[go: up one dir, main page]

KR920000681A - 데카브로모디페닐 알칸의 제조방법 - Google Patents

데카브로모디페닐 알칸의 제조방법 Download PDF

Info

Publication number
KR920000681A
KR920000681A KR1019910005394A KR910005394A KR920000681A KR 920000681 A KR920000681 A KR 920000681A KR 1019910005394 A KR1019910005394 A KR 1019910005394A KR 910005394 A KR910005394 A KR 910005394A KR 920000681 A KR920000681 A KR 920000681A
Authority
KR
South Korea
Prior art keywords
liquid
diphenylalkane
bromine
reaction mass
moles
Prior art date
Legal status (The legal status is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the status listed.)
Granted
Application number
KR1019910005394A
Other languages
English (en)
Other versions
KR0175673B1 (ko
Inventor
헨리 랜스포드 죠오지
Original Assignee
필립 맥키니 피펜저
에틸 코오포레이션
Priority date (The priority date is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the date listed.)
Filing date
Publication date
Family has litigation
First worldwide family litigation filed litigation Critical https://patents.darts-ip.com/?family=24123228&utm_source=google_patent&utm_medium=platform_link&utm_campaign=public_patent_search&patent=KR920000681(A) "Global patent litigation dataset” by Darts-ip is licensed under a Creative Commons Attribution 4.0 International License.
Application filed by 필립 맥키니 피펜저, 에틸 코오포레이션 filed Critical 필립 맥키니 피펜저
Publication of KR920000681A publication Critical patent/KR920000681A/ko
Application granted granted Critical
Publication of KR0175673B1 publication Critical patent/KR0175673B1/ko
Anticipated expiration legal-status Critical
Expired - Lifetime legal-status Critical Current

Links

Classifications

    • C—CHEMISTRY; METALLURGY
    • C07—ORGANIC CHEMISTRY
    • C07C—ACYCLIC OR CARBOCYCLIC COMPOUNDS
    • C07C17/00—Preparation of halogenated hydrocarbons
    • C07C17/093—Preparation of halogenated hydrocarbons by replacement by halogens
    • C07C17/10—Preparation of halogenated hydrocarbons by replacement by halogens of hydrogen atoms
    • C07C17/12—Preparation of halogenated hydrocarbons by replacement by halogens of hydrogen atoms in the ring of aromatic compounds
    • C—CHEMISTRY; METALLURGY
    • C07—ORGANIC CHEMISTRY
    • C07C—ACYCLIC OR CARBOCYCLIC COMPOUNDS
    • C07C25/00—Compounds containing at least one halogen atom bound to a six-membered aromatic ring
    • C07C25/18—Polycyclic aromatic halogenated hydrocarbons

Landscapes

  • Chemical & Material Sciences (AREA)
  • Organic Chemistry (AREA)
  • Organic Low-Molecular-Weight Compounds And Preparation Thereof (AREA)
  • Low-Molecular Organic Synthesis Reactions Using Catalysts (AREA)
  • Nitrogen Condensed Heterocyclic Rings (AREA)

Abstract

내용 없음

Description

데카브로모디페닐 알칸의 제조방법
본 내용은 요부공개 건이므로 전문내용을 수록하지 않았음

Claims (6)

  1. (a)반응용기를 브롬화 축매 및 액체 원소상 브롬으로 충전시키고;(b) 액체 디페닐 알칸을 원소상 브롬의 최초 충전몰당 디페닐알칸 0,055내지 0.033몰을 제공하는 양으로 엑체 브롬의 충전면 아래에서 반응용기에 공급하고;(c)반응 매스를 액체 디페닐알칸 공급 중 30~80℃로 유지시킴을 특징으로 하는 데카브로모디페닐 알카의 제조방법.
  2. 제1항에 있어서, 디페닐알칸이 디페닐에탄인 방법.
  3. 제1항 또는 제2항에 있어서, 액체 디페닐알칸이 브롬 1몰당 디페닐 알칸 0.05 내지 0.035몰을 제공하는 양으로 공급되는 방법.
  4. 제1항 내지 제3항중 어느 한 항에 있어서, 반응 매스가 액체 디페닐알칸 공급중 50~60℃로 유지되는 방법.
  5. 제1항 내지 제4항중 어는 한 항에 있어서, 액체 디페닐알칸 공급이 적어도 대체로 완결되는 1 시간 내에 물을 반응 매스에 첨가하여 브롬화 촉매를 불활성화시키는 방법.
  6. 제1항 내지 제5항 중 어느 한 항에 있어서, 액체 디페닐알칸이 액체브롬의 충전면으로 부터 약 1/2인치 아래에서 공급되는 방법.
    ※ 참고사항 : 최초출원 내용에 의하여 공개하는 것임.
KR1019910005394A 1990-06-04 1991-04-03 데카브로모디페닐 알칸의 제조방법 Expired - Lifetime KR0175673B1 (ko)

