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JPS62275646A - Production of high-viscosity oil-in-water type emulsion - Google Patents

Production of high-viscosity oil-in-water type emulsion

Info

Publication number
JPS62275646A
JPS62275646A JP62024396A JP2439687A JPS62275646A JP S62275646 A JPS62275646 A JP S62275646A JP 62024396 A JP62024396 A JP 62024396A JP 2439687 A JP2439687 A JP 2439687A JP S62275646 A JPS62275646 A JP S62275646A
Authority
JP
Japan
Prior art keywords
water
oil
weight
emulsion
parts
Prior art date
Legal status (The legal status is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the status listed.)
Granted
Application number
JP62024396A
Other languages
Japanese (ja)
Other versions
JPH051701B2 (en
Inventor
Hiroshi Edo
江戸 博
Satoshi Kawade
川出 智
Current Assignee (The listed assignees may be inaccurate. Google has not performed a legal analysis and makes no representation or warranty as to the accuracy of the list.)
Adeka Corp
Original Assignee
Asahi Denka Kogyo KK
Priority date (The priority date is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the date listed.)
Filing date
Publication date
Application filed by Asahi Denka Kogyo KK filed Critical Asahi Denka Kogyo KK
Publication of JPS62275646A publication Critical patent/JPS62275646A/en
Publication of JPH051701B2 publication Critical patent/JPH051701B2/ja
Granted legal-status Critical Current

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  • Grain Derivatives (AREA)
  • Edible Oils And Fats (AREA)

Abstract

PURPOSE:To obtain a filling.topping material having improved heat resistance and good flavor for confectionery and good flavor, by heating an emulsion of an oily phase consisting essentially of an edible fat or oil and an aqueous phase consisting essentially of a water-soluble proteinaceous material, starch, paste and water and cooling the emulsion. CONSTITUTION:An oil-in-water type preliminary emulsion containing and aqueous phase as a continuous phase is prepared from 5-45pts.wt. oily phase consisting essentially of a natural animal or vegetable fat or oil having <7 solid fat index at 25 deg.C and <10 solid fat index at 20 deg.C or a processed fat oil thereof and 55-95pts.wt. aqueous phase consisting of an edible material containing a water-soluble simple protein complex protein or protein hydrolyzate having surface activity, starch, paste and water. The resultant emulsion is then heat-treated and, as necessary, an antioxidant, coloring matter, tasting component and assistant emulsifying agent are suitably added. Thereby the aimed emulsion, having improved heat resistance and good flavor and suitable as a filling.topping material is obtained.

Description

【発明の詳細な説明】 3、発明の詳細な説明 〔産業上の利用分野〕 本発明は、高粘性水中油型乳化物の製造法、詳しくは、
耐熱性に優れ、且つ風味が良好で、製菓・製パン用のフ
ィリング・トッピング材として好適な高粘性水中油型乳
化物を製造する方法に関する。
[Detailed Description of the Invention] 3. Detailed Description of the Invention [Field of Industrial Application] The present invention relates to a method for producing a highly viscous oil-in-water emulsion, specifically,
The present invention relates to a method for producing a highly viscous oil-in-water emulsion that has excellent heat resistance and good flavor and is suitable as a filling/topping material for confectionery and bread making.

〔従来の技術及びその問題点〕[Conventional technology and its problems]

従来、製菓、製パン分野で、生地中に包み込むフィリン
グ材や生地表面に絞り込んだりあるいは塗布したりする
トッピング材として、カスタードクリーム、フラワーペ
ースト類(以下、ペースト類と略称する)が幅広く使用
されている。上記ペースト類をフィリング材として使用
する場合は、菓子パンに代表されるように、あらかしめ
生地中に包み込んだ後焼成する方法が作業性も良いため
一般的に採用されているが、それ自体が持つ水分が、焼
成時にパン類内部で蒸発・膨張するため、焼成後、フィ
リング材とパン類内層との間に大きな空洞を作り、好ま
しくないという問題があった。
Traditionally, custard cream and flower pastes (hereinafter referred to as pastes) have been widely used in the confectionery and bread making fields as filling materials wrapped in dough and topping materials squeezed or applied onto the surface of dough. There is. When using the above-mentioned pastes as a filling material, the method of wrapping them in a rough dough and baking them, as typified by sweet bread, is generally adopted as it is easy to work with, but Since moisture evaporates and expands inside the bread during baking, a large cavity is formed between the filling material and the inner layer of the bread after baking, which is an undesirable problem.

一方、上記ペースト類をトッピング材として使用する場
合においても同様に生地表面に絞り込んだりあるいは塗
布した後焼成する方法が採用されているものの、焼成時
高温に晒されることによってトッピング材としてのペー
スト類が著しく粘度低下しそれに伴って激しくIl!I
Hするため、釜から出してしばらくすると表面の艶が消
え、細かい亀裂が無数に入り、その上水が飛散して膜を
はるため口あたりが悪く、商品価値が著しく低下すると
いう問題があった。
On the other hand, when using the above-mentioned pastes as topping materials, the method of squeezing or applying them onto the dough surface and then baking is also adopted, but the pastes as topping materials are damaged by exposure to high temperatures during baking. The viscosity decreases significantly, and Il! I
Because of this, the surface loses its luster after a while after being taken out of the pot, and there are numerous small cracks, which cause the water to scatter and form a film, resulting in a poor taste and a significant decrease in product value. Ta.

そこで、焼成時の耐熱性を付与する目的で澱粉類を極端
に増量したり、熱凝固性蛋白質を多量に添加する試みが
行われているが、澱粉類独特の餅のような口あたりとな
ったり、熱凝固性蛋白質に起因する「もそついた」口あ
たりとなるなど、風味が著しく FMなわれるといった
問題があった。
Therefore, attempts have been made to dramatically increase the amount of starch or add a large amount of heat-coagulable protein in order to impart heat resistance during baking, but these efforts have resulted in a rice cake-like mouthfeel, which is unique to starches. There were also problems with the flavor being noticeably FM-like, such as a "mushy" mouthfeel caused by heat-coagulable proteins.

