KR930021686A - 메틸클로로실란 잔류 폐기물로부터 얻은 실록산 유체 - Google Patents
메틸클로로실란 잔류 폐기물로부터 얻은 실록산 유체 Download PDFInfo
- Publication number
- KR930021686A KR930021686A KR1019930006047A KR930006047A KR930021686A KR 930021686 A KR930021686 A KR 930021686A KR 1019930006047 A KR1019930006047 A KR 1019930006047A KR 930006047 A KR930006047 A KR 930006047A KR 930021686 A KR930021686 A KR 930021686A
- Authority
- KR
- South Korea
- Prior art keywords
- silicone fluid
- polymer
- siloxane
- integer greater
- disiloxane
- Prior art date
- Legal status (The legal status is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the status listed.)
- Withdrawn
Links
- KPUWHANPEXNPJT-UHFFFAOYSA-N disiloxane Chemical class [SiH3]O[SiH3] KPUWHANPEXNPJT-UHFFFAOYSA-N 0.000 title claims abstract 14
- 239000012530 fluid Substances 0.000 title claims abstract 13
- YGZSVWMBUCGDCV-UHFFFAOYSA-N chloro(methyl)silane Chemical compound C[SiH2]Cl YGZSVWMBUCGDCV-UHFFFAOYSA-N 0.000 title claims abstract 3
- 239000002699 waste material Substances 0.000 title 1
- 229920000642 polymer Polymers 0.000 claims abstract 10
- 238000000034 method Methods 0.000 claims abstract 5
- PZPGRFITIJYNEJ-UHFFFAOYSA-N disilane Chemical compound [SiH3][SiH3] PZPGRFITIJYNEJ-UHFFFAOYSA-N 0.000 claims abstract 4
- 239000000203 mixture Substances 0.000 claims abstract 4
- -1 silylmethylenes Chemical class 0.000 claims abstract 4
- 238000003776 cleavage reaction Methods 0.000 claims abstract 2
- 229920001296 polysiloxane Polymers 0.000 claims 10
- 125000000217 alkyl group Chemical group 0.000 claims 3
- 230000003301 hydrolyzing effect Effects 0.000 claims 1
- 239000003607 modifier Substances 0.000 claims 1
- 150000004756 silanes Chemical class 0.000 claims 1
- 238000003786 synthesis reaction Methods 0.000 claims 1
- 239000004034 viscosity adjusting agent Substances 0.000 claims 1
- 238000011084 recovery Methods 0.000 abstract 1
- 230000007017 scission Effects 0.000 abstract 1
Classifications
-
- C—CHEMISTRY; METALLURGY
- C08—ORGANIC MACROMOLECULAR COMPOUNDS; THEIR PREPARATION OR CHEMICAL WORKING-UP; COMPOSITIONS BASED THEREON
- C08G—MACROMOLECULAR COMPOUNDS OBTAINED OTHERWISE THAN BY REACTIONS ONLY INVOLVING UNSATURATED CARBON-TO-CARBON BONDS
- C08G77/00—Macromolecular compounds obtained by reactions forming a linkage containing silicon with or without sulfur, nitrogen, oxygen or carbon in the main chain of the macromolecule
- C08G77/48—Macromolecular compounds obtained by reactions forming a linkage containing silicon with or without sulfur, nitrogen, oxygen or carbon in the main chain of the macromolecule in which at least two but not all the silicon atoms are connected by linkages other than oxygen atoms
- C08G77/50—Macromolecular compounds obtained by reactions forming a linkage containing silicon with or without sulfur, nitrogen, oxygen or carbon in the main chain of the macromolecule in which at least two but not all the silicon atoms are connected by linkages other than oxygen atoms by carbon linkages
-
- C—CHEMISTRY; METALLURGY
- C08—ORGANIC MACROMOLECULAR COMPOUNDS; THEIR PREPARATION OR CHEMICAL WORKING-UP; COMPOSITIONS BASED THEREON
- C08G—MACROMOLECULAR COMPOUNDS OBTAINED OTHERWISE THAN BY REACTIONS ONLY INVOLVING UNSATURATED CARBON-TO-CARBON BONDS