Applications Claiming Priority (3)

Application Number Priority Date Filing Date Title
US532800 1990-06-04
US532,800 1990-06-04
US07/532,800 US5030778A (en) 1990-06-04 1990-06-04 Decabromodiphenyl alkane process

Publications (2)

Publication Number Publication Date
KR920000681A true KR920000681A (ko) 1992-01-29
KR0175673B1 KR0175673B1 (ko) 1999-05-15

Family

ID=24123228

Family Applications (1)

Application Number Title Priority Date Filing Date
KR1019910005394A Expired - Lifetime KR0175673B1 (ko) 1990-06-04 1991-04-03 데카브로모디페닐 알칸의 제조방법

Country Status (7)

Country Link
US (1) US5030778A (ko)
EP (1) EP0460922B1 (ko)
JP (1) JP2902158B2 (ko)
KR (1) KR0175673B1 (ko)
DE (1) DE69105046T2 (ko)
ES (1) ES2064043T3 (ko)
IL (1) IL97658A (ko)

Families Citing this family (34)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
CA2047256C (en) * 1990-07-30 2002-03-05 Saadat Hussain Process for decabromodiphenylalkane predominant product
TW284788B (ko) * 1991-05-28 1996-09-01 L Air Liquide Soliete And Nyme Dour L Expl Des Proce
JP3193494B2 (ja) * 1992-01-03 2001-07-30 レール・リキード・ソシエテ・アノニム・プール・レテュード・エ・レクスプロワタシオン・デ・プロセデ・ジョルジュ・クロード 希ガスを使用し、グルコースから高フルクトースコーンシロップを製造する方法
CA2102888A1 (en) 1992-04-03 1993-10-04 Kevin C. Spencer A method of controlling browning reactions using noble gases
US6342261B1 (en) 1992-04-03 2002-01-29 American Air Liquide Method of preserving foods using noble gases
US5364777A (en) * 1992-04-03 1994-11-15 American Air Liquide Method of improving lipase activity using noble gases
US5324874A (en) * 1992-05-26 1994-06-28 Ethyl Corporation Process for a decarbromodiphenylethane predominate product having enhanced whiteness
EP0571859A3 (en) * 1992-05-26 1994-11-02 Ethyl Corp Product consisting predominantly of decabromodiphenylethane with increased whiteness.
US5328823A (en) * 1992-11-27 1994-07-12 American Air Liquide Enzyme-based biosensors for detecting noble gases
US5382525A (en) * 1992-11-27 1995-01-17 American Air Liquide Method of effecting increased performance of diagnostic enzyme reaction systems using noble gases
CA2109458A1 (en) 1992-11-27 1994-05-28 Kevin C. Spencer Method of improving processes using pectinase enzymes with noble gases
KR960701969A (ko) * 1993-04-07 1996-03-28 스티븐 디. 크레크 브롬화 디페닐알칸 제품 및 제조방법(brominated diphenylalkane products and processes)
JP2596889B2 (ja) * 1993-08-18 1997-04-02 チッソ株式会社 樹脂組成物
US6518468B1 (en) * 1994-09-16 2003-02-11 Albemarle Corporation Bromination process
CA2200081C (en) * 1994-09-16 2007-04-24 John C. Parks Improved bromination process
EP0784648B2 (en) * 1994-10-05 2010-10-27 Great Lakes Chemical Corporation Continuous bromination process and products thereof
US6117371A (en) * 1994-10-05 2000-09-12 Great Lakes Chemical Corporation Continuous bromination process and products thereof