上記問題を解決する目的でレンネットカゼインとリン酸
塩を添加する方法(特開昭58−212752号)があ
るが、この方法では、水に不溶性のレンネットカゼイン
を熔解させるためにリン酸塩を用いるため、食感・風味
になお不満足な点があった。
In order to solve the above problem, there is a method of adding rennet casein and phosphate (Japanese Patent Application Laid-Open No. 58-212752). However, there were still some dissatisfaction with the texture and flavor.

従って、本発明の目的は、耐熱性に優れ、且つ風味が良
好で、製菓・製パン用のフィリング・トッピング材とし
て好適な高粘性水中油型乳化物を製造する方法を堤供す
ることにある。
Therefore, an object of the present invention is to provide a method for producing a highly viscous oil-in-water emulsion that has excellent heat resistance and good flavor and is suitable as a filling/topping material for confectionery and bread making.

を問題点を解決するための手段〕 本発明は、食用油脂を主たる成分とする油相5〜45重
量部と、水溶性蛋白質素材、デンプン類、糊料、及び水
を主たる成分とする水相55〜95i111部とから、
水相を連続相とする水中油型予備乳化物を調整し、得ら
れた水中油型予備乳化物を加熱処理することにより、上
記目的を達成したものである。
[Means for Solving the Problem] The present invention provides an oil phase containing 5 to 45 parts by weight of edible fats and oils as a main component, and an aqueous phase containing a water-soluble protein material, starch, thickening material, and water as main components. From 55-95i 111 copies,
The above object was achieved by preparing an oil-in-water pre-emulsion having an aqueous phase as a continuous phase and heat-treating the obtained oil-in-water pre-emulsion.

以下、本発明の高粘性水中油型乳化物の製造法について
詳述する。尚、水溶性蛋白質素材、デンプン類及び糊料
の含有量(%)(添加量)は、水相中の割合(水相に対
する百分率)を示す。
Hereinafter, the method for producing the highly viscous oil-in-water emulsion of the present invention will be described in detail. Note that the content (%) (added amount) of the water-soluble protein material, starch, and thickening agent indicates the proportion in the aqueous phase (percentage to the aqueous phase).

本発明で用いられる食用油脂としては、天然の動植物油
脂の他、それらにエステル交換、水@添加、分別等を施
した加工油脂を単独、もしくは混合した物が用いられる
が、好ましくは常温で液体である油脂、もしくは常温で
液状を呈する油脂を主体とし、それに常温で固体を呈す
る油脂を少量混合する等したものを用いるのが良い。
The edible oils and fats used in the present invention include natural animal and vegetable oils, as well as processed oils and fats that have been subjected to transesterification, addition of water, fractionation, etc. alone or in combination, but are preferably liquid at room temperature. It is preferable to use oils and fats that are mainly composed of oils and fats that are liquid at room temperature and mixed with a small amount of oils and fats that are solid at room temperature.

上記食用油脂は、固体脂指数(SFI)が25℃で7未
満、20℃で10未満であるものが好ましい。
The above-mentioned edible fats and oils preferably have a solid fat index (SFI) of less than 7 at 25°C and less than 10 at 20°C.

また、上記食用油脂(油相)には、必要に応じて、抗酸
化剤、油溶性色素、後述する油溶性乳化剤等の/d]熔
性物性物質加することができる。
Further, /d] meltable physical substances such as antioxidants, oil-soluble pigments, and oil-soluble emulsifiers described below can be added to the edible fat (oil phase) as necessary.

本発明で用いられる水溶性蛋白質素材は、界面活性を有
する水溶性の単純蛋白質(アルブミン区分)、複合蛋白
質(糖蛋白質、リン蛋白質、核蛋白質、色素蛋白質等)
及び蛋白質の加水分解物を含んでいる食用素材で、その
例としては、獣乳、カゼイン、カゼインナトリウム、乳
脂粉乳、ホエーパウダー、卵黄・卵白及びその粉末、大
豆蛋白質及びこれらを酵素的もしくは化学的に分解後、
水抽出したもの等が挙げられ、これらを単独で用いても
良いし、2種以上を併用しても良い。
The water-soluble protein materials used in the present invention include water-soluble simple proteins (albumin class) and complex proteins (glycoproteins, phosphoproteins, nuclear proteins, chromoproteins, etc.) that have surface activity.
and edible materials containing protein hydrolysates, such as animal milk, casein, sodium caseinate, milk powder, whey powder, egg yolks, egg whites and their powders, soybean proteins, and their processing by enzymatic or chemical processing. After decomposition into
Examples include those extracted with water, and these may be used alone or in combination of two or more.

上記水溶性蛋白質素材の添加量は、水相中の水溶性蛋白
質素材に含まれている水溶性蛋白質の含有量がO,0Q
5ffi量%以上、5M量%未満、好ましくは0.05
〜3重量%になるようにするのが良い。上記水溶性蛋白
質の含有量が0.005重量%より少ないと、水中油型
乳化が不安定となり油分離が発生し易く、また5重量%
以上であると、得られた高粘度水中油型乳化物の焼成後
の食感が極めて固いものとなり、好ましくない。
The amount of the above water-soluble protein material added is such that the content of water-soluble protein contained in the water-soluble protein material in the aqueous phase is O, 0Q.
5ffi amount% or more, less than 5M amount%, preferably 0.05
It is preferable to adjust the amount to 3% by weight. If the content of the water-soluble protein is less than 0.005% by weight, oil-in-water emulsification becomes unstable and oil separation is likely to occur;
If it is more than that, the texture of the obtained high viscosity oil-in-water emulsion after baking becomes extremely hard, which is not preferable.

