KR102072651B1 - 핸드 블렌더의 사용이 없는 수제 물비누 페이스트의 제조방법 - Google Patents
핸드 블렌더의 사용이 없는 수제 물비누 페이스트의 제조방법 Download PDFInfo
- Publication number
- KR102072651B1 KR102072651B1 KR1020190095028A KR20190095028A KR102072651B1 KR 102072651 B1 KR102072651 B1 KR 102072651B1 KR 1020190095028 A KR1020190095028 A KR 1020190095028A KR 20190095028 A KR20190095028 A KR 20190095028A KR 102072651 B1 KR102072651 B1 KR 102072651B1
- Authority
- KR
- South Korea
- Prior art keywords
- oil
- alcohol
- paste
- water
- caustic solution
- Prior art date
- Legal status (The legal status is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the status listed.)
- Active
Links
- XLYOFNOQVPJJNP-UHFFFAOYSA-N water Substances O XLYOFNOQVPJJNP-UHFFFAOYSA-N 0.000 title claims abstract description 81
- 239000000344 soap Substances 0.000 title claims abstract description 51
- 238000004519 manufacturing process Methods 0.000 title claims abstract description 20
- KWYUFKZDYYNOTN-UHFFFAOYSA-M Potassium hydroxide Chemical compound [OH-].[K+] KWYUFKZDYYNOTN-UHFFFAOYSA-M 0.000 claims abstract description 72
- LFQSCWFLJHTTHZ-UHFFFAOYSA-N Ethanol Chemical compound CCO LFQSCWFLJHTTHZ-UHFFFAOYSA-N 0.000 claims abstract description 63
- 238000007127 saponification reaction Methods 0.000 claims abstract description 52
- 239000003518 caustics Substances 0.000 claims abstract description 51
- 238000000034 method Methods 0.000 claims abstract description 43
- 235000000346 sugar Nutrition 0.000 claims abstract description 42
- 239000008213 purified water Substances 0.000 claims abstract description 25
- 238000010438 heat treatment Methods 0.000 claims abstract description 12
- 239000003054 catalyst Substances 0.000 claims description 24
- 235000019198 oils Nutrition 0.000 description 51
- 239000003921 oil Substances 0.000 description 50
- 239000000243 solution Substances 0.000 description 37
- 238000003756 stirring Methods 0.000 description 11
- HEMHJVSKTPXQMS-UHFFFAOYSA-M Sodium hydroxide Chemical compound [OH-].[Na+] HEMHJVSKTPXQMS-UHFFFAOYSA-M 0.000 description 9
- 239000000203 mixture Substances 0.000 description 9
- 229920001296 polysiloxane Polymers 0.000 description 9
- 239000003925 fat Substances 0.000 description 7
- 235000019197 fats Nutrition 0.000 description 7
- 239000004359 castor oil Substances 0.000 description 6
- 235000019438 castor oil Nutrition 0.000 description 6
- 230000000052 comparative effect Effects 0.000 description 6
- ZEMPKEQAKRGZGQ-XOQCFJPHSA-N glycerol triricinoleate Natural products CCCCCC[C@@H](O)CC=CCCCCCCCC(=O)OC[C@@H](COC(=O)CCCCCCCC=CC[C@@H](O)CCCCCC)OC(=O)CCCCCCCC=CC[C@H](O)CCCCCC ZEMPKEQAKRGZGQ-XOQCFJPHSA-N 0.000 description 6
- 239000003240 coconut oil Substances 0.000 description 5
- 235000019864 coconut oil Nutrition 0.000 description 5
- 239000007787 solid Substances 0.000 description 5
- 238000001879 gelation Methods 0.000 description 4
- 239000000463 material Substances 0.000 description 4
- 238000002156 mixing Methods 0.000 description 4
- 239000000828 canola oil Substances 0.000 description 3