- C08G77/00—Macromolecular compounds obtained by reactions forming a linkage containing silicon with or without sulfur, nitrogen, oxygen or carbon in the main chain of the macromolecule
- C08G77/04—Polysiloxanes
- C08G77/06—Preparatory processes
-
- C—CHEMISTRY; METALLURGY
- C08—ORGANIC MACROMOLECULAR COMPOUNDS; THEIR PREPARATION OR CHEMICAL WORKING-UP; COMPOSITIONS BASED THEREON
- C08G—MACROMOLECULAR COMPOUNDS OBTAINED OTHERWISE THAN BY REACTIONS ONLY INVOLVING UNSATURATED CARBON-TO-CARBON BONDS
- C08G77/00—Macromolecular compounds obtained by reactions forming a linkage containing silicon with or without sulfur, nitrogen, oxygen or carbon in the main chain of the macromolecule
- C08G77/48—Macromolecular compounds obtained by reactions forming a linkage containing silicon with or without sulfur, nitrogen, oxygen or carbon in the main chain of the macromolecule in which at least two but not all the silicon atoms are connected by linkages other than oxygen atoms
-
- Y—GENERAL TAGGING OF NEW TECHNOLOGICAL DEVELOPMENTS; GENERAL TAGGING OF CROSS-SECTIONAL TECHNOLOGIES SPANNING OVER SEVERAL SECTIONS OF THE IPC; TECHNICAL SUBJECTS COVERED BY FORMER USPC CROSS-REFERENCE ART COLLECTIONS [XRACs] AND DIGESTS
- Y10—TECHNICAL SUBJECTS COVERED BY FORMER USPC
- Y10S—TECHNICAL SUBJECTS COVERED BY FORMER USPC CROSS-REFERENCE ART COLLECTIONS [XRACs] AND DIGESTS
- Y10S516/00—Colloid systems and wetting agents; subcombinations thereof; processes of
- Y10S516/01—Wetting, emulsifying, dispersing, or stabilizing agents
-
- Y—GENERAL TAGGING OF NEW TECHNOLOGICAL DEVELOPMENTS; GENERAL TAGGING OF CROSS-SECTIONAL TECHNOLOGIES SPANNING OVER SEVERAL SECTIONS OF THE IPC; TECHNICAL SUBJECTS COVERED BY FORMER USPC CROSS-REFERENCE ART COLLECTIONS [XRACs] AND DIGESTS
- Y10—TECHNICAL SUBJECTS COVERED BY FORMER USPC
- Y10S—TECHNICAL SUBJECTS COVERED BY FORMER USPC CROSS-REFERENCE ART COLLECTIONS [XRACs] AND DIGESTS
- Y10S516/00—Colloid systems and wetting agents; subcombinations thereof; processes of
- Y10S516/01—Wetting, emulsifying, dispersing, or stabilizing agents
- Y10S516/07—Organic amine, amide, or n-base containing
Landscapes
- Chemical & Material Sciences (AREA)
- Health & Medical Sciences (AREA)
- Chemical Kinetics & Catalysis (AREA)
- Medicinal Chemistry (AREA)
- Polymers & Plastics (AREA)
- Organic Chemistry (AREA)
- Silicon Polymers (AREA)
Abstract
본 발명은 디실란, 디실록산 및 실릴메틸렌의 혼합물로 부터 제조된 신규의 실록산 폴리머를 함유한 실록산 유체, 및 메틸클로로실란 잔류물 절단 하부 증류 물로부터 디실란, 디실록산 및 실릴메틸렌 결합을 가진 충분히 알칼화된 선형 및 고리형 실록산의 회수를 위한 방법에 관한 것이다.
Description
본 내용은 요부공개 건이므로 전문내용을 수록하지 않았음
Claims (11)
- 하기 일반식의 실록산 폴리머로 이루어진 실리콘 유체.식중, X는 알킬기 또는 실록산 분자를 나타내고, a는 0보다 큰 정수이고, b및 c는 0또는 0보다 큰 정수이고, 단 b 및 c가 둘 다 0은 아니며, a,b 및 c는 폴리머 골격중에서 무작위적으로 배열될 수 있다.
- 제1항에 있어서, 상기 실록산 폴리머가 선형 폴리머 또는 분지쇄 폴리머로 이루어진 실리콘 유체.
- 제1항에 있어서, 상기 실록산 폴리머가 약 5내지 약 100,000센티스토크의 점도를 갖는 실리콘 유체.
- 제1항에 있어서, X가 알킬기인 실리콘 유체.
- 제1항에 있어서, 좀도 조절제를 추가로 포함하는 실리콘 유체.
- 제5항에 있어서, 상기 점도 조절제가 단량체 유기 관능성 실란 중에서 선택되는 실리콘 유체.
- 제1항에 있어서, 약 70 내지 약 85중량%의 상기 실록산 폴리머로 이루어진 실리콘 유체.
- 디실란, 디실록산 및 실랄메틸렌의 혼합물을 가수분해시키는 것을 특징으로 하는 하기 일반식의 실록산 폴리머로 이루어진 실리콘 유체의 제조방법.식중, X는 알킬기 또는 실록산 분자를 나타내고, a는 0보다 큰 정수이고, b및 c는 0또는 0보다 큰 정수이고, 단 b 및 c가 둘 다 0은 아니며, a,b 및 c는 폴리머 골격중에서 무작위적으로 배열될 수 있다.