本発明で用いられるデンプン類としては、馬鈴薯、コメ
、コーン、フキシーコーン、甘蔗、小麦、タピオカ、小
豆、インゲン豆、ササゲ、ソラ豆及びその他の豆類等に
由来するデンプンの他に、これらのデンプンを原料とす
る、焙焼デキストリン、酵素変性デンプン、エステル化
デンプン、酸化デンプン、エーテル化デンプン、架橋デ
ンプン等の化エデンブンが挙げられ、これらを単独で用
いても良いし、2 [以上を併用しても良い。
Starches used in the present invention include starches derived from potatoes, rice, corn, fuchsia corn, cane, wheat, tapioca, adzuki beans, kidney beans, cowpeas, fava beans, and other legumes, as well as starches such as these. Examples of raw materials include chemically modified starch such as roasted dextrin, enzyme-modified starch, esterified starch, oxidized starch, etherified starch, and crosslinked starch. Also good.

上記デンプン類の添加量は、水相中のデンプン類の含有
量が2〜30重量%、好ましくは5〜20重量%、更に
好ましくは7〜15重量%になるようにするのが良い。
The amount of starch added is preferably such that the content of starch in the aqueous phase is 2 to 30% by weight, preferably 5 to 20% by weight, and more preferably 7 to 15% by weight.

上記デンプン類の含有量が2重量%より少ないと、低粘
性の水中油型乳化物となり、トッピング材又はフィリン
グ材として具備されるべき粘性及び耐熱性が得られ難く
、また30重量%より多いと、「餅」様の性状を呈し、
口の中でもそつくばかりでなく、粘度が高くなり、後述
する加熱処理が困難となるので好ましくない。
If the content of the starches is less than 2% by weight, the resulting oil-in-water emulsion will have low viscosity, making it difficult to obtain the viscosity and heat resistance required for topping or filling materials, and if the content is more than 30% by weight, , exhibits "rice cake"-like properties,
This is not preferable because it not only feels sticky in the mouth but also has a high viscosity, making it difficult to perform the heat treatment described below.

また、本発明で用いられる糊料としては、高メトキシル
ペクチン、低メトキシルペクチン等のペクチン類、ロー
カストビーンガム、キサンタンガム、カラギーナン、フ
ァーセレラン、寒天、及ヒタマリンド種子多tf1類の
中から選ばれた一種または二種以上の糊料が挙げられる
In addition, as the thickening material used in the present invention, one selected from pectins such as high methoxyl pectin and low methoxyl pectin, locust bean gum, xanthan gum, carrageenan, farcellan, agar, and tf1 type of htamarind seeds, or Two or more types of glue may be used.

上記糊料の添加量は、特に限定されないが、水相中の糊
料の含有量が0.005〜3重量%、好ましくはO,1
〜1.5重量%なるようにするのが良い。
The amount of the above-mentioned thickening agent added is not particularly limited, but the content of the thickening agent in the aqueous phase is 0.005 to 3% by weight, preferably O,1
It is preferable to adjust the amount to 1.5% by weight.

上記糊料の含有量が0.005重量%より少ないと、低
粘性の水中油型乳化物となり、トッピング材またはフィ
リング材として具備されるべき粘性及び耐熱性が得られ
難く、また3重量%より多いと、粘度が高くなり、後述
する加熱処理が困難となるので好ましくない。
If the content of the above-mentioned glue is less than 0.005% by weight, it will become a low-viscosity oil-in-water emulsion, and it will be difficult to obtain the viscosity and heat resistance required for a topping material or filling material. If the amount is too large, the viscosity becomes high and the heat treatment described below becomes difficult, which is not preferable.

本発明においては、水相に、副成分として必要に応して
、ブドウ糖、果糖、シa 1m、麦芽糖、麦芽糖水飴、
糖アルコール、デキストリン等の水溶性糖類や、食塩、
塩化カリウム、クエン酸ナトリウム、リン酸塩、グルタ
ミン酸ソーダ等の塩類や、ビーナンツ粉末、ビーナツツ
ペース、カカオパウダー、チーズパウダー、ゴマ、化ア
ン、練すアン、果汁、果肉、酸味料、調味料、香辛料、
香料等の水溶性、水分散性呈味物質を適宜組み合わせて
使用することができる。これらの副成分を使用する場合
、副成分中に水溶性蛋白質又はデンプンが含まれている
時には、水相中の水溶性蛋白質の含有量が0.005f
i量%以上、5重量%未満、またデンプンの含有量が2
〜30重量%になるように副成分を加えなければならな
い。
In the present invention, in the aqueous phase, glucose, fructose, sia 1m, maltose, maltose starch syrup,
Water-soluble sugars such as sugar alcohols and dextrins, salt,
Salts such as potassium chloride, sodium citrate, phosphate, monosodium glutamate, bean powder, bean paste, cacao powder, cheese powder, sesame seeds, bean paste, kneaded bean paste, fruit juice, pulp, acidulants, seasonings, spices,
Water-soluble and water-dispersible taste substances such as fragrances can be used in appropriate combinations. When using these subcomponents, if the subcomponents contain water-soluble protein or starch, the content of water-soluble protein in the aqueous phase should be 0.005f.
i amount% or more and less than 5% by weight, and the starch content is 2%
Sub-components should be added to ~30% by weight.