- 235000019519 canola oil Nutrition 0.000 description 3
- 230000001939 inductive effect Effects 0.000 description 3
- 239000004006 olive oil Substances 0.000 description 3
- 235000008390 olive oil Nutrition 0.000 description 3
- 239000000126 substance Substances 0.000 description 3
- 230000008961 swelling Effects 0.000 description 3
- 125000000391 vinyl group Chemical group [H]C([*])=C([H])[H] 0.000 description 3
- 229920002554 vinyl polymer Polymers 0.000 description 3
- 235000004443 Ricinus communis Nutrition 0.000 description 2
- CZMRCDWAGMRECN-UGDNZRGBSA-N Sucrose Chemical compound O[C@H]1[C@H](O)[C@@H](CO)O[C@@]1(CO)O[C@@H]1[C@H](O)[C@@H](O)[C@H](O)[C@@H](CO)O1 CZMRCDWAGMRECN-UGDNZRGBSA-N 0.000 description 2
- 239000010495 camellia oil Substances 0.000 description 2
- 235000014113 dietary fatty acids Nutrition 0.000 description 2
- 239000000194 fatty acid Substances 0.000 description 2
- 229930195729 fatty acid Natural products 0.000 description 2
- 150000004665 fatty acids Chemical class 0.000 description 2
- 239000008149 soap solution Substances 0.000 description 2
- 235000015112 vegetable and seed oil Nutrition 0.000 description 2
- AJBZENLMTKDAEK-UHFFFAOYSA-N 3a,5a,5b,8,8,11a-hexamethyl-1-prop-1-en-2-yl-1,2,3,4,5,6,7,7a,9,10,11,11b,12,13,13a,13b-hexadecahydrocyclopenta[a]chrysene-4,9-diol Chemical compound CC12CCC(O)C(C)(C)C1CCC(C1(C)CC3O)(C)C2CCC1C1C3(C)CCC1C(=C)C AJBZENLMTKDAEK-UHFFFAOYSA-N 0.000 description 1
- 235000003880 Calendula Nutrition 0.000 description 1
- 240000001432 Calendula officinalis Species 0.000 description 1
- 244000025254 Cannabis sativa Species 0.000 description 1
- 235000012766 Cannabis sativa ssp. sativa var. sativa Nutrition 0.000 description 1
- 235000012765 Cannabis sativa ssp. sativa var. spontanea Nutrition 0.000 description 1
- 239000004166 Lanolin Substances 0.000 description 1
- 240000002853 Nelumbo nucifera Species 0.000 description 1
- 235000006508 Nelumbo nucifera Nutrition 0.000 description 1
- 235000006510 Nelumbo pentapetala Nutrition 0.000 description 1
- 235000019482 Palm oil Nutrition 0.000 description 1
- OAICVXFJPJFONN-UHFFFAOYSA-N Phosphorus Chemical compound [P] OAICVXFJPJFONN-UHFFFAOYSA-N 0.000 description 1
- 244000018633 Prunus armeniaca Species 0.000 description 1
- 235000009827 Prunus armeniaca Nutrition 0.000 description 1
- 235000019774 Rice Bran oil Nutrition 0.000 description 1
- 229930006000 Sucrose Natural products 0.000 description 1
- 244000269722 Thea sinensis Species 0.000 description 1
- 235000018936 Vitellaria paradoxa Nutrition 0.000 description 1
- 241001135917 Vitellaria paradoxa Species 0.000 description 1
- 239000000654 additive Substances 0.000 description 1
- 235000009120 camo Nutrition 0.000 description 1
- 235000005607 chanvre indien Nutrition 0.000 description 1
- 238000006243 chemical reaction Methods 0.000 description 1
- 238000007796 conventional method Methods 0.000 description 1
- 238000001816 cooling Methods 0.000 description 1
- 235000008524 evening primrose extract Nutrition 0.000 description 1
