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MX2012000556A - Metodo para la separacion de acetonitrilo a partir de agua. - Google Patents

Metodo para la separacion de acetonitrilo a partir de agua.

Info

Publication number
MX2012000556A
MX2012000556A MX2012000556A MX2012000556A MX2012000556A MX 2012000556 A MX2012000556 A MX 2012000556A MX 2012000556 A MX2012000556 A MX 2012000556A MX 2012000556 A MX2012000556 A MX 2012000556A MX 2012000556 A MX2012000556 A MX 2012000556A
Authority
MX
Mexico
Prior art keywords
acetonitrile
water
stream
weight ratio
separation
Prior art date
Application number
MX2012000556A
Other languages
English (en)
Inventor
Peter Bassler
Joaquim Henrique Teles
Ulrich Mueller
Hans-Georg Goebbel
Meinolf Weidenbach
Natalia Trukhan
Philip Kampe
Kai Gumlich
Christian Bartosch
Richard Jacubinas
Martin Cogswell
Original Assignee
Basf Se
Priority date (The priority date is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the date listed.)
Filing date
Publication date
Application filed by Basf Se filed Critical Basf Se
Publication of MX2012000556A publication Critical patent/MX2012000556A/es

Links

Classifications

    • B—PERFORMING OPERATIONS; TRANSPORTING
    • B01—PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
    • B01D—SEPARATION
    • B01D17/00—Separation of liquids, not provided for elsewhere, e.g. by thermal diffusion
    • B01D17/02—Separation of non-miscible liquids
    • B01D17/04—Breaking emulsions
    • B01D17/047—Breaking emulsions with separation aids
    • B—PERFORMING OPERATIONS; TRANSPORTING
    • B01—PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
    • B01D—SEPARATION
    • B01D17/00—Separation of liquids, not provided for elsewhere, e.g. by thermal diffusion
    • B01D17/02—Separation of non-miscible liquids
    • B01D17/0208—Separation of non-miscible liquids by sedimentation
    • B—PERFORMING OPERATIONS; TRANSPORTING
    • B01—PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
    • B01D—SEPARATION
    • B01D3/00—Distillation or related exchange processes in which liquids are contacted with gaseous media, e.g. stripping
    • B01D3/34—Distillation or related exchange processes in which liquids are contacted with gaseous media, e.g. stripping with one or more auxiliary substances
    • C—CHEMISTRY; METALLURGY
    • C07—ORGANIC CHEMISTRY
    • C07C—ACYCLIC OR CARBOCYCLIC COMPOUNDS
    • C07C253/00—Preparation of carboxylic acid nitriles
    • C07C253/32—Separation; Purification; Stabilisation; Use of additives
    • C07C253/34—Separation; Purification
    • C—CHEMISTRY; METALLURGY
    • C07—ORGANIC CHEMISTRY
    • C07C—ACYCLIC OR CARBOCYCLIC COMPOUNDS
    • C07C7/00—Purification; Separation; Use of additives
    • C07C7/20—Use of additives, e.g. for stabilisation
    • C—CHEMISTRY; METALLURGY
    • C07—ORGANIC CHEMISTRY
    • C07D—HETEROCYCLIC COMPOUNDS
    • C07D301/00—Preparation of oxiranes
    • C07D301/02—Synthesis of the oxirane ring
    • C07D301/03—Synthesis of the oxirane ring by oxidation of unsaturated compounds, or of mixtures of unsaturated and saturated compounds
    • C07D301/12—Synthesis of the oxirane ring by oxidation of unsaturated compounds, or of mixtures of unsaturated and saturated compounds with hydrogen peroxide or inorganic peroxides or peracids
    • Y—GENERAL TAGGING OF NEW TECHNOLOGICAL DEVELOPMENTS; GENERAL TAGGING OF CROSS-SECTIONAL TECHNOLOGIES SPANNING OVER SEVERAL SECTIONS OF THE IPC; TECHNICAL SUBJECTS COVERED BY FORMER USPC CROSS-REFERENCE ART COLLECTIONS [XRACs] AND DIGESTS
    • Y02—TECHNOLOGIES OR APPLICATIONS FOR MITIGATION OR ADAPTATION AGAINST CLIMATE CHANGE
    • Y02P—CLIMATE CHANGE MITIGATION TECHNOLOGIES IN THE PRODUCTION OR PROCESSING OF GOODS
    • Y02P20/00—Technologies relating to chemical industry
    • Y02P20/50—Improvements relating to the production of bulk chemicals
    • Y02P20/582—Recycling of unreacted starting or intermediate materials

Landscapes

  • Chemical & Material Sciences (AREA)
  • Organic Chemistry (AREA)
  • Chemical Kinetics & Catalysis (AREA)
  • Physics & Mathematics (AREA)
  • Thermal Sciences (AREA)
  • Inorganic Chemistry (AREA)
  • Engineering & Computer Science (AREA)
  • Analytical Chemistry (AREA)
  • Oil, Petroleum & Natural Gas (AREA)
  • Water Supply & Treatment (AREA)
  • Epoxy Compounds (AREA)
  • Organic Low-Molecular-Weight Compounds And Preparation Thereof (AREA)

