KR102319608B1 - Perfume composition comprising an essential oil as an active ingredient and a method for preparing a perfume comprising thereof - Google Patents

Abstract

The present invention relates to a perfume composition comprising essential oil (essential oil) as an active ingredient and a method for producing a perfume comprising the same, and more specifically, to aromatherapy including domestic natural essential oil and aroma oil as active ingredients. It relates to a perfume composition comprising a natural essential oil applicable to an active ingredient and a method for producing a perfume comprising the same.

Description

Perfume composition comprising an essential oil as an active ingredient and a method for manufacturing a perfume comprising the same

The present invention relates to a perfume composition comprising essential oil (essential oil) as an active ingredient and a method for producing a perfume comprising the same, and more specifically, to aromatherapy including domestic natural essential oil and aroma oil as active ingredients. It relates to a perfume composition comprising a natural essential oil applicable to an active ingredient and a method for producing a perfume comprising the same.

There are about 300,000 species of plants worldwide, and depending on their use, a toll plant, a medicinal plant, a spice plant, a spice plant, a fiber plant, a starch plant, a sugar plant, a sweetener plant, a pigment plant, a paint plant, and a wild vegetable plant , bioenergy plants, and fragrance plants.

Fragrances composed of substances that transmit fragrance are largely divided into natural fragrances and synthetic fragrances. Natural fragrances are obtained through various methods from animals, plants, and microorganisms, and synthetic fragrances are obtained through organic synthesis. Among the natural fragrances, animal-based fragrances are mainly Ambergris obtained from whales, civets obtained from civet cats, Muscones obtained from musk deer, and Casrorium obtained from beavers. Plant-based fragrances are obtained from plants with various scents. Well-known ones include bergamot, sage, eucalyptus, juniper, patchouli, sandalwood, vanilla, ylang-ylang, hyssop, chamomile, thyme (CK Dodt. 1996. The Essential Oils Book. Storey Books.).

Natural fragrances are divided into fragrance (fragrance for cosmetics) and flavor (food fragrance) according to their use. It is known that the market share of fragrances and flavors is around 51% and 49% worldwide.

Natural fragrance has been used as a raw material for perfume since ancient times (Han Sang-gil. 2002. The Story of Immortal Luxury Perfume. Shinkwang Publishing Company), and has been used as a raw material for making products that change with the times (People who love incense. 1999. Incense, Perfume Story) .Han Song). Some of the most famous perfume manufacturers around the world today are Gallin, Esté Rohde, Aramis, Lancome, Elizabeth Arden, Giorgio Beverly Hills, Molinar, Carron, Bourjois, Borsari, Carita, Clarence, Aveda, Gail Heyman, La Prairie, and Chanel. , Christian Dior, Calvin Klein, Davidoff, Georgie Armani, Gucci, Kenzo, Hugo Boss, Nina Ricci, Pierre Cardin, Ralph Lauren, Versace, and these companies are launching new products every year (Lee Sang-woo. 2006. All About Perfume) . meeting).

World-famous perfume companies are releasing a variety of perfumes according to the changing times. In the 1920s, innovative fragrances that insist on individuality, in the 1940s, green fragrances, and in the 1970s, feminine green-floral series. In the 1990s, it launched a fragrance that could be used by both men and women, and in the 2000s, it launched a new fragrance, the unfamiliar Flanker.

However, essential oils added to most perfumes currently manufactured are foreign products, and the supply of perfumes using essential oils for domestic plants is somewhat insufficient.

Therefore, in order to supplement the above-mentioned problems, the present inventors have completed the present invention, recognizing that it is urgent to develop a perfume including an essential oil that can be produced in Korea as an active ingredient.

Republic of Korea Patent Publication No. 10-0843680 Republic of Korea Patent Publication No. 10-0843692 Republic of Korea Patent Publication No. 10-0529819

An object of the present invention is to produce a perfume composition and perfume containing the same as an active ingredient, which can be supplied in Korea and is easy to mass-produce, has an excellent fragrance of natural fragrance, is harmless to the human body, and is eco-friendly and has a natural natural fragrance to provide a way

Another object of the present invention is to provide a perfume composition comprising an essential oil applicable to aromatherapy, such as recovery from mental fatigue and stress recovery, as an active ingredient, as an active ingredient, and a method for producing a perfume comprising the same with the unique scent of essential oils and aroma oils.

Another object of the present invention is not only perfume, but also various cosmetics including perfume (aromatic cosmetics, basic cosmetics, powder, hair cosmetics, bath products), food additives (juice, ice cream, candy, seasonings, spices, for flavored cigarettes, pharmaceuticals) ), to provide a perfume composition including an essential oil applicable to various industries such as household products (cleansing agent, soap), etc. as an active ingredient, and a method for producing a perfume including the same.