- 239000010475 evening primrose oil Substances 0.000 description 1
- 229940089020 evening primrose oil Drugs 0.000 description 1
- 239000010685 fatty oil Substances 0.000 description 1
- 238000000855 fermentation Methods 0.000 description 1
- 230000004151 fermentation Effects 0.000 description 1
- 235000021552 granulated sugar Nutrition 0.000 description 1
- 239000008169 grapeseed oil Substances 0.000 description 1
- 235000009569 green tea Nutrition 0.000 description 1
- 239000011487 hemp Substances 0.000 description 1
- 125000002887 hydroxy group Chemical group [H]O* 0.000 description 1
- 229940119170 jojoba wax Drugs 0.000 description 1
- 235000019388 lanolin Nutrition 0.000 description 1
- 229940039717 lanolin Drugs 0.000 description 1
- -1 lard Substances 0.000 description 1
- 239000007788 liquid Substances 0.000 description 1
- 235000013575 mashed potatoes Nutrition 0.000 description 1
- 239000011259 mixed solution Substances 0.000 description 1
- 238000012986 modification Methods 0.000 description 1
- 230000004048 modification Effects 0.000 description 1
- 230000003020 moisturizing effect Effects 0.000 description 1
- 238000006386 neutralization reaction Methods 0.000 description 1
- 239000003960 organic solvent Substances 0.000 description 1
- 239000002540 palm oil Substances 0.000 description 1
- 239000011574 phosphorus Substances 0.000 description 1
- 229910052698 phosphorus Inorganic materials 0.000 description 1
- 230000000704 physical effect Effects 0.000 description 1
- 238000002360 preparation method Methods 0.000 description 1
- 239000008165 rice bran oil Substances 0.000 description 1
- 235000003441 saturated fatty acids Nutrition 0.000 description 1
- 150000004671 saturated fatty acids Chemical class 0.000 description 1
- 150000003333 secondary alcohols Chemical class 0.000 description 1
- 229940057910 shea butter Drugs 0.000 description 1
- 235000015096 spirit Nutrition 0.000 description 1
- 235000020238 sunflower seed Nutrition 0.000 description 1
- 150000004670 unsaturated fatty acids Chemical class 0.000 description 1
- 235000021122 unsaturated fatty acids Nutrition 0.000 description 1
- 238000010792 warming Methods 0.000 description 1
Images
Classifications
-
- C—CHEMISTRY; METALLURGY
- C11—ANIMAL OR VEGETABLE OILS, FATS, FATTY SUBSTANCES OR WAXES; FATTY ACIDS THEREFROM; DETERGENTS; CANDLES
- C11D—DETERGENT COMPOSITIONS; USE OF SINGLE SUBSTANCES AS DETERGENTS; SOAP OR SOAP-MAKING; RESIN SOAPS; RECOVERY OF GLYCEROL
- C11D9/00—Compositions of detergents based essentially on soap
- C11D9/04—Compositions of detergents based essentially on soap containing compounding ingredients other than soaps
- C11D9/22—Organic compounds, e.g. vitamins
- C11D9/26—Organic compounds, e.g. vitamins containing oxygen
-
- C—CHEMISTRY; METALLURGY
- C11—ANIMAL OR VEGETABLE OILS, FATS, FATTY SUBSTANCES OR WAXES; FATTY ACIDS THEREFROM; DETERGENTS; CANDLES
- C11D—DETERGENT COMPOSITIONS; USE OF SINGLE SUBSTANCES AS DETERGENTS; SOAP OR SOAP-MAKING; RESIN SOAPS; RECOVERY OF GLYCEROL