Abstract

Se describe un método para separar acetonitrilo a partir de agua, el cual consiste en: i) disponer de una corriente Si que contenga al menos 95% en peso, con base en el peso total de S1, de acetonitrilo y agua, en donde la relación en peso de acetonitriio:agua sea mayor que 1; ii) adicionar una corriente P que contenga al menos 95% en peso de C3, con base en el peso total de la corriente P, a S1 para obtener una corriente mixta S2, siendo C3 propeno opcionalmente mezclado con propano, con una relación en peso mínima de propeno:propano de 7:3; iii) someter la corriente S2 a una temperatura de 92°C a lo sumo y una presión de al menos 10 bar, obteniéndose una primera fase líquida Li consistente principalmente en C3, acetonitrilo y agua, y una segunda fase líquida I2 [sic] consistente principalmente en agua y acetonitrilo, en donde la relación en peso de acetonitrilo:agua en L2 es menor que 1; iv) separar L1 de L2.
MX2012000556A 2009-07-16 2010-07-16 Metodo para la separacion de acetonitrilo a partir de agua. MX2012000556A (es)

Applications Claiming Priority (2)

Application Number Priority Date Filing Date Title
US22611609P 2009-07-16 2009-07-16
PCT/EP2010/060310 WO2011006990A1 (en) 2009-07-16 2010-07-16 Method for the separation of acetonitrile from water

Publications (1)

Publication Number Publication Date
MX2012000556A true MX2012000556A (es) 2012-04-11

Family

ID=42734794

Family Applications (1)

Application Number Title Priority Date Filing Date
MX2012000556A MX2012000556A (es) 2009-07-16 2010-07-16 Metodo para la separacion de acetonitrilo a partir de agua.

Country Status (12)

Country Link
US (1) US8609879B2 (es)
EP (1) EP2454245B1 (es)
KR (1) KR101802535B1 (es)
CN (1) CN102482241B (es)
BR (1) BR112012001033B8 (es)
ES (1) ES2522929T3 (es)
MX (1) MX2012000556A (es)
MY (1) MY156574A (es)
RU (1) RU2537296C2 (es)
SG (1) SG178027A1 (es)
WO (1) WO2011006990A1 (es)
ZA (1) ZA201201064B (es)

Families Citing this family (10)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
US8993819B2 (en) 2011-07-12 2015-03-31 Basf Se Process for preparing cycloheptene
US9329159B2 (en) * 2013-03-08 2016-05-03 Ecolab Usa Inc. Methods and systems for analyzing a liquid medium
ES2662584T3 (es) * 2013-04-29 2018-04-09 Basf Se Destilación de corriente parcial
US9725428B2 (en) 2013-07-24 2017-08-08 Basf Se Process for preparing propylene oxide
EP3024578B1 (en) 2013-07-24 2018-05-30 Basf Se A process for preparing propylene oxide
KR102302531B1 (ko) 2013-07-24 2021-09-16 바스프 에스이 프로필렌 옥사이드의 제조 방법
WO2016066629A1 (en) 2014-10-27 2016-05-06 Basf Se Part-stream distillation
RU2734823C2 (ru) 2016-02-17 2020-10-23 Басф Се Способ получения пропиленоксида
KR102451361B1 (ko) 2016-07-20 2022-10-05 바스프 에스이 프로필렌 옥사이드의 정제 방법
CN108212206B (zh) * 2017-12-29 2021-01-05 中触媒新材料股份有限公司 一种磁性复合Ti-MWW分子筛微球催化剂制备方法

Family Cites Families (13)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
DE3936854A1 (de) 1989-11-06 1991-05-08 Basf Ag Verfahren zur herstellung von methylformiat
BE1011456A3 (fr) 1997-09-18 1999-09-07 Solvay Procede de fabrication d'un oxiranne.
EP1122246A1 (de) 2000-02-07 2001-08-08 Degussa AG Verfahren zur Epoxidierung von Olefinen
DE10105528A1 (de) 2001-02-07 2002-08-08 Basf Ag Verfahren zur Online-Bestimmung von Wasserstoffperoxid
DE10105527A1 (de) 2001-02-07 2002-08-08 Basf Ag Verfahren zur Herstellung eines Epoxids
WO2004058737A1 (ja) 2002-12-24 2004-07-15 Showa Denko K.K. 炭素−炭素二重結合の酸化方法および酸化化合物の製造方法
US7531674B2 (en) 2003-03-06 2009-05-12 Sumitomo Chemical Company, Limited Process for producing propylene oxide
DE10320635A1 (de) 2003-05-08 2004-11-18 Basf Ag Verfahren zur Herstellung von Propylenoxid
EP1682492A2 (en) 2003-11-04 2006-07-26 Lonza Ag Acetonitrile recycling process
US20070004926A1 (en) 2005-06-29 2007-01-04 Basf Aktiengesellschaft Process for producing propylene oxide
KR20090011002A (ko) 2006-04-27 2009-01-30 스미또모 가가꾸 가부시끼가이샤 프로필렌옥사이드의 제조 방법
EP2173731B1 (en) * 2007-07-10 2011-10-26 Sumitomo Chemical Company, Limited Method for producing propylene oxide
CN101397283B (zh) 2007-09-28 2011-04-20 中国石油化工股份有限公司 一种催化丙烯环氧化生产环氧丙烷的方法

Also Published As

Publication number Publication date
ES2522929T3 (es) 2014-11-19
WO2011006990A1 (en) 2011-01-20
BR112012001033B8 (pt) 2021-03-23
EP2454245B1 (en) 2014-09-10
SG178027A1 (en) 2012-03-29
BR112012001033A2 (pt) 2020-07-28
ZA201201064B (en) 2013-05-29
US20110065939A1 (en) 2011-03-17
MY156574A (en) 2016-03-15
RU2537296C2 (ru) 2014-12-27
RU2012105120A (ru) 2013-08-27
CN102482241A (zh) 2012-05-30
KR101802535B1 (ko) 2017-11-28
EP2454245A1 (en) 2012-05-23
BR112012001033B1 (pt) 2021-02-09
KR20120050452A (ko) 2012-05-18
US8609879B2 (en) 2013-12-17
CN102482241B (zh) 2014-06-18

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