DE19512407A1 (de) * 1995-04-03 1996-10-10 Basf Ag Flammgeschützte thermoplastische Formmassen
US6743825B1 (en) * 2001-08-03 2004-06-01 Albemarle Corporation Poly(bromoaryl)alkane additives and methods for their preparation and use
US7255927B2 (en) * 2001-12-05 2007-08-14 Isola Usa Corp. Laminate composition
WO2003048249A1 (en) * 2001-12-05 2003-06-12 Isola Laminate Systems Corp. Thermosetting resin composition for high performance laminates
US20030158337A1 (en) * 2001-12-05 2003-08-21 Isola Laminate Systems Corp. Thermosetting resin composition for high performance laminates
WO2003055832A1 (en) * 2001-12-21 2003-07-10 Pabu Services, Inc. Method and apparatus for producing decabromodiphenyl alkanes
US20080058458A1 (en) * 2006-08-29 2008-03-06 Albemarle Corporation Preparation of decahalodiphenyl ethane
WO2008027779A1 (en) * 2006-08-29 2008-03-06 Albemarle Corporation Preparation of decabromodiphenyl oxide
CN101528654B (zh) * 2006-08-31 2012-12-26 溴化合物有限公司 制备多溴化化合物的方法
WO2008057645A1 (en) * 2006-11-08 2008-05-15 Albemarle Corporation Preparation of high assay decabromodiphenylalkane
CN103641677A (zh) * 2006-11-09 2014-03-19 雅宝公司 包含吸留溴的固态溴化芳香族有机化合物的处理方法
WO2008066980A1 (en) * 2006-12-01 2008-06-05 Albemarle Corporation Production of high purity decabromodiphenylalkanes
WO2008097348A1 (en) 2007-02-08 2008-08-14 Albemarle Corporation Process for separation of bromine from gaseous hydrogen bromide and use of such process in production of decabromodiphenylethane
ES2501443T3 (es) * 2007-03-16 2014-10-01 Albemarle Corporation Preparación y suministro de decabromodifeniletano de alto ensayo
KR101397245B1 (ko) 2007-03-16 2014-05-20 알베마를 코포레이션 고순도 데카브로모디페닐에탄의 제조와 공급
CN101643388B (zh) * 2009-06-22 2012-06-27 泰州百力化学股份有限公司 十溴二苯乙烷的制备方法
PL2459506T3 (pl) * 2009-07-27 2014-09-30 Albemarle Corp Wytwarzanie wysokiej próby produktu dekabromodifenyloalkanowego o niskiej zawartości zokludowanego wolnego bromu

Family Cites Families (6)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
FR1229815A (fr) * 1959-03-10 1960-09-09 Electro Chimie Soc D Procédé de préparation de diphényle chloré et produits ainsi obtenus
FR2031649A5 (ko) * 1969-02-03 1970-11-20 Ugine Kuhlmann
US3763248A (en) * 1971-03-02 1973-10-02 Ethyl Corp Process for production of poly brominated aromatics
US3833674A (en) * 1972-08-24 1974-09-03 Ethyl Corp Recovery of brominated biphenyl
FR2236818B1 (ko) * 1973-07-13 1976-04-30 Ugine Kuhlmann
CA1321213C (en) * 1988-06-13 1993-08-10 Saadat Hussain Bromination process

Also Published As

Publication number Publication date
ES2064043T3 (es) 1995-01-16
DE69105046D1 (de) 1994-12-15
IL97658A (en) 1994-07-31
JP2902158B2 (ja) 1999-06-07
DE69105046T2 (de) 1995-04-06
JPH04261128A (ja) 1992-09-17
EP0460922B1 (en) 1994-11-09
KR0175673B1 (ko) 1999-05-15
US5030778A (en) 1991-07-09
IL97658A0 (en) 1992-06-21
EP0460922A1 (en) 1991-12-11

