014009406A MX2014009406A MX364711B MX 364711 B MX364711 B MX 364711B MX 2014009406 A MX2014009406 A MX 2014009406A MX 2014009406 A MX2014009406 A MX 2014009406A MX 364711 B MX364711 B MX 364711B
- Authority
- MX
- Mexico
- Prior art keywords
- lead
- mixed oxidized
- mixed
- oxidized material
- recovering lead
- Prior art date
Links
- 239000000463 material Substances 0.000 title abstract 5
- AFVFQIVMOAPDHO-UHFFFAOYSA-N Methanesulfonic acid Chemical compound CS(O)(=O)=O AFVFQIVMOAPDHO-UHFFFAOYSA-N 0.000 abstract 4
- 239000007788 liquid Substances 0.000 abstract 3
- 229940098779 methanesulfonic acid Drugs 0.000 abstract 2
- MFEVGQHCNVXMER-UHFFFAOYSA-L 1,3,2$l^{2}-dioxaplumbetan-4-one Chemical compound [Pb+2].[O-]C([O-])=O MFEVGQHCNVXMER-UHFFFAOYSA-L 0.000 abstract 1
- 229910000003 Lead carbonate Inorganic materials 0.000 abstract 1
- 239000002253 acid Substances 0.000 abstract 1
- 238000005868 electrolysis reaction Methods 0.000 abstract 1
- 238000002386 leaching Methods 0.000 abstract 1
- 229910000464 lead oxide Inorganic materials 0.000 abstract 1
- LLABTCPIBSAMGS-UHFFFAOYSA-L lead(2+);methanesulfonate Chemical class [Pb+2].CS([O-])(=O)=O.CS([O-])(=O)=O LLABTCPIBSAMGS-UHFFFAOYSA-L 0.000 abstract 1
- 238000000034 method Methods 0.000 abstract 1
- YEXPOXQUZXUXJW-UHFFFAOYSA-N oxolead Chemical compound [Pb]=O YEXPOXQUZXUXJW-UHFFFAOYSA-N 0.000 abstract 1
Classifications
-
- C—CHEMISTRY; METALLURGY
- C25—ELECTROLYTIC OR ELECTROPHORETIC PROCESSES; APPARATUS THEREFOR
- C25C—PROCESSES FOR THE ELECTROLYTIC PRODUCTION, RECOVERY OR REFINING OF METALS; APPARATUS THEREFOR
- C25C1/00—Electrolytic production, recovery or refining of metals by electrolysis of solutions
- C25C1/18—Electrolytic production, recovery or refining of metals by electrolysis of solutions of lead
-
- C—CHEMISTRY; METALLURGY
- C22—METALLURGY; FERROUS OR NON-FERROUS ALLOYS; TREATMENT OF ALLOYS OR NON-FERROUS METALS
- C22B—PRODUCTION AND REFINING OF METALS; PRETREATMENT OF RAW MATERIALS
- C22B13/00—Obtaining lead
- C22B13/04—Obtaining lead by wet processes
-
- C—CHEMISTRY; METALLURGY
- C22—METALLURGY; FERROUS OR NON-FERROUS ALLOYS; TREATMENT OF ALLOYS OR NON-FERROUS METALS
- C22B—PRODUCTION AND REFINING OF METALS; PRETREATMENT OF RAW MATERIALS
- C22B13/00—Obtaining lead
- C22B13/04—Obtaining lead by wet processes
- C22B13/045—Recovery from waste materials
-
- Y—GENERAL TAGGING OF NEW TECHNOLOGICAL DEVELOPMENTS; GENERAL TAGGING OF CROSS-SECTIONAL TECHNOLOGIES SPANNING OVER SEVERAL SECTIONS OF THE IPC; TECHNICAL SUBJECTS COVERED BY FORMER USPC CROSS-REFERENCE ART COLLECTIONS [XRACs] AND DIGESTS
- Y02—TECHNOLOGIES OR APPLICATIONS FOR MITIGATION OR ADAPTATION AGAINST CLIMATE CHANGE
- Y02P—CLIMATE CHANGE MITIGATION TECHNOLOGIES IN THE PRODUCTION OR PROCESSING OF GOODS
- Y02P10/00—Technologies related to metal processing
- Y02P10/20—Recycling
Landscapes
- Chemical & Material Sciences (AREA)
- Engineering & Computer Science (AREA)
- Materials Engineering (AREA)
- Metallurgy (AREA)
- Organic Chemistry (AREA)
- Manufacturing & Machinery (AREA)
- Mechanical Engineering (AREA)
- Chemical Kinetics & Catalysis (AREA)
- Electrochemistry (AREA)
- Manufacture And Refinement Of Metals (AREA)
- Electrolytic Production Of Metals (AREA)
Abstract
En un ejemplo de un método para la recuperación de plomo de un material de plomo oxidado mixto, se selecciona ácido metano sulfónico como un ácido de lixiviación para el material de plomo oxidado mixto. Se expone el material de plomo oxidado mixto a una solución que incluye el ácido metano sulfónico, que produce la lixiviación del plomo de cualquiera de un óxido de plomo o un carbonato de plomo en el material de plomo oxidado mixto y genera un lixiviado líquido que incluye una sal de sulfonato de metano-plomo; Se purifica el lixiviado líquido y se recupera el plomo del lixiviado líquido purificado utilizando electrólisis.
