KR920700183A - 특정한 금속-함유 촉매를 사용하여 1,4- 비스(4- 페녹시벤조일)벤젠을 제조하는 방법 - Google Patents
특정한 금속-함유 촉매를 사용하여 1,4- 비스(4- 페녹시벤조일)벤젠을 제조하는 방법Info
- Publication number
- KR920700183A KR920700183A KR1019900702433A KR900702433A KR920700183A KR 920700183 A KR920700183 A KR 920700183A KR 1019900702433 A KR1019900702433 A KR 1019900702433A KR 900702433 A KR900702433 A KR 900702433A KR 920700183 A KR920700183 A KR 920700183A
- Authority
- KR
- South Korea
- Prior art keywords
- chloride
- sulfate
- iron
- catalyst
- iii
- Prior art date
Links
Classifications
-
- C—CHEMISTRY; METALLURGY
- C07—ORGANIC CHEMISTRY
- C07C—ACYCLIC OR CARBOCYCLIC COMPOUNDS
- C07C49/00—Ketones; Ketenes; Dimeric ketenes; Ketonic chelates
- C07C49/76—Ketones containing a keto group bound to a six-membered aromatic ring
- C07C49/84—Ketones containing a keto group bound to a six-membered aromatic ring containing ether groups, groups, groups, or groups
-
- C—CHEMISTRY; METALLURGY
- C07—ORGANIC CHEMISTRY
- C07C—ACYCLIC OR CARBOCYCLIC COMPOUNDS
- C07C45/00—Preparation of compounds having >C = O groups bound only to carbon or hydrogen atoms; Preparation of chelates of such compounds
- C07C45/45—Preparation of compounds having >C = O groups bound only to carbon or hydrogen atoms; Preparation of chelates of such compounds by condensation
- C07C45/46—Friedel-Crafts reactions
Landscapes
- Chemical & Material Sciences (AREA)
- Organic Chemistry (AREA)
- Chemical Kinetics & Catalysis (AREA)
- Organic Low-Molecular-Weight Compounds And Preparation Thereof (AREA)
- Catalysts (AREA)
- Low-Molecular Organic Synthesis Reactions Using Catalysts (AREA)
Abstract
Description
Claims (10)
- 지지되지 않은 염화 철(Ⅱ) (염화 제1철), 황산철(Ⅱ) (황산 제1철), 황산 칼륨(Ⅲ), 및 황산 인듐(Ⅲ); 및 불활성 지지체상의 염화철(Ⅲ) 및 염화철(Ⅱ) 황산철(Ⅱ), 황산 칼륨(Ⅲ), 황산인듐(Ⅲ) (염화 제2철)로 이루어진 군으로부터 선택된 적어도 하나의 촉매하에 약 220-258℃의 온도에서 약60-약360분 동안 약 5:1-약 25:1의 각각의 몰 비율로 디페닐 에테르와 1, 4-벤젠 디카르보닐 클로라이드를 접촉시키고, (여기서 1, 4-벤젠 디카르보닐 클로라이드대 촉매의 몰 비율은 약 10:1-1000:1이다.); 두과량의 디페닐 에테르 및 촉매로부터 분리시킴으로써 BPBB생성물을 회수하는 것으로 구성되는, 1, 4-비스(4-페녹시벤조일)벤젠의 제조 방법.
- 제1항에 있어서, 반응 온도가 약 240-258℃인 방법.
- 제2항에 있어서, 디페닐 ;르 대 1, 4-벤젠디카르보닐 클로라이드의 몰 비율이 6-10:1인 방법.
- 제2항에 있어서, 반응시간이 180-360분인 방법.
- 제4항에 있어서, 반응이 약 5시간 동안 약 250℃에서 수행되는 방법.
- 제1항에 있어서, 촉매가 지지되지 않은 철(Ⅱ) 화합물인 방법.
- 제6항에 있어서, 철(Ⅱ) 화합물이 염화 제1철인 방법.
- 제1항에 있어서, 촉매가 불활성 지지체성의 철, 칼륨, 또는 인듐 화합물인 방법.
- 제8항에 있어서, 촉매가 불활성 지지체상의 염화 제2철인 방법.
