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JPS63227697A - 粘着性グリ−ス組成物 - Google Patents

粘着性グリ−ス組成物

Info

Publication number
JPS63227697A
JPS63227697A JP62060070A JP6007087A JPS63227697A JP S63227697 A JPS63227697 A JP S63227697A JP 62060070 A JP62060070 A JP 62060070A JP 6007087 A JP6007087 A JP 6007087A JP S63227697 A JPS63227697 A JP S63227697A
Authority
JP
Japan
Prior art keywords
grease
component
oil
grease composition
parts
Prior art date
Legal status (The legal status is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the status listed.)
Granted
Application number
JP62060070A
Other languages
English (en)
Other versions
JPH0534394B2 (ja
Inventor
Shigeru Mori
滋 森
Takayuki Takahashi
孝行 高橋
Current Assignee (The listed assignees may be inaccurate. Google has not performed a legal analysis and makes no representation or warranty as to the accuracy of the list.)
Shin Etsu Chemical Co Ltd
Original Assignee
Shin Etsu Chemical Co Ltd
Priority date (The priority date is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the date listed.)
Filing date
Publication date
Application filed by Shin Etsu Chemical Co Ltd filed Critical Shin Etsu Chemical Co Ltd
Priority to JP62060070A priority Critical patent/JPS63227697A/ja
Priority to KR1019880002702A priority patent/KR930011076B1/ko
Priority to US07/169,038 priority patent/US4840739A/en
Publication of JPS63227697A publication Critical patent/JPS63227697A/ja
Publication of JPH0534394B2 publication Critical patent/JPH0534394B2/ja
Granted legal-status Critical Current

Links

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    • C10M169/00—Lubricating compositions characterised by containing as components a mixture of at least two types of ingredient selected from base-materials, thickeners or additives, covered by the preceding groups, each of these compounds being essential
    • C10M169/02—Mixtures of base-materials and thickeners
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    • C10M105/00—Lubricating compositions characterised by the base-material being a non-macromolecular organic compound
    • C10M105/08—Lubricating compositions characterised by the base-material being a non-macromolecular organic compound containing oxygen
    • C10M105/32—Esters
    • C10M105/36—Esters of polycarboxylic acids
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    • C10M2229/053—Siloxanes with specific structure containing atoms other than silicon, hydrogen, oxygen or carbon containing sulfur
    • C10M2229/0535—Siloxanes with specific structure containing atoms other than silicon, hydrogen, oxygen or carbon containing sulfur used as base material
    • C—CHEMISTRY; METALLURGY
    • C10—PETROLEUM, GAS OR COKE INDUSTRIES; TECHNICAL GASES CONTAINING CARBON MONOXIDE; FUELS; LUBRICANTS; PEAT
    • C10M—LUBRICATING COMPOSITIONS; USE OF CHEMICAL SUBSTANCES EITHER ALONE OR AS LUBRICATING INGREDIENTS IN A LUBRICATING COMPOSITION
    • C10M2229/00—Organic macromolecular compounds containing atoms of elements not provided for in groups C10M2205/00, C10M2209/00, C10M2213/00, C10M2217/00, C10M2221/00 or C10M2225/00 as ingredients in lubricant compositions
    • C10M2229/04—Siloxanes with specific structure
    • C10M2229/05—Siloxanes with specific structure containing atoms other than silicon, hydrogen, oxygen or carbon
    • C10M2229/054—Siloxanes with specific structure containing atoms other than silicon, hydrogen, oxygen or carbon containing phosphorus
    • C—CHEMISTRY; METALLURGY
    • C10—PETROLEUM, GAS OR COKE INDUSTRIES; TECHNICAL GASES CONTAINING CARBON MONOXIDE; FUELS; LUBRICANTS; PEAT
    • C10M—LUBRICATING COMPOSITIONS; USE OF CHEMICAL SUBSTANCES EITHER ALONE OR AS LUBRICATING INGREDIENTS IN A LUBRICATING COMPOSITION
    • C10M2229/00—Organic macromolecular compounds containing atoms of elements not provided for in groups C10M2205/00, C10M2209/00, C10M2213/00, C10M2217/00, C10M2221/00 or C10M2225/00 as ingredients in lubricant compositions
    • C10M2229/04—Siloxanes with specific structure
    • C10M2229/05—Siloxanes with specific structure containing atoms other than silicon, hydrogen, oxygen or carbon
    • C10M2229/054—Siloxanes with specific structure containing atoms other than silicon, hydrogen, oxygen or carbon containing phosphorus
    • C10M2229/0545—Siloxanes with specific structure containing atoms other than silicon, hydrogen, oxygen or carbon containing phosphorus used as base material
    • C—CHEMISTRY; METALLURGY
    • C10—PETROLEUM, GAS OR COKE INDUSTRIES; TECHNICAL GASES CONTAINING CARBON MONOXIDE; FUELS; LUBRICANTS; PEAT
    • C10N—INDEXING SCHEME ASSOCIATED WITH SUBCLASS C10M RELATING TO LUBRICATING COMPOSITIONS
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    • C10N2010/02—Groups 1 or 11