更に、本発明においては、水溶性蛋白質素材の界面活性
により食用油脂(油相)と水相の乳化を行うが、この食
用油脂と水相の乳化を更に補う目的で乳化剤を水中油型
予備乳化物全体に対して0゜01〜5重量%加えること
が好ましい。かかる乳化剤としては、グリセリン脂肪酸
エステル、ポリグリセリン脂肪酸エステル、ソルビタン
脂肪酸エステル、ショ糖脂肪酸エステル、プロピレング
リコール脂肪酸エステル、リン脂質の中から選ばれた口
重又は2種以上の食用乳化剤を使用するのが良い。
Furthermore, in the present invention, the edible oil (oil phase) and the aqueous phase are emulsified by the surface activity of the water-soluble protein material, but in order to further supplement the emulsification of the edible oil and the aqueous phase, an emulsifier is used for oil-in-water pre-emulsification. It is preferable to add 0.01 to 5% by weight based on the entire product. As such an emulsifier, it is preferable to use an edible emulsifier selected from glycerin fatty acid esters, polyglycerin fatty acid esters, sorbitan fatty acid esters, sucrose fatty acid esters, propylene glycol fatty acid esters, and phospholipids, or two or more types of edible emulsifiers. good.

これらの乳化剤の中でも、特に、m合度7以上のポリグ
リセリン脂肪酸エステル及び/又はHLB3以下のシa
 t1!脂肪酸エステルを用いると一層口溶けの良い乳
化物を得ることができる。
Among these emulsifiers, in particular, polyglycerin fatty acid esters with m degree of 7 or more and/or shea with HLB of 3 or less are used.
t1! When fatty acid ester is used, an emulsion that melts in the mouth even better can be obtained.

上記重合度7以上のポリグリセリン脂肪酸エステルとは
、グリセリン重合度7以上のポリグリセリンの、脂肪酸
エステルである。このポリグリセリン脂肪酸エステルと
しては、デカグリセリン七ノ飽和脂肪酸エステルが特に
好ましい。また、このポリグリセリン脂肪酸エステルの
構成脂肪酸としては、例えば、ミリスチン酸、バルミチ
ン酸、ステアリン酸、アラキン酸、ベヘン酸、オレイン
酸等が挙げられる。
The polyglycerin fatty acid ester having a degree of polymerization of 7 or more is a fatty acid ester of polyglycerin having a degree of glycerin polymerization of 7 or more. As the polyglycerin fatty acid ester, decaglycerin heptanosaturated fatty acid ester is particularly preferred. In addition, examples of the constituent fatty acids of this polyglycerin fatty acid ester include myristic acid, valmitic acid, stearic acid, arachidic acid, behenic acid, and oleic acid.

上記ポリグリセリン脂肪酸エステルの使用量は、高粘性
水中油型乳化物の使用目的によって適宜法められるが、
水中油型予備乳化物に対して、好ましくは0.01〜2
M量%、更に好ましくは0,1〜1重量%である。
The amount of the polyglycerol fatty acid ester used is determined as appropriate depending on the purpose of use of the high viscosity oil-in-water emulsion.
For oil-in-water preemulsions, preferably 0.01 to 2
The amount of M is %, preferably 0.1 to 1% by weight.

更に、本発明で使用するシatfA脂肪酸エステルとし
ては、ショ糖の脂肪酸エステルのうち、モノエステル含
量が30%以下で、ジ・トリエステル以上の含量が70
%以上のものである、HLB3以下のショ糖脂肪酸エス
テルが特に好ましい。
Furthermore, as the satfA fatty acid ester used in the present invention, among the fatty acid esters of sucrose, the monoester content is 30% or less, and the di-triester content is 70% or less.
% or more, sucrose fatty acid esters with an HLB of 3 or less are particularly preferred.

このようなン=1糖脂肪酸エステルは、油溶性が強く、
乳化作用とともに油脂に対して結晶防止作用を有してい
る。
Such monosaccharide fatty acid esters are highly oil-soluble;
It has an emulsifying effect and an anti-crystallization effect on fats and oils.

上記HLB3以下のショ糖脂肪酸エステルの使用量も高
粘性水中油型乳化物の使用目的によって適宜法められる
が、水中油型予備乳化物に対して、好ましくは0.01
〜2重量%、更に好ましくは0゜05〜0.5重量%で
ある。
The amount of the sucrose fatty acid ester with an HLB of 3 or less to be used is determined as appropriate depending on the purpose of use of the highly viscous oil-in-water emulsion, but it is preferably 0.01
~2% by weight, more preferably 0.05~0.5% by weight.

これらの乳化剤を使用する場合、油溶性の乳化剤は油相
に熔解させるのが良く、また水溶性の乳化剤は水相に熔
解させるのが良い。
When these emulsifiers are used, oil-soluble emulsifiers are preferably dissolved in the oil phase, and water-soluble emulsifiers are preferably dissolved in the aqueous phase.

而して、本発明の高粘性水中油型乳化物を製造するに際
しては、先ず水溶性蛋白質素材、デンプン類、糊料及び
水、更に必要に応じ、水溶性の乳化剤、呈味物質より水
相を調製し、また、食用油脂、必要に応じ、油溶性の乳
化剤、油溶性物質より油相を関製し、上記水相55〜9
5重量部と上記油相5〜45重量部とから水中油型予備
乳化物を製造する。上記油相の使用量が5重量部より少
ないと、口あたりが糊っぽくなり、また45重量部より
多いと、耐熱性が弱くなり、焼成中に沸騰するため、実
用に供しえない、また、予備乳化の方法は、バンチで行
う方法でも良いし、水相と浦和を連続的にライン中で乳
化する方法の何れでも良い。
Therefore, when producing the highly viscous oil-in-water emulsion of the present invention, first a water-soluble protein material, starch, thickening agent, and water, and if necessary, a water-soluble emulsifier and a taste substance are added to the aqueous phase. In addition, an oil phase is prepared from edible fats and oils, an oil-soluble emulsifier as necessary, and an oil-soluble substance, and the above aqueous phase 55-9 is prepared.
An oil-in-water pre-emulsion is prepared from 5 parts by weight and 5 to 45 parts by weight of the above oil phase. If the amount of the oil phase used is less than 5 parts by weight, the mouthfeel will be sticky, and if it is more than 45 parts by weight, the heat resistance will be weakened and it will boil during baking, making it unusable. The pre-emulsification method may be either a bunch method or a method of continuously emulsifying the aqueous phase and Urawa in a line.

