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KR950008490A - 히드록시옥사알킬멜라민류의 제조방법 - Google Patents

히드록시옥사알킬멜라민류의 제조방법 Download PDF

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Publication number
KR950008490A
KR950008490A KR1019940023302A KR19940023302A KR950008490A KR 950008490 A KR950008490 A KR 950008490A KR 1019940023302 A KR1019940023302 A KR 1019940023302A KR 19940023302 A KR19940023302 A KR 19940023302A KR 950008490 A KR950008490 A KR 950008490A
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KR
South Korea
Prior art keywords
mol
hydrogen
radicals
hydroxyoxaalkylmelamines
alkyl
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KR1019940023302A
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English (en)
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KR100346083B1 (ko
Inventor
귄터 에르하르트
로이터 볼프강
쉐르 귄터
딤러 만프레드
Original Assignee
랑핑어, 슈타인호프
바스프 악티엔게젤샤프트
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Publication of KR950008490A publication Critical patent/KR950008490A/ko
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Publication of KR100346083B1 publication Critical patent/KR100346083B1/ko

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    • C—CHEMISTRY; METALLURGY
    • C07—ORGANIC CHEMISTRY
    • C07D—HETEROCYCLIC COMPOUNDS
    • C07D251/00—Heterocyclic compounds containing 1,3,5-triazine rings
    • C07D251/02—Heterocyclic compounds containing 1,3,5-triazine rings not condensed with other rings
    • C07D251/12—Heterocyclic compounds containing 1,3,5-triazine rings not condensed with other rings having three double bonds between ring members or between ring members and non-ring members
    • C07D251/26—Heterocyclic compounds containing 1,3,5-triazine rings not condensed with other rings having three double bonds between ring members or between ring members and non-ring members with only hetero atoms directly attached to ring carbon atoms
    • C07D251/40—Nitrogen atoms
    • C07D251/54—Three nitrogen atoms
    • C07D251/56—Preparation of melamine
    • C—CHEMISTRY; METALLURGY
    • C07—ORGANIC CHEMISTRY
    • C07D—HETEROCYCLIC COMPOUNDS
    • C07D251/00—Heterocyclic compounds containing 1,3,5-triazine rings
    • C07D251/02—Heterocyclic compounds containing 1,3,5-triazine rings not condensed with other rings
    • C07D251/12—Heterocyclic compounds containing 1,3,5-triazine rings not condensed with other rings having three double bonds between ring members or between ring members and non-ring members
    • C07D251/26—Heterocyclic compounds containing 1,3,5-triazine rings not condensed with other rings having three double bonds between ring members or between ring members and non-ring members with only hetero atoms directly attached to ring carbon atoms
    • C07D251/40—Nitrogen atoms
    • C07D251/54—Three nitrogen atoms
    • C07D251/70—Other substituted melamines
    • B—PERFORMING OPERATIONS; TRANSPORTING
    • B01—PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
    • B01J—CHEMICAL OR PHYSICAL PROCESSES, e.g. CATALYSIS OR COLLOID CHEMISTRY; THEIR RELEVANT APPARATUS
    • B01J27/00—Catalysts comprising the elements or compounds of halogens, sulfur, selenium, tellurium, phosphorus or nitrogen; Catalysts comprising carbon compounds
    • B01J27/14—Phosphorus; Compounds thereof
    • B01J27/16—Phosphorus; Compounds thereof containing oxygen, i.e. acids, anhydrides and their derivates with N, S, B or halogens without carriers or on carriers based on C, Si, Al or Zr; also salts of Si, Al and Zr

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  • Chemical & Material Sciences (AREA)
  • Organic Chemistry (AREA)
  • Engineering & Computer Science (AREA)
  • Materials Engineering (AREA)
  • Chemical Kinetics & Catalysis (AREA)
  • Low-Molecular Organic Synthesis Reactions Using Catalysts (AREA)
  • Organic Low-Molecular-Weight Compounds And Preparation Thereof (AREA)
  • Phenolic Resins Or Amino Resins (AREA)
  • Pharmaceuticals Containing Other Organic And Inorganic Compounds (AREA)
  • Steroid Compounds (AREA)
  • Medicinal Preparation (AREA)
  • Catalysts (AREA)

Abstract

본 발명은, 120℃ 내지 250℃의 온도와 멜라민 1mol을 기초로 0.01 내지 0.15mol, 바람직하게는 0.02 내지 0.12mol, 가장 바람직하게는 0.03 내지 0.1mol의 농도인 산촉매의 존재하에서 멜라민을 다음의 일반식(Ⅲ)의 화합물과 함께 반응시켜서
[이때, R'은 같거나 다르고 수소 또는 C1-C4알킬이며 n은 2 또는 3이다] 다음 일반식(I)의 히드록시옥사알킬멜라민류를 제조하는 방법에 관한 것이다.
상기 식에서 R1은 다음 일반식(II)의 잔기를 나타내고,
여기에서 라디칼 R'은 동일하거나 상이한 것으로서 수소나 C1-C4알킬을 나타내고, n은 2 또는 3이고, 라디칼 R2와 R3는 라디칼 R1중의 하나 또는 수소를 나타낸 것에 관한 것이다.