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  • Organic Chemistry (AREA)
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Abstract

(57)【要約】本公報は電子出願前の出願データであるた
め要約のデータは記録されません。

Description

【発明の詳細な説明】 〔産業上の利用分野〕 本発明は、粘着性グリース組成物に関する。
粘着性グリースは、粘着力を有する潤滑剤として自動車
、航空機、加熱炉コンベヤー、送風機、家電製品、事務
用機器、精密機器、計測機器等の潤滑部分に広く使用さ
れており、低温ないしは高温の厳しい条件下においても
安定な潤滑性を保たれることが要求される。
〔従来の技術〕
従来、粘着性グリースとしては次のものが知られている
。
先ず潤滑性が良好なポリブテン系の粘着性グリースがあ
る。このポリブテン系粘着性グリースには、通常のグリ
ースにポリブテンを加えて粘着力を付与したものや、ポ
リブテンをベースにして増稠剤を加えてグリース状にし
たものがあるが、潤滑性が良い反面、温度−トルク値特
性（以下、温度特性と略称）が悪いという欠点がある。
また、温度特性に優れるシリコーン系の粘着性グリース
（特公昭５３−７７６号および特公昭６０−４５２４０
号参照）があるが、このシリコーン系粘着性グリースは
潤滑性が非常に悪いという欠点がある。
さらに、ポリブテンの特性とシリコーンの特性とを活か
した粘着性グリース（特公昭５６−１６１９５号参照）
もあるが、この粘着性グリースはポリブテン系粘着性グ
リースに比べると潤滑性が劣るという欠点がある。
〔発明が解決しようとする問題点〕
本発明は、上記従来技術の欠点を解決しようとするもの
である。すなわち、潤滑性の点で優れているポリブテン
糸数の潤滑性を有しながら温度特性がポリブテン系より
も優れている高性能の粘着性グリースを提供しようとす
るものである。
ｃ問題点を解決するための手段〕 本発明の粘着性グリース組成物は、第１成分の式　　　
　　　　　　　　　　　　　　　　　Ｒ（＋ＣＨ，−Ｃ
Ｈ２−）−（−ＣＨ，−ＣＨ−←〕　　ｐ （こ＼に、Ｒはアルキル基であり、ｘ、ｙおよびｐは正
の整数である） で示されるエチレンおよびα−オレフィンの重合体（ベ
ースオイル）１００重量部と、第２成分の増稠剤５乃至
１００重量部とからなることを特徴とするグリース組成
物である。第１成分のベースオイルとしては、例えばル
ーカント（ＨＣ−２０、ＨＣ−５０、ＨＣ−１００，Ｈ
Ｃ−１５０、ＨＣ−６００、ＨＣ−２０００等）〔三井
石油化学工業■製〕が用いられるが、ルーカントＨＣ−
６００またはルーカントＨＣ−２０００が本発明用のベ
ースオイルとして好ましい。
第２成分の増稠剤としては、グリースの増稠剤として一
般的に使用される増稠剤でよく、例えば、アルミニウム
、鉛、マンガン、リチウム、プルトニウム、カルシウム
、バリウム、ストロンチウム、銅、水銀、ビスマス、ク
ロム、鉄、ニッケル等の金属石ケン類、シリカ、アルミ
ナ、酸化鉄、酸化鉛、粘土、グラファイト、カーボン等
の無機質物質、あるいはアリール尿素、フタロシアニン
、インダスレン、ポリ四フッ化エチレン等が用いられる
。このうち、リチウムステアレート、リチウムヒドロキ
システアレートまたはシリカが本発明用の増稠剤として
好ましい。また、このシリカは、表面がアルコキシシラ
ン、クロルシラン、末端に水酸基を含有するオルガノポ
リシロキサン、有機アミン化合物または有機ホウ素化合
物等で処理されたものであってもよい。