次いで、得られた水中油型予備乳化物を好ましくは90
℃以上で加熱処理する。この加熱処理により、デンプン
類を膨潤せしめ、高粘性水中油型乳化物を得ることがで
きるのである。
Then, the obtained oil-in-water pre-emulsion is preferably heated to 90%
Heat treatment at temperatures above ℃. This heat treatment makes it possible to swell the starch and obtain a highly viscous oil-in-water emulsion.

かかる加熱処理は、市販の各種加熱装置を用いて行うこ
とができるが、このような装置としては、間接加熱方式
のものとして、例えばAPVプレート式UHT処理装置
(A、  P、 V、社m> 、c。
Such heat treatment can be carried out using various commercially available heating devices, and examples of such devices include indirect heating type devices such as APV plate type UHT processing devices (A, P, V, Co., Ltd.). ,c.

P、UHT段菌装置(クリマリイ・パンケージ社′M)
、ストルク・チューブラ−型U HT滅菌装置(ストル
ク社製)、コンサームを蚕取式UHT滅菌装五(アルフ
ァ・ラバル社製)、KRCニーター(■栗本鐵工所製)
等、また、直接加熱方式のものとしてユーベリゼーショ
ン滅菌装置(アルプラ社!31)、VT+S滅菌装置(
アルファ・ラハル社ff1) 、ラキ7−UHTfA菌
装rxt(−7ギア一社製)、パラリゼーター(パ、シ
ュ・アンド・シルケボーグ社製) 、C,P、 Vac
−11eae−UHT殺菌装置(クリマリイ・パッケー
ジ社製)、呉羽式U HT殺菌装置(呉羽エンジニアリ
ング0鴫製)等がある。
P, UHT stage bacteria device (Climaly Pancakes'M)
, Stork tubular type UHT sterilizer (manufactured by Stork), Contherm type UHT sterilizer (manufactured by Alfa Laval), KRC Neater (manufactured by Kurimoto Iron Works)
etc., as well as direct heating methods such as the Uberization sterilizer (Alpura! 31) and the VT+S sterilizer (
Alpha Rahal Co., Ltd. ff1), Raki7-UHTfA fungicide rxt (manufactured by -7 Gear Co., Ltd.), Paralyzator (manufactured by Pa, Shu & Silkeborg Co., Ltd.), C, P, Vac
-11eae-UHT sterilizer (manufactured by Kurimaly Package Co., Ltd.), Kureha-type UHT sterilizer (manufactured by Kureha Engineering Co., Ltd.), etc.

水中油型予備乳化物は、これらの加熱装置により好まし
くは90℃以上、更に好ましくは95〜150℃で、2
〜60秒程度加熱された後、適当な温度に冷却され、製
品とされる。
The oil-in-water pre-emulsion is heated by these heating devices preferably at 90°C or higher, more preferably at 95-150°C, for 2
After being heated for about 60 seconds, it is cooled to an appropriate temperature and made into a product.

〔実施例〕〔Example〕

以下に実施例を挙げ、本発明を更に詳しく説明するが、
これらの実施例は本発明を同等制限するものではない。
The present invention will be explained in more detail with reference to Examples below.
These examples are not intended to limit the invention in the same way.

実施例1 麦芽糖水飴(水分25重量%)50重量部、脱脂粉乳(
水溶性蛋白質含有量35重皿%)2重量部、リン酸架橋
デンプン8重量部、高メトキシル化ペクチン0.3 f
fi量部、ローカストビーンガム0゜2重量部、ココア
パウダー(水溶性蛋白質含有量0重量%、デンプン質含
有量25重量%)3重量部、HLBIIのシー!糖脂肪
酸エステル0.2重量部、チョコレートフレーバー0.
2重量部及び水16重量部を混合し、水相を調製した。
Example 1 50 parts by weight of maltose starch syrup (water content 25% by weight), skim milk powder (
Water-soluble protein content (35%) 2 parts by weight, phosphoric acid cross-linked starch 8 parts by weight, highly methoxylated pectin 0.3 f
fi parts, locust bean gum 0°2 parts by weight, cocoa powder (water-soluble protein content 0% by weight, starch content 25% by weight) 3 parts by weight, HLBII Sea! Sugar fatty acid ester 0.2 parts by weight, chocolate flavor 0.
2 parts by weight and 16 parts by weight of water were mixed to prepare an aqueous phase.

別に、食用大豆油15M量部と上昇融点30℃の魚硬化
油〔固体脂指数(SFI):25℃で14.20℃で2
0〕5重量部を混合し、油相〔固体脂指数(SFI):
25℃で3.5.20℃で5〕を調製した。
Separately, 15 M parts of edible soybean oil and hydrogenated fish oil with an elevated melting point of 30°C [solid fat index (SFI): 14 at 25°C, 2 at 20°C
0] 5 parts by weight, and the oil phase [solid fat index (SFI):
3 at 25°C and 5 at 20°C].