Similar Documents

Publication Publication Date Title
KR920000681A (ko) 데카브로모디페닐 알칸의 제조방법
GB1046313A (en) Process for the preparation of chlorine, bromine or iodine and for the preparation of halogenated hydrocarbons
KR840001595A (ko) 할로겐화 엘라스토머의 제조방법
ES517704A0 (es) Recipiente para el almacenamiento de acetileno.
GB980983A (en) Oxychlorination process
GB883256A (en) Halogenation process
JPS6463540A (en) Bromination
ES2143634T3 (es) Procedimiento de produccion de difluorometano.
ES291002A1 (es) Procedimiento de producciën de hidrocarburos clorados
GB1244811A (en) Process for the preparation of substituted aromatic compounds
ES8303339A1 (es) Un procedimiento para la preparacion de 2,3-dicloro-5-triclorometilpiridina.
ES8406407A1 (es) Procedimiento para la preparacion de 1,2-dicloroetano
CA2094469A1 (en) Process for a decabromodiphenylethane predominate product having enhanced whiteness
GB1441457A (en) Reactors
GB1050540A (ko)
GB1313524A (en) Conversion of vinylbenzenes to ethynylbenzenes
GB867198A (en) Process for the production of trans-1,2-dihalogenoethylenes
US2849501A (en) Process for making chloromesitylene
GB1497015A (en) Process for the continuous manufacture of nuclear chlorinated toluenes
GB1019150A (en) Improvements in or relating to the manufacture of 1,2,3,4-tetrachlorobutane
ES421724A1 (es) Procedimiento de cloracion de etileno.
ES391440A3 (es) Un procedimiento de cloracion parcial.
KR910016655A (ko) 디에티닐벤젠의 개선된 합성법
KR920011981A (ko) 데카브로모디페닐알칸 공정
KR910007844A (ko) 2, 5-디클로로 톨루엔 및 2, 6-디클로로 톨루엔을 병행적으로 제조하는 방법

Legal Events

Date Code Title Description
PA0109 Patent application

Patent event code: PA01091R01D

Comment text: Patent Application

Patent event date: 19910403

PG1501 Laying open of application
A201 Request for examination
PA0201 Request for examination

Patent event code: PA02012R01D

Patent event date: 19960322

Comment text: Request for Examination of Application

Patent event code: PA02011R01I

Patent event date: 19910403

Comment text: Patent Application

N231 Notification of change of applicant
PN2301 Change of applicant

Patent event date: 19960412

Comment text: Notification of Change of Applicant

Patent event code: PN23011R01D

E701 Decision to grant or registration of patent right
PE0701 Decision of registration

Patent event code: PE07011S01D

Comment text: Decision to Grant Registration

Patent event date: 19980831

GRNT Written decision to grant
PR0701 Registration of establishment

Comment text: Registration of Establishment

Patent event date: 19981111

Patent event code: PR07011E01D

PR1002 Payment of registration fee

Payment date: 19981111

End annual number: 3

Start annual number: 1

PG1601 Publication of registration
PR1001 Payment of annual fee

Payment date: 20011101

Start annual number: 4

End annual number: 4

PR1001 Payment of annual fee

Payment date: 20021104

Start annual number: 5

End annual number: 5

PR1001 Payment of annual fee

Payment date: 20031030

Start annual number: 6

End annual number: 6

PR1001 Payment of annual fee

Payment date: 20041102

Start annual number: 7

End annual number: 7

PR1001 Payment of annual fee

Payment date: 20051108

Start annual number: 8

End annual number: 8

PR1001 Payment of annual fee

Payment date: 20061102

Start annual number: 9

End annual number: 9

PR1001 Payment of annual fee

Payment date: 20071108

Start annual number: 10

End annual number: 10

PR1001 Payment of annual fee

Payment date: 20081104

Start annual number: 11

End annual number: 11

PR1001 Payment of annual fee

Payment date: 20091111

Start annual number: 12

End annual number: 12

FPAY Annual fee payment

Payment date: 20101028

Year of fee payment: 13

PR1001 Payment of annual fee

Payment date: 20101028

Start annual number: 13

End annual number: 13

EXPY Expiration of term
PC1801 Expiration of term

Termination date: 20120110

Termination category: Expiration of duration