- 제8항에 있어서, 상기 디실란, 디실록산 및 실릴메틸렌의 혼합물이 메틸클로실란 합성 반응으로부터 유도되는 방법.
- 제8항에 있어서, 상기 디실란, 디실록산 및 실릴메틸렌의 혼합물이 메틸클로로실란 절단 반응의 하부 잔류물, 또는 하부 잔류물의 일부로부터 유도되는 방법.
- 제9항에 있어서, 실리콘 유체를 스트립시켜 스트립된 유체를 얻고, 휘발성 분획을 회수하는 것을 추가로 포함되는 방법.※ 참고사항 : 최초출원 내용에 의하여 공개하는 것임.
Applications Claiming Priority (2)
Application Number | Priority Date | Filing Date | Title |
---|---|---|---|
US07/867,938 | 1992-04-13 | ||
US07/867,938 US5312946A (en) | 1992-04-13 | 1992-04-13 | Siloxane fluid from methylchlorosilane residue waste |
Publications (1)
Publication Number | Publication Date |
---|---|
KR930021686A true KR930021686A (ko) | 1993-11-22 |
Family
ID=25350752
Family Applications (1)
Application Number | Title | Priority Date | Filing Date |
---|---|---|---|
KR1019930006047A Withdrawn KR930021686A (ko) | 1992-04-13 | 1993-04-12 | 메틸클로로실란 잔류 폐기물로부터 얻은 실록산 유체 |
Country Status (5)
Country | Link |
---|---|
US (2) | US5312946A (ko) |
EP (1) | EP0566311A3 (ko) |
JP (1) | JPH0616815A (ko) |
KR (1) | KR930021686A (ko) |
AU (1) | AU3677293A (ko) |
Families Citing this family (22)
Publication number | Priority date | Publication date | Assignee | Title |
---|---|---|---|---|
JPH0841206A (ja) * | 1994-07-26 | 1996-02-13 | Toray Dow Corning Silicone Co Ltd | 有機ケイ素重合体およびその製造方法 |
AU6559996A (en) * | 1996-09-13 | 1998-03-19 | Huntsman, Peter Harold | Process for the recovery of methyl polysiloxanes in the form of methyl cyclosiloxanes |
US6228289B1 (en) * | 1998-09-25 | 2001-05-08 | Q2100, Inc. | Plastic lens systems and methods |
KR101271662B1 (ko) * | 2005-02-16 | 2013-06-05 | 다우 코닝 도레이 캄파니 리미티드 | 강화 실리콘 수지 필름 및 이의 제조방법 |
US8092910B2 (en) * | 2005-02-16 | 2012-01-10 | Dow Corning Toray Co., Ltd. | Reinforced silicone resin film and method of preparing same |
WO2007018756A1 (en) * | 2005-08-04 | 2007-02-15 | Dow Corning Corporation | Reinforced silicone resin film and method of preparing same |
US8912268B2 (en) * | 2005-12-21 | 2014-12-16 | Dow Corning Corporation | Silicone resin film, method of preparing same, and nanomaterial-filled silicone composition |
KR101426316B1 (ko) * | 2006-01-19 | 2014-08-06 | 다우 코닝 코포레이션 | 실리콘 수지 필름, 이의 제조방법, 및 나노물질로 충전된실리콘 조성물 |
KR20080094783A (ko) * | 2006-02-02 | 2008-10-24 | 다우 코닝 코포레이션 | 실리콘 수지 필름, 이의 제조방법 및 나노 물질-충전된실리콘 조성물 |
WO2007097835A2 (en) * | 2006-02-20 | 2007-08-30 | Dow Corning Corporation | Silicone resin film, method of preparing same, and nanomaterial-filled silicone composition |
WO2009113971A1 (en) * | 2006-07-27 | 2009-09-17 | Dow Corning Corporation | Method of preparing a silicone resin |
CN103319718A (zh) | 2006-07-27 | 2013-09-25 | 陶氏康宁公司 | 硅氧烷树脂、硅氧烷组合物和涂布的基底 |
CN101522838B (zh) * | 2006-10-05 | 2012-07-04 | 陶氏康宁公司 | 有机硅树脂膜及其制备方法 |
CN101595166A (zh) * | 2007-02-06 | 2009-12-02 | 陶氏康宁公司 | 有机硅树脂、有机硅组合物、涂覆基材和增强有机硅树脂膜 |
US8283025B2 (en) * | 2007-02-22 | 2012-10-09 | Dow Corning Corporation | Reinforced silicone resin films |
US20100087581A1 (en) * | 2007-02-22 | 2010-04-08 | Mark Fisher | Reinforced Silicone Resin Film and Method of Preparing Same |
CN101636270B (zh) * | 2007-02-22 | 2012-07-04 | 道康宁公司 | 增强硅树脂膜 |
US20100129625A1 (en) * | 2007-05-01 | 2010-05-27 | Bizhong Zhu | Reinforced Silicone Resin Film |
KR20100017500A (ko) * | 2007-05-01 | 2010-02-16 | 다우 코닝 코포레이션 | 나노물질-충전된 실리콘 조성물 및 강화 실리콘 수지 필름 |