- C11D11/00—Special methods for preparing compositions containing mixtures of detergents
- C11D11/0094—Process for making liquid detergent compositions, e.g. slurries, pastes or gels
-
- C—CHEMISTRY; METALLURGY
- C11—ANIMAL OR VEGETABLE OILS, FATS, FATTY SUBSTANCES OR WAXES; FATTY ACIDS THEREFROM; DETERGENTS; CANDLES
- C11D—DETERGENT COMPOSITIONS; USE OF SINGLE SUBSTANCES AS DETERGENTS; SOAP OR SOAP-MAKING; RESIN SOAPS; RECOVERY OF GLYCEROL
- C11D13/00—Making of soap or soap solutions in general; Apparatus therefor
- C11D13/02—Boiling soap; Refining
- C11D13/04—Continuous methods therefor
-
- C—CHEMISTRY; METALLURGY
- C11—ANIMAL OR VEGETABLE OILS, FATS, FATTY SUBSTANCES OR WAXES; FATTY ACIDS THEREFROM; DETERGENTS; CANDLES
- C11D—DETERGENT COMPOSITIONS; USE OF SINGLE SUBSTANCES AS DETERGENTS; SOAP OR SOAP-MAKING; RESIN SOAPS; RECOVERY OF GLYCEROL
- C11D9/00—Compositions of detergents based essentially on soap
- C11D9/02—Compositions of detergents based essentially on soap on alkali or ammonium soaps
-
- C—CHEMISTRY; METALLURGY
- C11—ANIMAL OR VEGETABLE OILS, FATS, FATTY SUBSTANCES OR WAXES; FATTY ACIDS THEREFROM; DETERGENTS; CANDLES
- C11D—DETERGENT COMPOSITIONS; USE OF SINGLE SUBSTANCES AS DETERGENTS; SOAP OR SOAP-MAKING; RESIN SOAPS; RECOVERY OF GLYCEROL
- C11D9/00—Compositions of detergents based essentially on soap
- C11D9/04—Compositions of detergents based essentially on soap containing compounding ingredients other than soaps
- C11D9/22—Organic compounds, e.g. vitamins
- C11D9/26—Organic compounds, e.g. vitamins containing oxygen
- C11D9/262—Organic compounds, e.g. vitamins containing oxygen containing carbohydrates
Landscapes
- Chemical & Material Sciences (AREA)
- Life Sciences & Earth Sciences (AREA)
- Engineering & Computer Science (AREA)
- Chemical Kinetics & Catalysis (AREA)
- Oil, Petroleum & Natural Gas (AREA)
- Wood Science & Technology (AREA)
- Organic Chemistry (AREA)
- Health & Medical Sciences (AREA)
- Emergency Medicine (AREA)
- Molecular Biology (AREA)
- Detergent Compositions (AREA)
Abstract
Description
도 2는 본 발명의 제2 실시예에 의한 수제 물비누 페이스트의 제조방법을 나타낸 순서도이다.
도 3은 본 발명의 제3 실시예에 의한 수제 물비누 페이스트의 제조방법을 나타낸 순서도이다.
Claims (6)
- 수산화칼륨(KOH)을 정제수에 녹여 65~75℃의 가성 용액을 준비하는 단계와,
오일을 65~75℃로 가열하는 단계와,
상기 가열된 오일에 상기 준비된 가성 용액을 첨가하는 단계와,
상기 가성 용액이 첨가된 오일에 촉매제인 알코올을 첨가하여 트레이스를 내지 않고 비누화하는 단계와,
상기 비누화된 페이스트에 설탕물을 첨가하는 단계를 포함하며,
상기 알코올의 사용량은,
상기 오일 100중량부에 대하여 10~20중량부인 것을 특징으로 하는 핸드 블렌더의 사용이 없는 수제 물비누 페이스트의 제조방법.
- 제1항에 있어서,
상기 가성 용액이 첨가된 오일에 촉매제인 알코올을 첨가하여 비누화하는 단계는,
상기 가성 용액이 첨가된 오일에 촉매제인 알코올을 1차 첨가하여 1차 비누화하는 과정과,
상기 1차 비누화된 페이스트에 촉매제인 알코올을 2차 첨가하여 2차 비누화하는 과정을 포함하며,
상기 알코올의 사용량은,
상기 오일 100중량부에 대하여 1차 첨가 알코올 5~10중량부, 2차 첨가 알코올 5~10중량부인 것을 특징으로 하는 핸드 블렌더의 사용이 없는 수제 물비누 페이스트의 제조방법.
- 수산화칼륨을 정제수에 녹여 가성 용액을 준비하는 단계와,
상기 준비된 가성 용액에 촉매제인 알코올을 첨가하고, 65~75℃로 온도를 맞
춰주는 단계와,
오일을 65~75℃로 가열하는 단계와,
상기 가열된 오일에 상기 알코올이 첨가된 가성 용액을 첨가하여 트레이스를 내지 않고 비누화하는 단계와,
상기 비누화된 페이스트에 설탕물을 첨가하는 단계를 포함하며,
상기 알코올의 사용량은,
상기 오일 100중량부에 대하여 10~20중량부인 것을 특징으로 하는 핸드 블렌더의 사용이 없는 수제 물비누 페이스트의 제조방법.