The problems of the present invention are not limited to the problems mentioned above, and other problems not mentioned will be clearly understood by those skilled in the art from the following description.

In order to achieve the above object, the present invention provides a perfume composition comprising an essential oil as an active ingredient and a method for producing a perfume comprising the same.

Hereinafter, the present specification will be described in more detail.

The present invention relates to a perfume composition comprising essential oil (essential oil) as an active ingredient, and 1 to 5 parts by weight of lavender extract, 1 to 15 parts by weight of essential oil, and 1 aromatic oil based on the total weight of the perfume composition. to 10 parts by weight, 1 to 5 parts by weight of baby powder, 15 to 40 parts by weight of purified water, and 50 to 80 parts by weight of anhydrous vegetable ethanol;

More specifically, the perfume composition contains 2 to 4 parts by weight of lavender extract, 3 to 7 parts by weight of aroma oil, 3 to 10 parts by weight of essential oil, 2.5 to 4 parts by weight of baby powder, 25 to 35 parts by weight of purified water, based on the total weight. And 65 to 75 parts by weight of vegetable absolute ethanol; characterized in that it contains.

In the present invention, the essential oil is characterized in that at least one selected from the group consisting of cypress, pine, citron, grapefruit and fir essential oil.

In the present invention, the aroma oil is one or more selected from the group consisting of sweet orange oil, rosemary oil, cinnamon oil, peppermint oil, and lavender oil. do it with

In addition, the present invention provides a perfume manufacturing method, characterized in that the perfume composition is prepared using a steam distillation method.

All the matters mentioned in the perfume composition of the present invention and the perfume manufacturing method comprising the same are equally applied as long as they do not contradict each other.

The perfume composition containing the essential oil of the present invention as an active ingredient and the manufacturing method of the perfume including the same can be supplied domestically, so it is easy to mass-produce, and the natural fragrance has excellent fragrance and is harmless to the human body. It can be applied to aromatherapy such as mental fatigue recovery and stress recovery.

In addition, the perfume composition containing the essential oil of the present invention as an active ingredient and the manufacturing method of the perfume including the same are not only perfumes, but also various cosmetics (aromatic cosmetics, basic cosmetics, powders, hair cosmetics, bath products) including perfumes, and food products. It can be applied to various industries such as additives (juice, ice cream, candy, seasonings, spices, incense tobacco, pharmaceuticals), household goods (detergent, soap), etc.

Effects of the present invention are not limited to the effects mentioned above, and other effects not mentioned will be clearly understood by those skilled in the art from the description of the claims.

1 is a view showing the result of preparing a perfume composition (Example 4) containing the essential oil of the present invention as an active ingredient.

The terms used in this specification have been selected as currently widely used general terms as possible while considering the functions in the present invention, which may vary depending on the intention or precedent of a person skilled in the art, the emergence of new technology, and the like. In addition, in a specific case, there is a term arbitrarily selected by the applicant, and in this case, the meaning will be described in detail in the description of the corresponding invention. Therefore, the term used in the present invention should be defined based on the meaning of the term and the overall content of the present invention, rather than the name of a simple term.

Unless defined otherwise, all terms used herein, including technical and scientific terms, have the same meaning as commonly understood by one of ordinary skill in the art to which this invention belongs. Terms such as those defined in a commonly used dictionary should be interpreted as having a meaning consistent with the meaning in the context of the related art, and should not be interpreted in an ideal or excessively formal meaning unless explicitly defined in the present application. does not

Numerical ranges are inclusive of the values defined in that range. Every maximum numerical limitation given throughout this specification includes all lower numerical limitations as if the lower numerical limitation were expressly written. Every minimum numerical limitation given throughout this specification includes all higher numerical limitations as if the higher numerical limitation were expressly written. Any numerical limitation given throughout this specification shall include all numerical ranges within the broader numerical range, as if the narrower numerical limitation were expressly written.

Hereinafter, examples of the present invention will be described in detail, but it is obvious that the present invention is not limited by the following examples.

perfume composition

The present invention relates to a perfume composition comprising essential oil as an active ingredient, and more particularly, to a perfume composition comprising lavender extract, essential oil (essential oil), aroma oil, baby powder, purified water and vegetable absolute ethanol. will be.

The perfume composition includes 1 to 5 parts by weight of lavender extract, 1 to 15 parts by weight of essential oil, 1 to 10 parts by weight of aroma oil, 1 to 5 parts by weight of baby powder, purified water based on the total weight of the perfume composition. 15 to 40 parts by weight and 50 to 80 parts by weight of anhydrous vegetable ethanol; preferably, 2 to 4 parts by weight of lavender extract, 3 to 7 parts by weight of aroma oil, 3 to 10 parts by weight of essential oil , 2.5 to 4 parts by weight of baby powder, 25 to 35 parts by weight of purified water, and 65 to 75 parts by weight of anhydrous vegetable ethanol; may include.