WO2009048694A1 (en) * | 2007-10-12 | 2009-04-16 | Dow Corning Corporation | Reinforced silicone resin film and nanofiber-filled silicone composition |
TW201245289A (en) * | 2011-03-11 | 2012-11-16 | Dow Corning | Polysilanesiloxane copolymers and method of converting to silicon dioxide |
CN107652317B (zh) * | 2017-10-30 | 2020-10-30 | 山东大学 | 一种由硅橡胶系列物质裂解反应制取ɑ,ω‐二氯封端硅氧烷的方法 |
Family Cites Families (14)
Publication number | Priority date | Publication date | Assignee | Title |
---|---|---|---|---|
US2380995A (en) * | 1941-09-26 | 1945-08-07 | Gen Electric | Preparation of organosilicon halides |
US2383818A (en) * | 1943-07-26 | 1945-08-28 | Gen Electric | Preparation of organosilicon halides |
US2575141A (en) * | 1948-10-26 | 1951-11-13 | Gen Electric | Surfaces having low adhesion to ice |
GB736971A (en) * | 1952-08-18 | 1955-09-14 | Rhone Poulenc Sa | New organosilicon resins and their preparation |
BE536407A (ko) * | 1954-03-12 | |||
US3336352A (en) * | 1963-04-29 | 1967-08-15 | Union Carbide Corp | Branched chain polysiloxanes and process therefor |
FR1446520A (fr) * | 1964-07-17 | 1966-07-22 | Midland Silicones Ltd | Composition organosilicique utilisable notamment dans les matériaux de construction |
US3445389A (en) * | 1965-03-29 | 1969-05-20 | Dow Corning | Silicone lubricant |
US4221691A (en) * | 1979-02-16 | 1980-09-09 | Dow Corning Corporation | Method of hydrolyzing chlorosilanes |
US4408030A (en) * | 1982-03-22 | 1983-10-04 | Dow Corning Corporation | Waste chlorosilane treatment |
US4487950A (en) * | 1982-04-16 | 1984-12-11 | General Electric Company | Method for making methylchlorosilanes |
FR2564470B1 (fr) * | 1984-05-18 | 1987-01-02 | Rhone Poulenc Spec Chim | Resine organosilicique a motifs disilaniques et a proprietes thermomecaniques ameliorees et en outre utilisables notamment pour l'hydrofugation du batiment |
US4626583A (en) * | 1985-07-11 | 1986-12-02 | Petrarch Systems Inc. | Polysilane-siloxane oligomers and copolymers and methods of making the same |
JP2761931B2 (ja) * | 1989-08-10 | 1998-06-04 | 東レ・ダウコーニング・シリコーン株式会社 | オルガノポリシロキサン及びその製造方法 |
-
1992
- 1992-04-13 US US07/867,938 patent/US5312946A/en not_active Expired - Lifetime
-
1993
- 1993-04-06 AU AU36772/93A patent/AU3677293A/en not_active Abandoned
- 1993-04-07 JP JP5080395A patent/JPH0616815A/ja not_active Withdrawn
- 1993-04-07 EP EP19930302755 patent/EP0566311A3/en not_active Withdrawn
- 1993-04-12 KR KR1019930006047A patent/KR930021686A/ko not_active Withdrawn
- 1993-12-30 US US08/175,897 patent/US5391227A/en not_active Expired - Fee Related
Also Published As
Publication number | Publication date |
---|---|
JPH0616815A (ja) | 1994-01-25 |
AU3677293A (en) | 1993-10-14 |
US5391227A (en) | 1995-02-21 |
US5312946A (en) | 1994-05-17 |
EP0566311A2 (en) | 1993-10-20 |
EP0566311A3 (en) | 1993-11-10 |
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Legal Events
Date | Code | Title | Description |
---|---|---|---|
PA0109 | Patent application |
Patent event code: PA01091R01D Comment text: Patent Application Patent event date: 19930412 |
|
PG1501 | Laying open of application | ||
PC1203 | Withdrawal of no request for examination | ||
WITN | Application deemed withdrawn, e.g. because no request for examination was filed or no examination fee was paid |