- 삭제
- 제1항 내지 제3항 중 어느 한 항에 있어서,
상기 알코올은,
무수 에탄올 또는 발효 주정인 것을 특징으로 하는 핸드 블렌더의 사용이 없는 수제 물비누 페이스트의 제조방법.
- 제1항 내지 제3항 중 어느 한 항에 있어서,
상기 설탕물은,
설탕을 정제수에 녹여 가열한 것으로,
상기 설탕의 사용량은,
상기 오일 100중량부에 대하여 9~11중량부인 것을 특징으로 하는 핸드 블렌더의 사용이 없는 수제 물비누 페이스트의 제조방법.
Priority Applications (1)
Application Number | Priority Date | Filing Date | Title |
---|---|---|---|
KR1020190095028A KR102072651B1 (ko) | 2019-08-05 | 2019-08-05 | 핸드 블렌더의 사용이 없는 수제 물비누 페이스트의 제조방법 |
Applications Claiming Priority (1)
Application Number | Priority Date | Filing Date | Title |
---|---|---|---|
KR1020190095028A KR102072651B1 (ko) | 2019-08-05 | 2019-08-05 | 핸드 블렌더의 사용이 없는 수제 물비누 페이스트의 제조방법 |
Publications (1)
Publication Number | Publication Date |
---|---|
KR102072651B1 true KR102072651B1 (ko) | 2020-02-03 |
Family
ID=69627054
Family Applications (1)
Application Number | Title | Priority Date | Filing Date |
---|---|---|---|
KR1020190095028A Active KR102072651B1 (ko) | 2019-08-05 | 2019-08-05 | 핸드 블렌더의 사용이 없는 수제 물비누 페이스트의 제조방법 |
Country Status (1)
Country | Link |
---|---|
KR (1) | KR102072651B1 (ko) |
Cited By (1)
Publication number | Priority date | Publication date | Assignee | Title |
---|---|---|---|---|
KR102172002B1 (ko) * | 2020-08-20 | 2020-10-30 | 주식회사 코빅스 | 식물성 오일을 이용한 천연 물비누의 제조방법 및 이에 의해 제조된 천연 물비누 |
Citations (5)
Publication number | Priority date | Publication date | Assignee | Title |
---|---|---|---|---|
KR20070058782A (ko) * | 2005-12-05 | 2007-06-11 | 천병익 | 천연 비누 및 그 제조 방법 |
KR20070063081A (ko) | 2005-12-14 | 2007-06-19 | 황영규 | 천연원료를 이용한 물비누의 제조방법 |
KR101213619B1 (ko) | 2010-11-19 | 2012-12-18 | 김민우 | 물비누 제조방법 |
KR20150066188A (ko) * | 2013-12-06 | 2015-06-16 | 구동회 | 천연 미용액상비누의 제조방법 |
KR20170094573A (ko) | 2016-02-11 | 2017-08-21 | 대전대학교 산학협력단 | 새싹을 이용한 물비누의 제조방법 |
-
2019
- 2019-08-05 KR KR1020190095028A patent/KR102072651B1/ko active Active
Patent Citations (5)
Publication number | Priority date | Publication date | Assignee | Title |
---|---|---|---|---|
KR20070058782A (ko) * | 2005-12-05 | 2007-06-11 | 천병익 | 천연 비누 및 그 제조 방법 |
KR20070063081A (ko) | 2005-12-14 | 2007-06-19 | 황영규 | 천연원료를 이용한 물비누의 제조방법 |
KR101213619B1 (ko) | 2010-11-19 | 2012-12-18 | 김민우 | 물비누 제조방법 |
KR20150066188A (ko) * | 2013-12-06 | 2015-06-16 | 구동회 | 천연 미용액상비누의 제조방법 |
KR20170094573A (ko) | 2016-02-11 | 2017-08-21 | 대전대학교 산학협력단 | 새싹을 이용한 물비누의 제조방법 |
Non-Patent Citations (1)
Title |
---|
네이버 블로그, "천연비누의 종류 HP (고온법)" (2012.10.08.) https://blog.naver.com/audtjs6/130148905678* * |
Cited By (1)
Publication number | Priority date | Publication date | Assignee | Title |
---|---|---|---|---|