Applications Claiming Priority (2)
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| US201261725824P | 2012-11-13 | 2012-11-13 | |
| PCT/IB2013/002540 WO2014076547A1 (en) | 2012-11-13 | 2013-11-13 | Recovering lead from a mixed oxidized material |
Publications (2)
| Publication Number | Publication Date |
|---|---|
| MX2014009406A MX2014009406A (es) | 2014-11-10 |
| MX364711B true MX364711B (es) | 2019-05-06 |
Family
ID=49880838
Family Applications (1)
| Application Number | Title | Priority Date | Filing Date |
|---|---|---|---|
| MX2014009406A MX364711B (es) | 2012-11-13 | 2013-11-13 | Recuperacion de plomo de un material oxidado mixto. |
Country Status (12)
| Country | Link |
|---|---|
| US (1) | US9322104B2 (es) |
| EP (1) | EP2920330B1 (es) |
| JP (1) | JP6356137B2 (es) |
| CN (1) | CN104039991B (es) |
| AU (1) | AU2013346480B2 (es) |
| CA (1) | CA2860614C (es) |
| ES (1) | ES2657632T3 (es) |
| MX (1) | MX364711B (es) |
| PL (1) | PL2920330T3 (es) |
| PT (1) | PT2920330T (es) |
| RS (1) | RS56991B1 (es) |
| WO (1) | WO2014076547A1 (es) |
Families Citing this family (19)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| SMT201900214T1 (it) | 2013-11-19 | 2019-05-10 | Aqua Metals Inc | Dispositivi e metodi per il riciclaggio senza fonderia di batterie al piombo acido |
| AU2015350562B2 (en) * | 2013-11-19 | 2018-07-26 | Aqua Metals Inc. | Improved devices and method for smelterless recycling of lead acid batteries |
| US9670565B2 (en) | 2014-06-20 | 2017-06-06 | Johnson Controls Technology Company | Systems and methods for the hydrometallurgical recovery of lead from spent lead-acid batteries and the preparation of lead oxide for use in new lead-acid batteries |
| US9708689B2 (en) * | 2015-04-08 | 2017-07-18 | Honeywell International Inc. | Isotope displacement refining process for producing low alpha materials |
| EP3294931A4 (en) * | 2015-05-13 | 2018-12-26 | Aqua Metals Inc. | Electrodeposited lead composition, methods of production, and uses |
| MX387016B (es) | 2015-05-13 | 2025-03-19 | Aqua Metals Inc | Sistemas y metodos para la recuperacion de plomo de baterias de plomo-acido. |
| PE20180151A1 (es) | 2015-05-13 | 2018-01-18 | Aqua Metals Inc | Sistemas y metodos de bucle cerrado para reciclado de baterias de plomo acido |
| CN106676578B (zh) * | 2015-11-11 | 2018-09-28 | 沈阳有色金属研究院 | 一种锌电积新型高效联合添加剂 |
| US10316420B2 (en) | 2015-12-02 | 2019-06-11 | Aqua Metals Inc. | Systems and methods for continuous alkaline lead acid battery recycling |
| CN106498446A (zh) * | 2016-10-20 | 2017-03-15 | 北京矿冶研究总院 | 一种硫酸铅悬浮电解的方法 |
| CN106756008B (zh) * | 2017-02-22 | 2018-08-14 | 中南大学 | 磺酸溶液两段逆流常压氧化浸出硫化铅精矿中铅的方法 |
| CN107227408B (zh) * | 2017-04-28 | 2019-01-04 | 昆明理工大学 | 一种硅质硫化铅精矿的低温常压快速浸出方法 |
| US12077834B2 (en) | 2018-02-28 | 2024-09-03 | Arizona Board Of Regents On Behalf Of The University Of Arizona | Efficient copper leaching using alkanesulfonic acids |