水相を60℃に加熱し、攪拌しつつ、これに60℃に加
熱した油相を少しずつ加え、水中油型に乳化させ、更に
ホモジナイザーを通して均質化処理し、水中油型予備乳
化物を得た。次いで、この水中油型予備乳化物を60℃
前後に保持しながら、呉羽式UHT殺菌装置(呉羽エン
ジニアリング■製)を用いて135℃で7秒間加熱処理
を行い、55℃に冷却して高粘性水中油型乳化物を得た
The aqueous phase was heated to 60°C, and while stirring, the oil phase heated to 60°C was added little by little to emulsify it into an oil-in-water type, and then homogenized through a homogenizer to obtain an oil-in-water pre-emulsion. Ta. Next, this oil-in-water pre-emulsion was heated to 60°C.
While holding the mixture back and forth, heat treatment was performed at 135°C for 7 seconds using a Kureha UHT sterilizer (manufactured by Kureha Engineering), and the mixture was cooled to 55°C to obtain a highly viscous oil-in-water emulsion.

このものをパイ生地上にトッピングし、200℃で12
分間焼成しても、また、パン生地で包み180℃で15
分間焼成しても、何れも形くずれは見られず、チョコレ
ート風味も良好であった。
Top this on pie dough and heat at 200℃ for 12 minutes.
Even if you bake it for a minute, you can also wrap it in bread dough and bake it at 180℃ for 15 minutes.
Even after baking for a minute, no deformation was observed and the chocolate flavor was good.

実施例2 薄力粉(水溶性蛋白質含有量1.5重量%、デンプン質
含を量70重量%)7重量部、脱脂粉乳(水溶性蛋白質
含有量35重量%)5重量部、リン酸架橋デンプン4重
量部、食塩0.9重量部、コンソメパウダー0.5mH
部、グルタミン酸ソーダ0゜4重量部、及びキサンタン
ガム0.2重量部を水66.7重量部に分散・熔解し、
水相を調製した。
Example 2 7 parts by weight of soft flour (water-soluble protein content: 1.5% by weight, starch content: 70% by weight), 5 parts by weight of skim milk powder (water-soluble protein content: 35% by weight), 4 parts by weight of phosphoric acid cross-linked starch Parts by weight, 0.9 parts by weight of salt, 0.5 mH of consommé powder
0.4 parts by weight of sodium glutamate, and 0.2 parts by weight of xanthan gum are dispersed and dissolved in 66.7 parts by weight of water,
An aqueous phase was prepared.

別ニ、食用パームオレイン〔固体脂指数(SFり:25
℃で3.20℃で9〕10重量部と食用大豆油5重量部
を混合し〔混合後の固体脂指数(SFI):25℃で2
.20℃で6)、次いで、ヨウ素lll12のグリセリ
ン脂肪酸エステル0.3m1i部を熔解し、油相を調製
した。
Another, edible palm olein [Solid fat index (SF): 25
3. At 20°C, 10 parts by weight of 9] and 5 parts by weight of edible soybean oil were mixed [solid fat index (SFI) after mixing: 2 at 25°C.
.. 6) at 20°C, then 0.3 m1 part of glycerin fatty acid ester of iodine lll12 was melted to prepare an oil phase.

水相を60℃に加熱しitsしつつ、これに60℃に加
熱した油相を少しずつ加え、水中油型に乳化させ、更に
ホモジナイザーを通して均質化処理し、水中油型予備乳
化物を得た0次いで、この水中油型予備乳化物を60℃
前後に保持しながら、呉羽式IJ)(TG菌装置を用い
て150℃で4秒間加熱処理を行い、50℃迄冷却し、
高粘性水中油型乳化物を得た。このものを食パンに塗り
、180℃で5分間焼成しても形くずれは見られず、風
味も良好であった。
While heating the aqueous phase to 60°C, the oil phase heated to 60°C was added little by little to emulsify it into an oil-in-water type, and the mixture was further homogenized through a homogenizer to obtain an oil-in-water pre-emulsion. Next, this oil-in-water pre-emulsion was heated to 60°C.
While holding it back and forth, heat treatment was performed at 150°C for 4 seconds using a Kureha style IJ (TG bacteria device), and then cooled to 50°C.
A highly viscous oil-in-water emulsion was obtained. Even when this product was spread on bread and baked at 180° C. for 5 minutes, no deformation was observed and the flavor was good.

実施例3 トマトピユーレ(水分含有量87重量%、水溶性蛋白質
含有量2%)55.6重量部、カゼインナトリウム0.
5重量部、コーンスターチ10重量部、上白糖3重量部
、食塩0.2重量部、グルタミン酸ソーダ0.2重量部
、ゴーリンクパウダー0.1重量部、カラギーナン0.
3M量部、寒天0.1重量部を混合し、水相をjlll
mした。得られた水相を50℃に加熱し、攪拌しつつ、
これに予め50℃に加熱した食用なたね油30川量部を
少しずつ加え、水中油型予備乳化物を得た。この水中油
型予備乳化物を50℃前後に保持しながら、コンサーム
掻取′iK、UHT滅菌装置(アルファ・ラバル社製)
を用いて120℃で20秒間加熱処理を行い、60℃に
冷却して高粘性水中油型乳化物を得た。このものをパイ
生地上にトッピングし、200℃で12分間焼成しても
形くずれは見られず、トマト風味も良好であった。
Example 3 Tomato puree (water content 87% by weight, water-soluble protein content 2%) 55.6 parts by weight, sodium caseinate 0.
5 parts by weight, 10 parts by weight of cornstarch, 3 parts by weight of white sugar, 0.2 parts by weight of common salt, 0.2 parts by weight of sodium glutamate, 0.1 parts by weight of GoLink powder, 0.0 parts by weight of carrageenan.
Mix 3M parts and 0.1 parts by weight of agar, and mix the aqueous phase.
I did m. The resulting aqueous phase was heated to 50°C and while stirring,
To this, 30 parts of edible rapeseed oil preheated to 50° C. was added little by little to obtain an oil-in-water pre-emulsion. While maintaining this oil-in-water pre-emulsion at around 50°C, use the Contherm scraping 'iK' and UHT sterilizer (manufactured by Alfa Laval).
The mixture was heat-treated at 120°C for 20 seconds and cooled to 60°C to obtain a highly viscous oil-in-water emulsion. Even when this product was topped on pie dough and baked at 200° C. for 12 minutes, no deformation was observed and the tomato flavor was good.