Description

히드록시옥사알킬멜라민류의 제조방법
본 내용은 요부공개 건이므로 전문내용을 수록하지 않았음

Claims (4)

120℃ 내지 250℃의 온도와 멜라민 1mol을 기초로 0.01 내지 0.15mol, 바람직하게는 0.02 내지 0.12mol, 가장 바람직하게는 0.03 내지 0.1mol의 농도인 산촉매의 존재하에서 멜라민을 다음의 일반식(Ⅲ)의 화합물과 함께 반응시켜서
[이때, R'은 같거나 다르고 수소 또는 C1-C4알킬이며 n은 2 또는 3이다] 다음 일반식(I)의 히드록시옥사알킬멜라민류를 제조하는 방법;
상기 식에서 R1은 다음 일반식(II)의 잔기를 나타내고,
여기에서 라디칼 R'은 동일하거나 상이한 것으로서 수소나 C1-C4알킬을 나타내고, n은 2 또는 3이고, 라디칼 R2와 R3는 라디칼 R1중의 하나 또는 수소를 나타낸다.
제1항에 있어서, 사용된 산촉매가 단독상태나 다른 촉매와 결부된 상태의 염화암모늄인 것을 특징으로 하는 방법.
제1항 또는 제2항에 있어서, 사용된 산촉매가 단독상태나 다른 촉매와 결부된 상태의 하이포인산(H2PO2)인 것을 특징으로 하는 방법.
제1항 내지 제3항중의 어느 한 항에 있어서, R'이 수소이고 n이 2인 것을 특징으로 하는 방법.
※ 참고사항 : 최초출원 내용에 의하여 공개하는 것임.
KR1019940023302A 1993-09-15 1994-09-15 히드록시옥사알킬멜라민류의제조방법 KR100346083B1 (ko)

Applications Claiming Priority (2)

Application Number Priority Date Filing Date Title
DEP4331233.0 1993-09-15
DE4331233A DE4331233A1 (de) 1993-09-15 1993-09-15 Verfahren zur Herstellung von Hydroxyoxaalkylmelaminen

Publications (2)

Publication Number Publication Date
KR950008490A true KR950008490A (ko) 1995-04-17
KR100346083B1 KR100346083B1 (ko) 2002-11-13

Family

ID=6497718

Family Applications (1)

Application Number Title Priority Date Filing Date
KR1019940023302A KR100346083B1 (ko) 1993-09-15 1994-09-15 히드록시옥사알킬멜라민류의제조방법

Country Status (8)

Country Link
US (1) US5637704A (ko)
EP (1) EP0648756B1 (ko)
JP (1) JP3731909B2 (ko)
KR (1) KR100346083B1 (ko)
AT (1) ATE178057T1 (ko)
CA (1) CA2131474C (ko)
DE (2) DE4331233A1 (ko)
ES (1) ES2130320T3 (ko)

Families Citing this family (7)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
US6239276B1 (en) 1998-06-22 2001-05-29 Cytec Technology Corporation Non-yellowing para-tertiary-alkyl phenyl substituted triazine and pyrimidine ultraviolet light absorbers
US6867250B1 (en) 2000-10-30 2005-03-15 Cytec Technology Corp. Non-yellowing ortho-dialkyl aryl substituted triazine ultraviolet light absorbers
AR040209A1 (es) * 2002-06-14 2005-03-16 Agrolinz Melamin Gmbh Material de moldeo de amino resina para productos con flexibilidad mejorada y productos de amino resina con flexibilidad mejorada
EP1941946A1 (en) * 2007-01-04 2008-07-09 Max-Planck-Gesellschaft zur Förderung der Wissenschaften e.V. Carbonitrides as catalysts
CN102292097B (zh) * 2008-12-11 2015-05-27 艾克赛特药品有限公司 染料木黄酮的晶型
CN102746532B (zh) * 2012-05-25 2014-11-05 武汉工程大学 一种含氮磷的阻燃剂及其制备方法
CN102731424B (zh) * 2012-06-27 2015-03-04 四川金象赛瑞化工股份有限公司 一种三聚氰胺衍生物的制备方法

Family Cites Families (6)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
US4312988A (en) * 1980-11-10 1982-01-26 American Cyanamid Company Synthesis of hydroxy functional melamine derivatives
DE3422218A1 (de) * 1984-06-15 1985-12-19 Basf Ag, 6700 Ludwigshafen Verfahren zur herstellung von (2-hydroxyethyl)melaminen und ihre verwendung als modifizierungsmittel bei der herstellung von aminoplastharzen
DE3438387A1 (de) * 1984-10-19 1986-04-24 Basf Ag, 6700 Ludwigshafen Verfahren zur herstellung von n,n',n"-tris(2-hydroxypropyl)-melamin
DE3438694A1 (de) * 1984-10-23 1986-04-24 Basf Ag, 6700 Ludwigshafen Neue amidoalkylmelamine und aminoalkylmelamine und verfahren zu ihrer herstellung
DE3531912A1 (de) * 1985-09-07 1987-03-19 Basf Ag Hydroxyoxaalkylmelamine, verfahren zu ihrer herstellung und deren verwendung
DE3922733A1 (de) * 1989-07-11 1991-01-24 Basf Ag Formkoerper aus melaminharzen mit erhoehter elastizitaet

Also Published As

Publication number Publication date
EP0648756A1 (de) 1995-04-19
EP0648756B1 (de) 1999-03-24
US5637704A (en) 1997-06-10
ATE178057T1 (de) 1999-04-15
DE59407996D1 (de) 1999-04-29
KR100346083B1 (ko) 2002-11-13
JPH07149740A (ja) 1995-06-13
JP3731909B2 (ja) 2006-01-05
CA2131474C (en) 2006-02-07
CA2131474A1 (en) 1995-03-16
DE4331233A1 (de) 1995-03-16
ES2130320T3 (es) 1999-07-01

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