| CN108754137A (zh) * | 2018-08-02 | 2018-11-06 | 桐乡市思远环保科技有限公司 | 采用溶剂萃取电积工艺生产金属铅的方法 |
| CN109097575B (zh) * | 2018-09-10 | 2020-06-05 | 中国恩菲工程技术有限公司 | 低品位铅锌矿中锌元素的提取方法 |
| CN110453077A (zh) * | 2019-08-26 | 2019-11-15 | 湘潭大学 | 一种废铅膏回收利用的方法 |
| CN113832344B (zh) * | 2020-06-08 | 2022-06-14 | 中南大学 | 一种从铜钴渣中回收铜、钴的方法 |
| CN111926187A (zh) * | 2020-08-19 | 2020-11-13 | 楚雄滇中有色金属有限责任公司 | 一种从酸泥中综合回收硒、汞、铅和银的方法 |
| CN114480862B (zh) * | 2022-01-25 | 2024-01-30 | 长沙有色冶金设计研究院有限公司 | 一种从铜浮渣中回收有价元素的方法 |
Family Cites Families (28)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| US1752356A (en) * | 1927-01-14 | 1930-04-01 | Primos Lead Company | Process for reclaiming battery-plate material |
| US2525942A (en) * | 1945-06-29 | 1950-10-17 | Standard Oil Co | Electrodepositing bath and process |
| US3929597A (en) * | 1974-05-17 | 1975-12-30 | Hecla Mining Co | Production of lead and silver from their sulfides |
| FI61721C (fi) * | 1976-03-25 | 1982-09-10 | Lyijyvalkoistehd Groenberg Bly | Saett att aotervinna bly av blyavfall |
| JPS5411829A (en) * | 1977-06-30 | 1979-01-29 | Sumikou Ai Esu Pii Kk | Electolytical refining of lead |
| JPS5493626A (en) * | 1978-01-06 | 1979-07-24 | Diamond Eng Co Ltd | Method of regenerating and recovering lead from leaddsulfateecontaining waste product |
| US4181588A (en) * | 1979-01-04 | 1980-01-01 | The United States Of America As Represented By The Secretary Of The Interior | Method of recovering lead through the direct reduction of lead chloride by aqueous electrolysis |
| US4272341A (en) * | 1980-01-09 | 1981-06-09 | Duval Corporation | Process for recovery of metal values from lead-zinc ores, even those having a high carbonate content |
| IT1188203B (it) * | 1985-11-19 | 1988-01-07 | Tecneco Spa | Processo idrometallurgico per ricuperare in forma metallica pura il piombo contenuto nella massa attiva delle batterie esauste |
| IT1191650B (it) * | 1986-01-09 | 1988-03-23 | Tecneco Spa | Processo idrometallurgico per un recupero complessivo dei componenti delle batterie acide al piombo esauste |
| US4650553A (en) * | 1986-03-21 | 1987-03-17 | Pennwalt Corporation | Electrolytic recovery of lead from scrap |
| IT1223314B (it) * | 1987-10-20 | 1990-09-19 | Engitec Impianti | Processo idrometallurgico per recuperare in forma metallica pura tutto il piombo contenuto nella massa attiva delle batterie esauste |
| US4944851A (en) * | 1989-06-05 | 1990-07-31 | Macdermid, Incorporated | Electrolytic method for regenerating tin or tin-lead alloy stripping compositions |
| US5262020A (en) * | 1991-03-13 | 1993-11-16 | M.A. Industries, Inc. | Hydrometallurgical method of producing metallic lead from materials containing oxides, particularly from the active material of accumulators |
| IT1245449B (it) * | 1991-03-13 | 1994-09-20 | Ginatta Spa | Procedimento idrometallurgico per la produzione del piombo sotto forma di metallo da materiali contenenti ossidi, particolarmete dalla materia attiva degli accumulatori |
