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KR840004709A - 일가 또는 다가페놀의 글리시딜 에테르의 제조방법 - Google Patents

일가 또는 다가페놀의 글리시딜 에테르의 제조방법 Download PDF

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Publication number
KR840004709A
KR840004709A KR1019830001782A KR830001782A KR840004709A KR 840004709 A KR840004709 A KR 840004709A KR 1019830001782 A KR1019830001782 A KR 1019830001782A KR 830001782 A KR830001782 A KR 830001782A KR 840004709 A KR840004709 A KR 840004709A
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South Korea
Prior art keywords
cyclic
monovalent
process according
ether compound
reaction
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Application number
KR1019830001782A
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English (en)
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KR910001133B1 (ko
Inventor
이꼬(외 3) 이또
Original Assignee
니시끼다 아끼요시
스미또모 가까꾸고교 가부시기 가이샤
Priority date (The priority date is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the date listed.)
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Publication date
Priority claimed from JP7183882A external-priority patent/JPS58189223A/ja
Priority claimed from JP7183982A external-priority patent/JPS5940831B2/ja
Application filed by 니시끼다 아끼요시, 스미또모 가까꾸고교 가부시기 가이샤 filed Critical 니시끼다 아끼요시
Publication of KR840004709A publication Critical patent/KR840004709A/ko
Application granted granted Critical
Publication of KR910001133B1 publication Critical patent/KR910001133B1/ko

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Classifications

    • C—CHEMISTRY; METALLURGY
    • C07—ORGANIC CHEMISTRY
    • C07D—HETEROCYCLIC COMPOUNDS
    • C07D301/00—Preparation of oxiranes
    • C07D301/27—Condensation of epihalohydrins or halohydrins with compounds containing active hydrogen atoms
    • C07D301/28—Condensation of epihalohydrins or halohydrins with compounds containing active hydrogen atoms by reaction with hydroxyl radicals
    • C—CHEMISTRY; METALLURGY
    • C07—ORGANIC CHEMISTRY
    • C07D—HETEROCYCLIC COMPOUNDS
    • C07D303/00—Compounds containing three-membered rings having one oxygen atom as the only ring hetero atom
    • C07D303/02—Compounds containing oxirane rings
    • C07D303/12—Compounds containing oxirane rings with hydrocarbon radicals, substituted by singly or doubly bound oxygen atoms
    • C07D303/18—Compounds containing oxirane rings with hydrocarbon radicals, substituted by singly or doubly bound oxygen atoms by etherified hydroxyl radicals
    • C07D303/20—Ethers with hydroxy compounds containing no oxirane rings
    • C07D303/22—Ethers with hydroxy compounds containing no oxirane rings with monohydroxy compounds
    • C—CHEMISTRY; METALLURGY
    • C07—ORGANIC CHEMISTRY
    • C07D—HETEROCYCLIC COMPOUNDS
    • C07D303/00—Compounds containing three-membered rings having one oxygen atom as the only ring hetero atom
    • C07D303/02—Compounds containing oxirane rings
    • C07D303/12—Compounds containing oxirane rings with hydrocarbon radicals, substituted by singly or doubly bound oxygen atoms
    • C07D303/18—Compounds containing oxirane rings with hydrocarbon radicals, substituted by singly or doubly bound oxygen atoms by etherified hydroxyl radicals
    • C07D303/20—Ethers with hydroxy compounds containing no oxirane rings
    • C07D303/24—Ethers with hydroxy compounds containing no oxirane rings with polyhydroxy compounds

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  • Chemical & Material Sciences (AREA)
  • Organic Chemistry (AREA)
  • Chemical Kinetics & Catalysis (AREA)
  • Epoxy Compounds (AREA)
  • Epoxy Resins (AREA)

Abstract

내용 없음

Description

일가 또는 다가페놀의 글리시딜 에테르의 제조방법
본 내용은 요부공개 건이므로 전문내용을 수록하지 않았음

Claims (5)

  1. 일가 또는 다가 페놀과 에피클로로하이드린을 알칼리 금속 수산화물의 존재하에 반응시켜 일가 또는 다가 페놀의 글리시딜 에테르를 제조하는 방법에 있어서, 환상 또는 직쇄상 에테르 화합물의 공존하에 반응시킴을 특징으로 하는 제조방법.
  2. 제1항에 있어서, 제4급 암모늄염 또는 제4급 암모늄 염기의 공존하에 반응시킴을 특징으로 하는 제조방법.
  3. 제1항 또는 제2항에 있어서, 환상 에테르가 디옥산임을 특징으로 하는 제조방법.
  4. 제1항 또는 제2항에 있어서, 반응 혼합물계 중에 수분을 0.2 내지 2.5중량% 존재시킴을 특징으로 하는 제조방법.
  5. 제1,2,3 또는 4항에 있어서, 일가 또는 다가 페놀의 에피클로로하이드린 용액과 환상 또는 직쇄 에테르 화합물을 용해한 용액에 알칼리 금속 수산화물의 수용액을 연속적으로 첨가하고 이 반응 혼합물로부터 물, 에피클롤히드린 및 환상 또는 직쇄 에테르 화합물을 공비시켜 액화 분액하고 유기 물층은 반응 혼합물 중에 순환시켜 수층을 제거함을 특징으로 하는 제조방법.
    ※ 참고사항 : 최초출원 내용에 의하여 공개하는 것임.
KR1019830001782A 1982-04-28 1983-04-27 1가 또는 다가 페놀의 글리시딜 에테르의 제조방법 KR910001133B1 (ko)