KR102172002B1 (ko) * | 2020-08-20 | 2020-10-30 | 주식회사 코빅스 | 식물성 오일을 이용한 천연 물비누의 제조방법 및 이에 의해 제조된 천연 물비누 |
Similar Documents
Publication | Publication Date | Title |
---|---|---|
KR910005994B1 (ko) | 투명비누의 연속 제조방법 | |
CN107594047A (zh) | 耐热巧克力组合物 | |
JPS61174300A (ja) | 固形化粧石鹸 | |
KR102072651B1 (ko) | 핸드 블렌더의 사용이 없는 수제 물비누 페이스트의 제조방법 | |
CN106189299A (zh) | 一种废旧轮胎胶粉改性沥青的制备方法 | |
HUP0401152A2 (hu) | Detergens készítmény és eljárás előállítására | |
US5284598A (en) | Process for making mild, detergent-soap, toilet bars and the bar resulting therefrom | |
JP2000503697A (ja) | 高ラウレートカノラ(canola)油をベースとする脂肪酸から製造された石鹸 | |
CN104312786A (zh) | 一种天然植物香皂及其制备方法 | |
CN105331757B (zh) | 一种皮革加脂剂 | |
KR20140035610A (ko) | 액상 비누 제조방법 | |
KR20170057207A (ko) | 재성형 기능을 갖는 피부저자극 공작용 비누클레이의 제조방법 | |
US1500276A (en) | Compounding vehicle or base | |
CN104543032B (zh) | 低热量、低饱和脂的奶油生产方法 | |
CN113881717A (zh) | 结构油脂的制备方法、由该方法制备的结构油脂 | |
CN103815104B (zh) | 一种利用化学酯交换法制备类可可脂的方法 | |
KR102150892B1 (ko) | 투명비누 제조방법 | |
TWI680962B (zh) | 碘化脂肪酸乙酯的製備方法 | |
JP2014193992A (ja) | 油リッチな固体石鹸 | |
US2087267A (en) | Process of manufacturing soap | |
WO2006079856A1 (en) | Procedure of making of transparent soap from olive oil with essential-oil admixtures | |
JP6480671B2 (ja) | 気泡含有黒糖およびその製造方法 | |
SU975767A1 (ru) | Способ получени жидких водосмываемых абразивных паст | |
KR20230131587A (ko) | 마요네즈를 이용한 천연비누 제조방법 및 그 제조방법으로 제조된 천연비누 | |
JP2015199854A (ja) | 脂肪酸マグネシウム含有石鹸組成物及びその製造方法 |
Legal Events
Date | Code | Title | Description |
---|---|---|---|
PA0109 | Patent application |
Patent event code: PA01091R01D Comment text: Patent Application Patent event date: 20190805 |
|
PA0201 | Request for examination | ||
PA0302 | Request for accelerated examination |
Patent event date: 20190805 Patent event code: PA03022R01D Comment text: Request for Accelerated Examination |
|
PE0902 | Notice of grounds for rejection |
Comment text: Notification of reason for refusal Patent event date: 20190829 Patent event code: PE09021S01D |
|
E701 | Decision to grant or registration of patent right | ||
PE0701 | Decision of registration |
Patent event code: PE07011S01D Comment text: Decision to Grant Registration Patent event date: 20200121 |
|
GRNT | Written decision to grant | ||
PR0701 | Registration of establishment |
Comment text: Registration of Establishment Patent event date: 20200128 Patent event code: PR07011E01D |
|
PR1002 | Payment of registration fee |
Payment date: 20200129 End annual number: 3 Start annual number: 1 |
|
PG1601 | Publication of registration | ||
PR1001 | Payment of annual fee |
Payment date: 20230103 Start annual number: 4 End annual number: 8 |