In the present invention, the lavender extract may be extracted from petals, stems, roots, etc. of lavender, preferably extracted from petals of lavender. In addition, the lavender may be collected, cultivated, or commercially available without limitation.

The lavender extract may include water, alcohol, or a mixed solvent thereof. When the alcohol is used as a solvent, the lavender extract may be preferably a C1-C4 alcohol, and more preferably, may be extracted with methanol or ethanol, , most preferably water, 30% to 80% methanol (v/v) or 30% to 80% ethanol (v/v). The lavender extract according to the present invention is 100 ℃ when the extraction solvent is water, 80 ℃ when 50% methanol (v/v), 85 ℃, 70% ethanol (v/v) when 30% ethanol (v/v) v), it is preferable to proceed with the extraction at 80 ℃. In the present invention, the 50% methanol extract of lavender means a methanol extract of about 50%, and may include 45% to 55% methanol extract. The 30% ethanol extract of lavender means an ethanol extract of about 30%, and may include 25% to 35% ethanol extract. The 70% ethanol extract of lavender means an ethanol extract of about 70%, and may include 65% to 75% ethanol extract.

The extraction solvent is preferably 2 to 20 times the dry weight of lavender. Thereafter, the process of filtration, concentration under reduced pressure and dry powdering of the extract may be additionally included.

The lavender extract may be extracted through hot water extraction, ultrasonic extraction, filtration, reflux extraction, immersion extraction, or high-temperature and high-pressure steam extraction, and these may be performed alone or in combination of two or more methods.

The lavender extract of the present invention may additionally include the steps of filtration, concentration under reduced pressure, and drying and powdering of the extract. In addition, it may include all lavender extracts prepared according to methods known in the art or similar in the art, and the method is an example, and the method for preparing a lavender extract is not limited thereto.

In the present invention, the essential oil may be at least one selected from the group consisting of cypress, pine, citron, grapefruit, and fir oil, preferably citron, grapefruit, fir, or a mixed oil thereof. .

The cypress essential oil is non-toxic and non-irritating essential oil, and it can emit significantly more phytoncide compared to other tree oils, thereby giving psychological stability.

The pine essential oil is a representative essential oil that affects the physical and mental level, and provides a user's vitality by giving a refreshing feeling, and can exhibit an antibacterial effect at the same time.

The citron essential oil contains more than three times more vitamin C than lemon, so it can improve concentration and prevent depression, so it is easy to apply to aromatherapy. The citron essential oil used in the present invention may include hesperidin and limonene as active ingredients.

The grapefruit essential oil has a high content ratio of aldehyde components and linalo, so it can prevent stress, depression, etc., and has an antibacterial effect, so it can be easily applied to colds and sterilization. The grapefruit essential oil used in the present invention may contain 80 to 85% limonene.

The fir essential oil can help prevent respiratory diseases and prevent respiratory diseases caused by fine dust and the like. The fir essential oil used in the present invention contains 30 to 40% by weight of bornyl acetate, 10 to 30% by weight of α-β-pinene, and 10 to 25% by weight of campene. (campene), 1 to 7% by weight of santene, 2 to 7% by weight of borneol, and 1 to 5% by weight of bisabolol (bisabolol).

In the present invention, the aroma oil may be one or more selected from the group consisting of sweet orange oil, rosemary oil, cinnamon oil, peppermint oil, and lavender oil. .

The sweet orange oil contains 95 to 98% limonene, which stimulates lymph flow to help improve skin such as acne and dryness, and relieves stress by lowering cholesterol levels and releasing tension has

The rosemary oil may most preferably be creeping rosemary. The rosemary oil relieves mental fatigue and helplessness and affects brain activity, so it is good for headaches and migraines as well as improving memory.

The cinnamon oil has a warm property, so it has an effect of making you feel warm in cold and cold emotions. It can also help relieve nervous tension and fatigue.

The peppermint oil contains menthol, a volatile essential oil component, as an active ingredient, which acts on the nervous system to promote dopamine secretion in the brain, thereby making you feel refreshed and good, increasing concentration and relieving tension. indicates. The peppermint oil used in the present invention may contain 40 to 65% by weight of menthol, 15 to 30% by weight of menthone, and 5 to 12% by weight of 1.8 cieole.

The lavender oil is a non-irritating and non-toxic oil, which can help with cell regeneration and insomnia, and can help to recover from physical fatigue and relieve mental stress at the same time. The lavender oil used in the present invention may contain 40 to 60% by weight of linalyl acetate and 40 to 60% by weight of linalool.