実施例4 チーズパウダー(水溶性蛋白質含有量10市量%)10
℃量部、卵白粉末2重グ部、米デンプン9重量部、食塩
0.5重量部、グルタミン酸ソーダ0.2重量部、チー
ズフレーバー0.2型口部、及びファーモレ9フ0.3
重量部を水38.5重量部に熔解・分散し、水相を調製
した。
Example 4 Cheese powder (water-soluble protein content 10% by market weight) 10
℃ weight part, egg white powder double weight part, rice starch 9 weight part, salt 0.5 weight part, sodium glutamate weight part 0.2 weight part, cheese flavor 0.2 type mouth part, and farmole 9f 0.3 weight part
Parts by weight were dissolved and dispersed in 38.5 parts by weight of water to prepare an aqueous phase.

別に、食用パームオレイン〔固体脂指数(SFl):2
5℃で3.20“Cで9〕39重量部、レシチン0.2
m1u部、β−カロチン液0. I 重量部をl昆合し
、油相を調製した。
Separately, edible palm olein [solid fat index (SFl): 2
3.20 at 5°C 9] 39 parts by weight, lecithin 0.2
m1u part, β-carotene solution 0. 1 parts by weight were combined to prepare an oil phase.

水相を70℃に加熱しつつ、これに50℃に加タハした
浦和を少しずつ加え水中油型に乳化させ、更にホモミキ
サー(特殊機化工業■!!I)にて均質化処理し、水中
油型予備乳化物を得た。次いで、この水中油型予備乳化
物を60℃前後に保持しながら、KRCニーダ−(■栗
本鐵工所製)にて、90℃で30秒間加熱処理を行い、
50℃に冷却し、高粘性水中油型乳化物を得た。このも
のをパイ生地上にトッピングし、200℃で12分間焼
成しても、また、パン生地で包み180℃で15分間焼
成しても、何れも形くずれは見られず、チーズ風味も良
好であった。
While heating the aqueous phase to 70°C, Urawa heated to 50°C was added little by little to emulsify it into an oil-in-water type, and further homogenized using a homomixer (Tokushu Kika Kogyo ■!!I). An oil-in-water pre-emulsion was obtained. Next, while maintaining this oil-in-water pre-emulsion at around 60°C, heat treatment was performed at 90°C for 30 seconds using a KRC kneader (manufactured by Kurimoto Iron Works).
It was cooled to 50°C to obtain a highly viscous oil-in-water emulsion. Even when this product was topped on pie dough and baked at 200℃ for 12 minutes, or wrapped in bread dough and baked at 180℃ for 15 minutes, it did not lose its shape and had a good cheese flavor. Ta.

実施例5 チーズパウダー(水溶性蛋白質含有量10重量%)10
重量部、ラクトアルブミン2重量部、米デンプン8重量
部、食塩0.5重量部、グルタミン酸ソーダ0.3M量
部、チーズフレーバー0.2重量部、カラギーナン0.
4151f量部、及びデカグリセリンモノステアレート
0.2重口部を水58重量部に熔解・分散し、水相を調
製した。
Example 5 Cheese powder (water-soluble protein content 10% by weight) 10
parts by weight, 2 parts by weight of lactalbumin, 8 parts by weight of rice starch, 0.5 parts by weight of salt, 0.3 parts by weight of sodium glutamate, 0.2 parts by weight of cheese flavor, 0.0 parts by weight of carrageenan.
Parts of 4151f and 0.2 parts by weight of decaglycerin monostearate were dissolved and dispersed in 58 parts by weight of water to prepare an aqueous phase.

別に、食用なたね油20重量部、β−カロチン液0.1
重量部、及びHLB lのシー!糖脂肪酸エステル0.
3重量部を混合し、油相を調製した。
Separately, 20 parts by weight of edible rapeseed oil, 0.1 part of β-carotene liquid
Weight parts, and HLB l sea! Sugar fatty acid ester 0.
3 parts by weight were mixed to prepare an oil phase.

水相を50℃に加熱しつつ、これに50℃に加熱した油
相を少しずつ加え、水中油型予備乳化物を得た。次いで
、この水中油型予備乳化物を50℃に保持しながら、コ
ンサーム掻取式UHTfA菌装置を用いて130℃で2
0秒間加熱処理を行い、75℃に冷却して高粘性水中’
nb型乳型物化物た。
While heating the aqueous phase to 50°C, the oil phase heated to 50°C was added little by little to obtain an oil-in-water pre-emulsion. Next, while maintaining this oil-in-water pre-emulsion at 50°C, it was incubated at 130°C for 2 hours using a contherm scraping type UHTfA bacteria device.
Heat treated for 0 seconds, cooled to 75°C, and poured into high viscosity water.
nb type emulsion.

このものをパン生地で包み、180℃で15分間焼成し
ても、形(ずれは見られず、チーズ風味も良好であった
Even when this product was wrapped in bread dough and baked at 180° C. for 15 minutes, no deformation was observed and the cheese flavor was good.

実施例6 カレー粉(水溶性蛋白質含有量6重量%、デンプン質含
有1it15重量%)6重量部、脱脂粉乳(水溶性蛋白
質含有量35重量%)4重量部、コーンスターチ2重量
部、薄力粉(水溶性蛋白質含有量1.5重量%、デンプ
ン賞金有量70重量%)5重量部、上白糖2重量部、食
塩1重量部、グルタミン酸ソーダ0.2重量部、ローカ
ストビーンガム0.05ii量部、及びデカグリセリン
モノバルミテ−) 0.05重量部を水46.2重量部
に溶解・分散し、水相を調製した。
Example 6 6 parts by weight of curry powder (water-soluble protein content: 6% by weight, starch content: 15% by weight), 4 parts by weight of skim milk powder (water-soluble protein content: 35% by weight), 2 parts by weight of cornstarch, soft flour (water-soluble 5 parts by weight, 2 parts by weight of white sugar, 1 part by weight of salt, 0.2 parts by weight of sodium glutamate, 0.05 parts by weight of locust bean gum, and decaglycerin monobalmite) was dissolved and dispersed in 46.2 parts by weight of water to prepare an aqueous phase.