Applications Claiming Priority (6)

Application Number Priority Date Filing Date Title
JP71839 1982-04-28
JP7183882A JPS58189223A (ja) 1982-04-28 1982-04-28 エポキシ樹脂の製造方法
JP71838 1982-04-28
JP71.839 1982-04-28
JP71.838 1982-04-28
JP7183982A JPS5940831B2 (ja) 1982-04-28 1982-04-28 １価又は多価フエノ−ルのグリシジルエ−テルの製造方法

Publications (2)

Publication Number Publication Date
KR840004709A true KR840004709A (ko) 1984-10-24
KR910001133B1 KR910001133B1 (ko) 1991-02-25

Family

ID=26412946

Family Applications (1)

Application Number Title Priority Date Filing Date
KR1019830001782A KR910001133B1 (ko) 1982-04-28 1983-04-27 1가 또는 다가 페놀의 글리시딜 에테르의 제조방법

Country Status (4)

Country Link
US (1) US4876371A (ko)
KR (1) KR910001133B1 (ko)
DE (1) DE3315365A1 (ko)
GB (1) GB2120659B (ko)

Families Citing this family (14)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
AU568601B2 (en) * 1982-09-13 1988-01-07 Dow Chemical Company, The Process for making epoxy resins
AU571499B2 (en) * 1983-04-01 1988-04-21 Dow Chemical Company, The Preparing epoxy resins
US4585838A (en) * 1985-08-06 1986-04-29 The Dow Chemical Company Process for preparing epoxy resins containing low levels of total halide
US4535150A (en) * 1984-12-04 1985-08-13 Celanese Corporation Process for preparing epoxy resins having low hydrolyzable chlorine contents
ES2059307T3 (es) * 1985-12-13 1994-11-16 Ciba Geigy Ag Procedimiento para la preparacion de compuestos glicidilo.
DE3635383A1 (de) * 1986-10-17 1988-04-21 Ruetgerswerke Ag Verfahren zur herstellung von glycidylverbindungen
US4785061A (en) * 1987-08-13 1988-11-15 The Dow Chemical Company Method for reducing the aliphatic halide content of epoxy resins using a solvent mixture including a polar aprotic solvent
US4778863A (en) * 1987-08-13 1988-10-18 The Dow Chemical Company Preparation of epoxy resins having low undesirable halogen content
US5223646A (en) * 1989-12-27 1993-06-29 Daiso Company, Ltd. Process for producing optically active atenolol and intermediate thereof
JPH0674243B2 (ja) * 1989-12-27 1994-09-21 ダイソー株式会社 光学純度の高い光学活性アテノロール塩及びアテノロールの製法
US5290958A (en) * 1993-03-18 1994-03-01 Industrial Technology Research Institute Phase transfer catalytic process for preparing intermediates of atenolol, propranolol, and their derivatives
WO2002059177A2 (en) * 2000-12-22 2002-08-01 Dow Global Technologies Inc. Poly (hydroxyaminoethers) having a low chloride content
CN104130217A (zh) * 2014-07-18 2014-11-05 苏州保力瑞生物材料科技开发有限公司 一种绿色分离植物单酚缩水甘油醚及回收工业盐的方法
US10961208B1 (en) 2019-12-24 2021-03-30 Chang Chun Plastics Co., Ltd. Product of glycidyl ether of a mono or polyhydric phenol

Family Cites Families (12)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
US2901462A (en) * 1956-11-30 1959-08-25 Shell Dev Process for the manufacture of epoxy resins
US3033817A (en) * 1958-10-17 1962-05-08 Devoe & Raynolds Co Production of aliphatic modified epoxide resins
GB1050641A (ko) * 1963-01-18
US3372142A (en) * 1964-01-31 1968-03-05 Dow Chemical Co Epoxidation process
US3417050A (en) * 1965-05-04 1968-12-17 Celanese Coatings Co Epoxide resin process
US3325452A (en) * 1966-03-15 1967-06-13 Celanese Coatings Co Preparation of glycidyl polyethers
GB1104494A (en) * 1966-04-05 1968-02-28 Chiyoda Chem Eng Construct Co A method of producing an epoxy resin condensate
CH593272A5 (ko) * 1974-05-24 1977-11-30 Inventa Ag
IT1051400B (it) * 1975-12-19 1981-04-21 S I R S P A Procedimento perfezionato per la preparazione di resine epossidiche liquide
US4072656A (en) * 1976-05-24 1978-02-07 Ici Americas Inc. Glycidyl ethers derived from 3,3',5,5'-tetraalkyl-4,4'-dihydroxybiphenyl
JPS53109600A (en) * 1977-03-07 1978-09-25 Ueno Seiyaku Oyo Kenkyujo Kk Manufacture of eposy resin
DE2947469A1 (de) * 1979-11-24 1981-06-04 Hoechst Ag, 6000 Frankfurt Verfahren zur herstellung von glycidylaethern ein- oder mehrwertiger phenole

Also Published As

Publication number Publication date
GB2120659B (en) 1985-12-04
KR910001133B1 (ko) 1991-02-25
DE3315365A1 (de) 1983-11-03
US4876371A (en) 1989-10-24
DE3315365C2 (ko) 1991-06-13
GB8311480D0 (en) 1983-06-02
GB2120659A (en) 1983-12-07

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