In the present invention, the baby powder may represent a warm energy by representing the scent of baby powder.

In the present invention, as the purified water, only pure water purified through distillation or ion exchange resin may be used.

In the present invention, the vegetable anhydrous ethanol is 99.9% or more of ultra-high purity absolute ethanol extracted from starch-based plants, and has good volatility and can exhibit long-lasting fragrance.

The perfume composition containing the essential oil of the present invention as an active ingredient can be supplied domestically, so it is easy to mass-produce. Applicable to aromatherapy.

How to make perfume

The present invention includes a perfume composition comprising the essential oil as an active ingredient, and a perfume can be manufactured using a steam distillation method.

The perfume composition comprising the essential oil as an active ingredient is as described above.

The steam distillation method used in the present invention is a method of cooling the steam by gradually increasing the temperature at a low temperature to generate steam.

All matters mentioned in the perfume composition of the present invention and the method for producing perfume comprising the same are equally applied as long as they do not contradict each other.

Advantages and features of the present invention, and methods for achieving them, will become apparent with reference to the embodiments described below in detail. However, the present invention is not limited to the embodiments disclosed below, but may be implemented in various different forms, and only the embodiments allow the disclosure of the present invention to be complete, and common knowledge in the technical field to which the present invention pertains It is provided to fully inform those who have the scope of the invention, and the present invention is only defined by the scope of the claims.

The reagents and solvents mentioned below were purchased from Sigma-Aldrich Korea, unless otherwise specified.

Preparation Example 1. Preparation of lavender extract 1

The commercially available lavender petals were dried and extracted using water at 100° C. to prepare a lavender extract. Water was added 10 times relative to the dry weight of the used lavender petals.

Preparation Example 2. Preparation of lavender extract 2

The commercially available lavender petals were dried and extracted using 50% methanol (v/v) at 80° C. to prepare a lavender extract. 50% methanol (v/v) was added 10 times relative to the dry weight of the used lavender petals.

Preparation Example 3. Preparation of lavender extract 3

The commercially available lavender petals were dried and extracted using 30% ethanol (v/v) at 85° C. to prepare a lavender extract. 30% ethanol (v/v) was added 10 times relative to the dry weight of the used lavender petals.

Preparation Example 4. Preparation of lavender extract 4

The commercially available lavender petals were dried and extracted using 70% ethanol (v/v) at 80° C. to prepare a lavender extract. 70% ethanol (v/v) was added 10 times relative to the dry weight of the used lavender petals.

Example. perfume manufacturing

Perfume containing the ingredients described in [Table 1] in parts by weight was prepared.

[Table 1]

experimental example. sensory experiment

For sensory analysis of the perfumes prepared in Examples 1 to 5, 5 experimenters selected non-specifically from among perfume experts were requested to analyze the scent. When the five experimenters sensory-evaluated the perfume prepared in Examples 1 to 5, it was determined as sweet, soft, animalic, earthy, green, floral, and warm.

From the above description, those skilled in the art to which the present invention pertains will understand that the present invention may be implemented in other specific forms without changing the technical spirit or essential characteristics thereof. In this regard, it should be understood that the embodiments described above are illustrative in all respects and not restrictive.

Claims (5)

A perfume composition comprising:
with respect to the total weight of the perfume composition,
Lavender extract 1 to 5 parts by weight, essential oil (essential oil) 1 to 15 parts by weight, aroma oil 1 to 10 parts by weight, baby powder 1 to 5 parts by weight, purified water 15 to 40 parts by weight, and vegetable anhydrous ethanol 50 to 80 parts by weight; including,
The essential oil is at least one selected from the group consisting of cypress, pine, citron, grapefruit and fir oil,
The fir oil is 30 to 40% by weight of bornyl acetate, 10 to 30% by weight of α-β-pinene (α-β-pinene), 10 to 25% by weight of camphene, 1 to 7% by weight of santene, 2 to 7% by weight of borneol; and 1 to 5% by weight of bisabolol,
The aroma oil is at least one selected from the group consisting of sweet orange oil, creeping rosemary oil, cinnamon oil, peppermint oil and lavender oil,
The sweet orange oil contains 95 to 98% limonene,
The peppermint oil comprises 40 to 65% by weight of menthol, 15 to 30% by weight of menthone; and 5 to 12% by weight of 1.8 cieole,
The lavender oil is 40 to 60% by weight of linalyl acetate (linaly acetate); and 40 to 60% by weight of linalool. delete delete delete A perfume manufacturing method, characterized in that the perfume composition according to claim 1 is prepared by steam distillation.

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