- 제9항에 있어서, 불활성 지지체가 실리카인 방법.※ 참고사항 : 최초출원 내용에 의하여 공개하는 것임.
Applications Claiming Priority (4)
Application Number | Priority Date | Filing Date | Title |
---|---|---|---|
US07/322,622 US4918237A (en) | 1989-03-13 | 1989-03-13 | Process for the manufacture of 1,4-bis(4-phenoxybenzoyl)benzene with certain metal-containing catalysts |
US07/322,622 | 1989-03-13 | ||
US07/322622 | 1989-03-13 | ||
PCT/US1990/000421 WO1990010613A1 (en) | 1989-03-13 | 1990-01-31 | Process for the manufacture of 1,4-bis(4-phenoxybenzoyl)benzene with certain metal-containing catalysts |
Publications (2)
Publication Number | Publication Date |
---|---|
KR920700183A true KR920700183A (ko) | 1992-02-19 |
KR950000638B1 KR950000638B1 (ko) | 1995-01-26 |
Family
ID=23255679
Family Applications (1)
Application Number | Title | Priority Date | Filing Date |
---|---|---|---|
KR1019900702433A KR950000638B1 (ko) | 1989-03-13 | 1990-01-31 | 특정한 금속-함유 촉매를 사용하여 1,4-비스(4-페녹시벤조일) 벤젠을 제조하는 방법 |
Country Status (9)
Country | Link |
---|---|
US (1) | US4918237A (ko) |
EP (1) | EP0463058B1 (ko) |
KR (1) | KR950000638B1 (ko) |
AT (1) | ATE114296T1 (ko) |
AU (1) | AU624045B2 (ko) |
CA (1) | CA2008693C (ko) |
DE (1) | DE69014299T2 (ko) |
FI (1) | FI93102C (ko) |
WO (1) | WO1990010613A1 (ko) |
Families Citing this family (14)
Publication number | Priority date | Publication date | Assignee | Title |
---|---|---|---|---|
EP3404009B1 (en) | 2017-05-16 | 2019-12-25 | Arkema France | Method for manufacturing 1,4-bis(4-phenoxybenzoyl)benzene in supersaturation conditions |
EP3404013B1 (en) | 2017-05-18 | 2021-10-27 | Arkema France | Purification of 1,4-bis (4-phenoxybenzoyl)benzene by centrifugal filtration |
EP3404012B1 (en) * | 2017-05-18 | 2020-09-09 | Arkema France | Ripening of 1,4-bis (4-phenoxybenzoyl)benzene |
EP3404010B1 (en) | 2017-05-16 | 2020-08-12 | Arkema France | Method for manufacturing 1,4-bis (4-phenoxybenzoyl)benzene using substantially non-hydrolyzed terephthaloyl chloride |
US10793500B2 (en) | 2017-05-16 | 2020-10-06 | Arkema France | Dissociation of 1,4-bis (4-phenoxybenzoyl)benzene—Lewis acid complex in a protic solvent |
ES2829265T3 (es) | 2017-05-16 | 2021-05-31 | Arkema France | Método para fabricar 1,4-bis(4-fenoxibenzoil)benceno a una temperatura elevada |
ES2829267T3 (es) * | 2017-05-18 | 2021-05-31 | Arkema France | Disociación de un complejo de 1,4-bis(4-fenoxibenzoilo)benceno-ácido de Lewis en una disolución acuosa |
EP3431522B1 (en) * | 2017-07-18 | 2020-11-18 | Arkema France | Purification of polyetherketoneketone by centrifugal filtration |
EP3438085A1 (en) * | 2017-08-04 | 2019-02-06 | Arkema France | Process for producing polyether ketone ketone |
KR102262524B1 (ko) | 2017-11-16 | 2021-06-07 | 한화솔루션 주식회사 | 폴리에테르케톤케톤 제조방법 및 이에 의해 제조된 폴리에테르케톤케톤 |
EP3650433B1 (en) * | 2018-11-09 | 2024-04-24 | Arkema France | Method for manufacturing 1,4-bis (4-phenoxybenzoylbenzene) at an elevated temperature |