前記第１および第２成分に対して任意成分として０〜１
００重量部のオイルを添加してもよく、この任意成分の
添加オイルとして、例えばシリコーンオイル、α−オレ
フィンオリゴマーまたはジエステル油等が用いられる。
このうち、シリコーンオイルとしてはジメチルシリコー
ンオイル、メチルフェニルシリコーンオイル、α−オレ
フィン変性シリコーンオイルまたはフルオロシリコーン
オイル等があり、それぞれＫＦ９６、ＫＦ５．ＯとＫＦ
５４、ＫＦ４１２とＫＦ７２３５Ｂ、ＦＬ−１００等〔
信越化学工業■製〕があげられる。第１および第２成分
との相溶性から、シリコーンオイルの中ではα−オレフ
ィン変性シリコーンオイルが好ましい。また、α−オレ
フィンオリゴマーとしてはＰＡＯＬ　［ライオン■製］
等のオリゴマー、ジエステルオイルとしてはジオクチル
セバケート（ＤＯ３）、ジオクチ／Ｌ／７ゼレート（Ｄ
ＯＺ）、ジオクチルアジペート（ＤＯＡ）等のオイルが
あげられる。
上記任意成分としてのシリコーンオイル、α−オレフィ
ンオリゴマーおよびジエステル油は、本発明の粘着性グ
リース組成物の粘着力の強さを調整するために適宜加え
られるものであって、前述したとおりの量を第１および
第２成分に対して加えればよい。さらに、必要に応じて
酸化防止剤等の添加剤を加えてもよい。
本発明のグリース組成物は、成分原料を単に混合するか
、熱処理混合または減圧熱処理混合等を行なうことによ
って十分に混合した後、三本ロール、コロイドミル等で
さらによく混練しグリース化することにより製造される
。
〔作用〕
本発明の粘着性グリース組成物における第１成分である
コオリゴマーは、鉱油に比べ次の点で優れている。すな
わち、該コオリゴマーは温度特性および熱酸化安定性が
優れている無色透明な液体であり、流動点が低く、引火
点（２５０乃至３００℃）および発火点（３９５乃至４
１５℃）が高く化学的に安定であって金属腐食性がほと
んどない。
また、第２成分である増稠剤は、第１成分のコオリゴマ
ー中に入り込んで網目構造を形成し、外部に余分のオイ
ルもしくはグリースが流出することを防止する。第１成
分１００重量部に対してこの第２成分の量が５重量部よ
りも小さい場合には前記網目構造が十分に形成されず、
稠度が大きくなり過ぎて粘着性が十分でないグリースと
なってしまう。また、第２成分の量が第１成分１００重
量部に対して１００重量部よりも大きくなると、稠度が
極度に小さくなり、硬すぎてグリースとしては使用でき
なくなってしまう。
以下、実施例により本発明を説明する。
〔実施例〕
実施例１〜１０ ＨＣ−６００またはＨＣ−２０００をベースオイルにし
て、このベースオイル成分と種々の増稠剤、添加オイル
成分とからなる場合の本発明のグリース組成物を表−１
に示す。各グリース組成物は、成分原料をプラネタリミ
キサーで予備混合し、ついで三本ロールによって混練し
て製造した。増稠剤が処理シリカであるもの（実施例１
〜３．７．９および１０）については、この三本ロール
による混線を数回行なった。混線後、得られた本発明グ
リース組成物を軸受に塗布し、各種測定試験を行った。
（表−１を参照）。
比較例１１および１２ シリコーン系またはポリブテン系のグリースについて実
施例１〜１０と同様の試験を行った結果を表−２に示す
。
以下に各種試験の実施方法について説明する。
トルク値の測定 ４φ×８１ｍの軸（アルミニウム製）とその軸受（亜鉛
環）にグリースを塗布して最初のトルク値を初期トルク
値とし、３６０度回転１往復／ｓｅｅをもって１サイク
ルとし、５ｏサイクル後、１５０サイクル後および３０
０サイクル後のトルク値をそれぞれ測定した。