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| US5762683A (en) * | 1994-12-09 | 1998-06-09 | Asarco Incorporated | Ferric fluoborate/organic extractant hydrometallurgical process for recovering metals |
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| US6428676B1 (en) * | 2000-11-08 | 2002-08-06 | Enthone Inc. | Process for producing low alpha lead methane sulfonate |
| US7368043B2 (en) | 2003-04-10 | 2008-05-06 | Applied Intellectual Capital | Configurations and methods of electrochemical lead recovery from contaminated soil |
| EP1994189B1 (de) | 2006-03-01 | 2014-02-12 | Basf Se | Verfahren zum sauren aufschluss von metallhaltigen verbindungen |
| ITVA20070007A1 (it) * | 2007-01-17 | 2008-07-18 | Millbrook Lead Recycling Techn | Recupero del piombo sottoforma di carbonato ad altissima purezza da pastello di recupero dalla frantumazione di accumulatori al piombo esausti |
| JP4798469B2 (ja) * | 2009-03-23 | 2011-10-19 | Ｊｘ日鉱日石金属株式会社 | 鉛の炭酸化方法 |
| JP2012072480A (ja) | 2010-09-27 | 2012-04-12 | Jx Nippon Mining & Metals Corp | ＩｎとＳｎの混合物からのＩｎの選択的回収方法 |
| CA2869431A1 (en) * | 2012-04-06 | 2013-10-10 | Entegris, Inc. | Removal of lead from solid materials |
-
2013
- 2013-11-11 US US14/076,564 patent/US9322104B2/en active Active
- 2013-11-13 WO PCT/IB2013/002540 patent/WO2014076547A1/en active Application Filing
- 2013-11-13 RS RS20180089A patent/RS56991B1/sr unknown
- 2013-11-13 PL PL13812067T patent/PL2920330T3/pl unknown
- 2013-11-13 MX MX2014009406A patent/MX364711B/es active IP Right Grant
- 2013-11-13 EP EP13812067.0A patent/EP2920330B1/en active Active
- 2013-11-13 ES ES13812067.0T patent/ES2657632T3/es active Active
- 2013-11-13 PT PT138120670T patent/PT2920330T/pt unknown
- 2013-11-13 CN CN201380004685.0A patent/CN104039991B/zh active Active
- 2013-11-13 JP JP2015541251A patent/JP6356137B2/ja not_active Expired - Fee Related
- 2013-11-13 CA CA2860614A patent/CA2860614C/en active Active
- 2013-11-13 AU AU2013346480A patent/AU2013346480B2/en active Active
Also Published As
| Publication number | Publication date |
|---|---|
| CA2860614A1 (en) | 2014-05-22 |
| MX2014009406A (es) | 2014-11-10 |
| US20140131219A1 (en) | 2014-05-15 |
| CN104039991B (zh) | 2018-03-27 |
| JP6356137B2 (ja) | 2018-07-11 |
| EP2920330B1 (en) | 2017-11-01 |
| PT2920330T (pt) | 2018-01-29 |
| RS56991B1 (sr) | 2018-05-31 |
| US9322104B2 (en) | 2016-04-26 |
| AU2013346480B2 (en) | 2017-08-31 |
| AU2013346480A1 (en) | 2014-07-24 |
| JP2016502602A (ja) | 2016-01-28 |
| PL2920330T3 (pl) | 2018-05-30 |
| WO2014076547A1 (en) | 2014-05-22 |
| CA2860614C (en) | 2020-10-27 |
| ES2657632T3 (es) | 2018-03-06 |
| EP2920330A1 (en) | 2015-09-23 |
| CN104039991A (zh) | 2014-09-10 |
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Legal Events
| Date | Code | Title | Description |
|---|---|---|---|
| FG | Grant or registration |