KR102250300B1 (ko) | 2018-12-11 | 2021-05-07 | 한화솔루션 주식회사 | 폴리에테르케톤케톤의 중합방법 및 이에 의해 중합된 폴리에테르케톤케톤 |
KR102250302B1 (ko) | 2018-12-12 | 2021-05-07 | 한화솔루션 주식회사 | 개선된 폴리에테르케톤케톤 제조방법 및 이에 의해 제조된 폴리에테르케톤케톤 |
KR20220028244A (ko) | 2020-08-28 | 2022-03-08 | 한화솔루션 주식회사 | 1,4-비스(4-페녹시벤조일)벤젠을 제조하는 방법 및 이에 의해 제조된 1,4-비스(4-페녹시벤조일)벤젠 |
Family Cites Families (8)
Publication number | Priority date | Publication date | Assignee | Title |
---|---|---|---|---|
US2879296A (en) * | 1955-07-26 | 1959-03-24 | Monsanto Chemicals | Chlorinated ketone synthesis |
US3288855A (en) * | 1963-03-25 | 1966-11-29 | Monsanto Res Corp | Fluorinated diones |
GB1086021A (en) * | 1964-01-22 | 1967-10-04 | Ici Ltd | Process for the production of aromatic polyketones |
US3360566A (en) * | 1964-11-25 | 1967-12-26 | Hooker Chemical Corp | Manufacture of 2', 4'-dichloroacetophenones and beta-polychlorinated 2', 4'-dichloroacetophenones from mixed dichlorobenzenes |
ES8700647A1 (es) * | 1984-10-11 | 1986-11-16 | Raychem Corp | Procedimiento para la preparacion de un compuesto carbonilo aromatico |
CA1246297A (en) * | 1985-03-11 | 1988-12-06 | Robert A. Clendinning | Process for preparing poly(aryl ether ketones) |
US4908425A (en) * | 1985-06-21 | 1990-03-13 | Amoco Corporation | Chain-extended poly(aryl ether ketones) |
US4827041A (en) * | 1988-03-10 | 1989-05-02 | E. I. Du Pont De Nemours And Company | Process for the manufacture of 1,4-bis(4-phenoxybenzoyl)benzene with a perfluorosulfonyl resin catalyst |
-
1989
- 1989-03-13 US US07/322,622 patent/US4918237A/en not_active Expired - Lifetime
-
1990
- 1990-01-26 CA CA002008693A patent/CA2008693C/en not_active Expired - Lifetime
- 1990-01-31 AU AU52855/90A patent/AU624045B2/en not_active Ceased
- 1990-01-31 AT AT90905016T patent/ATE114296T1/de not_active IP Right Cessation
- 1990-01-31 DE DE69014299T patent/DE69014299T2/de not_active Expired - Lifetime
- 1990-01-31 WO PCT/US1990/000421 patent/WO1990010613A1/en active IP Right Grant
- 1990-01-31 EP EP90905016A patent/EP0463058B1/en not_active Expired - Lifetime
- 1990-01-31 KR KR1019900702433A patent/KR950000638B1/ko not_active IP Right Cessation
-
1991
- 1991-09-11 FI FI914277A patent/FI93102C/fi active
Also Published As
Publication number | Publication date |
---|---|
AU624045B2 (en) | 1992-05-28 |
ATE114296T1 (de) | 1994-12-15 |
WO1990010613A1 (en) | 1990-09-20 |
DE69014299D1 (de) | 1995-01-05 |
AU5285590A (en) | 1990-10-09 |
CA2008693C (en) | 1999-06-01 |
CA2008693A1 (en) | 1990-09-13 |
FI93102B (fi) | 1994-11-15 |
FI93102C (fi) | 1995-02-27 |
EP0463058A1 (en) | 1992-01-02 |
FI914277A0 (fi) | 1991-09-11 |
EP0463058B1 (en) | 1994-11-23 |
KR950000638B1 (ko) | 1995-01-26 |
US4918237A (en) | 1990-04-17 |
DE69014299T2 (de) | 1995-05-18 |
JPH0581578B1 (ko) | 1993-11-15 |
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