尚、トルク値測定時の軸回転数は１０ｒ、ｐ、＋ｎ、で
ある。
回転寿命試験 ４φＸ８ｍｎの軸（アルミニウム製）とその軸受（亜鉛
環）にグリースを塗布して３６０度回転１往復／ｓｅｃ
　を１サイクルとし、１０００サイクル／ｈｒのスピー
ドで焼き付きに至るまでのサイクル数について測定した
。
髪腹笹炸莢酸 ４φＸ８ｍｎの軸（アルミニウム製）とその軸受（亜鉛
環）にグリースを塗布して周囲温度を変化させ、トルク
値の測定（トルク値測定時の軸回転数は１０ｒ、ｐ、ｍ
、である）を行なった。
Ｙ１ 〔効果〕 以上、実施例および比較例から明らかなとおり、本発明
の粘着性グリース組成物は、ポリブテン系グリースと同
等の潤滑性をもちながら温度特性がポリブテン系グリー
スよりも優れており、本発明粘着性グリース組成物によ
って高性能の粘着性グリースを提供することが可能にな
った。
手続補正書 ■、　事件の表示 昭和６２年特許願第６００７０号 ２、　　発明の名称 粘着性グリース組成物 ３、　補正をする者 「自発」 ５、　　補正の対象 明細書における「■特許請求の範囲の欄、■発明の詳細
な説明の欄」および「図面」６、　　補正の内容 　１ｌ− １）明細書第１頁４行〜１０行の「特許請求の範囲」を
別紙のとおりに補正する。
２）明細書第３頁１３行〜１８行の「ｐは正の整数であ
る・・・オイルとしては、」を 「ｐはｘ／ｙ＝０．５〜２．０、（Ｘ＋ｙ）ｐ＝５ｏ〜
１５０を満たす正の整数である）で示されるエチレンと
α−オレフィンとのランダム共重合体（コオリゴマー）
１００重量部と、第２成分の増稠剤５〜１００重量部と
からなることを特徴とするグリース組成物である。本発
明における第１成分のベースオイルとしてのコオリゴマ
ーは、」と補正する。
３）明細書第４頁２行〜５行のｒＨＣ−２０００が・・
・増稠剤でよ＜、」を １’−ＨＣ−２０００が好ましい。
第２成分の増稠剤としては、グリースの増稠剤として一
般的に使用される増稠剤であればよ＜、」と補正する。
４）明細書第４頁１３行〜１６行の「このうち、・・・
表面が」を 「上記のうち、金属石ケンとしてはりチウムステアレー
ト、リチウムヒドロキシステアレートが、無機質物質と
してはシリカが本発明用の増稠剤として好ましい。また
、シリカは、その表面が」と補正する。
５）明細書第４頁２０行〜第５頁２行の「前記第１・・
・添加オイルとして、」を 「また、任意成分として第１成分１００重量部に対して
１００重量部を越えない量のオイルを添加してもよく、
この任意成分の添加オイルとしては、」と補正する。
６）明細書第７頁１３行のｒＨＣ−６００Ｊを［ルーカ
ントＨＣ−６００Ｊと補正する。
７）明細書第７頁２０行の「この三本ロール」を「この
処理シリカをベースオイルによくなじませ、十分に混じ
り合うように三本ロール」 と補正する。
８）明細書第８頁８行〜９行の「以下に・・・土ル玄釦
１に」を 「以下に各種試験の実施方法について説明する。
貝斐０皿足 ＪＩＳ　Ｋ　２２２０の測定法に準じて稠度を測定した
。
Σ水文蒐■皿尤」と補正する。
９）明細書第９頁８行の「を行なった。」を「を行なっ
た。第１図にこの結果を示す。」と補正する。
１０）添付書類として別紙の図面（第１図）を補充する
。
以上 （別紙） 特許請求の範囲 式　　　　　　　　　　　　Ｒ １１−＋ＣＨ２−ＣＨ→「子ＣＨ２−ＣＨ斧］。
（こ＼にＲはアルキル基であり、Ｘ１ｙおよびｐはｘ／
ｙ＝０．５〜２．０、（ｘ十ｙ）ｐ＝５ｏ〜１５０を満
たす正の整数である）で示される重合体１００重量部と
、増稠剤５〜１００重量部とからなることを特徴とする
粘着性グリース組成物。

Claims (1)

  1. 【特許請求の範囲】 式 ▲数式、化学式、表等があります▼ （こゝに、Ｒはアルキル基であり、ｘ、ｙおよびｐは正
    の整数である） で示される重合体１００重量部と、増稠剤５乃至１００
    重量部とからなることを特徴とする粘着性グリース組成
    物。
JP62060070A 1987-03-17 1987-03-17 粘着性グリ−ス組成物 Granted JPS63227697A (ja)

Priority Applications (3)

Application Number Priority Date Filing Date Title
JP62060070A JPS63227697A (ja) 1987-03-17 1987-03-17 粘着性グリ−ス組成物
KR1019880002702A KR930011076B1 (ko) 1987-03-17 1988-03-15 점착성 그리이스 조성물
US07/169,038 US4840739A (en) 1987-03-17 1988-03-16 Adhesive grease composition comprising a random copolymer of ethylene and an alpha-olefin

Applications Claiming Priority (1)

Application Number Priority Date Filing Date Title
JP62060070A JPS63227697A (ja) 1987-03-17 1987-03-17 粘着性グリ−ス組成物

Publications (2)

Publication Number Publication Date
JPS63227697A true JPS63227697A (ja) 1988-09-21
JPH0534394B2 JPH0534394B2 (ja) 1993-05-21

Family

ID=13131454

Family Applications (1)

Application Number Title Priority Date Filing Date
JP62060070A Granted JPS63227697A (ja) 1987-03-17 1987-03-17 粘着性グリ−ス組成物

Country Status (3)

Country Link
US (1) US4840739A (ja)
JP (1) JPS63227697A (ja)
KR (1) KR930011076B1 (ja)

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* Cited by examiner, † Cited by third party
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JPH01308497A (ja) * 1988-06-06 1989-12-13 Kyodo Yushi Kk グリース組成物
JP2006070061A (ja) * 2004-08-31 2006-03-16 Matsushita Electric Ind Co Ltd クリック部用グリース
JP4687036B2 (ja) * 2004-08-31 2011-05-25 パナソニック株式会社 クリック部用グリース
JP2016204502A (ja) * 2015-04-21 2016-12-08 株式会社ジェイテクト トラクショングリース組成物およびトラクションドライブ装置
JP2021054945A (ja) * 2019-09-30 2021-04-08 トヨタ自動車株式会社 プロペラシャフト

Also Published As

Publication number Publication date
JPH0534394B2 (ja) 1993-05-21
US4840739A (en) 1989-06-20
KR930011076B1 (ko) 1993-11-20
KR880011314A (ko) 1988-10-27

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