別に、食用パームオレイン33重量部、ソルビタンモノ
ステアレート0.3 if量部、及び牛脂ステアリン酸
モノ・ジグリセライド混合物0.2重量部を混合し、油
相を調製した。
Separately, 33 parts by weight of edible palm olein, 0.3 parts by weight of sorbitan monostearate, and 0.2 parts by weight of beef tallow stearate mono-diglyceride mixture were mixed to prepare an oil phase.

水相を40℃に保持しつつ、これに60’Cに加熱した
油相を少しずつ加え、水中油型予備乳化物を得た。次い
で、この水中油型予備乳化物を45℃に保持しながら、
呉羽式UHT殺菌装置を用いて145℃で4秒間加熱処
理を行い、40℃迄冷却して高粘性水中油型乳化物を得
た。このものを食パンに塗り、180℃で2分間焼成し
ても、形くずれは見られず、カレー風味も良好であった
While maintaining the aqueous phase at 40°C, the oil phase heated to 60'C was added little by little to obtain an oil-in-water pre-emulsion. Next, while maintaining this oil-in-water pre-emulsion at 45°C,
Heat treatment was performed at 145° C. for 4 seconds using a Kureha UHT sterilizer, and the mixture was cooled to 40° C. to obtain a highly viscous oil-in-water emulsion. Even when this product was spread on bread and baked at 180°C for 2 minutes, it did not lose its shape and had a good curry flavor.

実施例7 脱脂粉乳(水溶性蛋白質含有量35重量%)6重量部、
ソルビトール30重量部、上白t’135重量部、リン
酸架橋デンプン6重量部、ペクチン0.5重量部0、及
びミルクフレーバー0.4重量部を水31.6重量部に
溶解・分散し、水相を調製した。
Example 7 Skim milk powder (water-soluble protein content 35% by weight) 6 parts by weight,
30 parts by weight of sorbitol, 135 parts by weight of Jojiro t', 6 parts by weight of phosphoric acid crosslinked starch, 0.5 parts by weight of pectin, and 0.4 parts by weight of milk flavor were dissolved and dispersed in 31.6 parts by weight of water, An aqueous phase was prepared.

別に、食用大豆油15重量部及び上昇融点30℃の魚硬
化油〔固体脂指数(SFI):25℃で14.20℃で
20)5M量部を混合したもの〔固体脂指数(SFI)
:25℃テ3.5.20℃で5〕に、HL B 2のシ
ヨ糖脂肪酸エステル0.02ffiiR及びソルビタン
モノオレート0.48ii部を溶解し、油相を調製した
Separately, a mixture of 15 parts by weight of edible soybean oil and 5 M parts of hydrogenated fish oil with an elevated melting point of 30°C [solid fat index (SFI): 14 at 25°C, 20 at 20°C] [solid fat index (SFI)
0.02 ffiiR of sucrose fatty acid ester of HL B 2 and 0.48 parts of sorbitan monooleate were dissolved in 3.5 at 25°C and 0.48 parts of sorbitan monooleate to prepare an oil phase.

水相を40℃に加熱しつつ、これに60℃に加熱した油
相を少しずつ加え、水中油型予備乳化物を得た0次いで
この水中油型予備乳化物を45℃に保持しながら、呉羽
式UHT殺菌装置を用いて130℃で4秒間加熱処理を
行い、40℃迄冷却して高粘性水中油型乳化物を得た。
While heating the aqueous phase to 40°C, the oil phase heated to 60°C was added little by little to obtain an oil-in-water pre-emulsion. Next, while maintaining this oil-in-water pre-emulsion at 45°C, Heat treatment was performed at 130° C. for 4 seconds using a Kureha UHT sterilizer, and the mixture was cooled to 40° C. to obtain a highly viscous oil-in-water emulsion.

このものをパイ生地上にトッピングしたものとフィリン
グしたものをそれぞれ200℃で12分間焼成しても、
何れも形くずれは見られず、ミルク風味も良好であった
Even if you bake this stuff on pie dough for 12 minutes at 200℃ with topping and filling,
No deformation was observed in any of them, and the milk flavor was good.

実施例8 しょうゆ(水溶性蛋白質含有量2.0重量%)35重量
部、コーンスターチ6重量部、薄力粉(水溶性蛋白質含
有ffl 1.5重量%、デンプン賞金有量70重量%
)3重口部、ラクトアルブミン0.3重量部、グルタミ
ン酸ソーダ0.1重量部、キサンタンガム0.1重量部
、デカグリセリンモノステアレ−ト0.075ffi量
部、ソルビトール(水分40%)25重量部及び水20
.425重量部を混合し、水相を調製した。
Example 8 Soy sauce (water-soluble protein content 2.0% by weight) 35 parts by weight, cornstarch 6 parts by weight, soft flour (water-soluble protein content ffl 1.5% by weight, starch content 70% by weight)
) 3 parts by weight, 0.3 parts by weight of lactalbumin, 0.1 parts by weight of sodium glutamate, 0.1 parts by weight of xanthan gum, 0.075 parts by weight of decaglycerin monostearate, 25 parts by weight of sorbitol (40% water) part and water 20
.. 425 parts by weight were mixed to prepare an aqueous phase.

水相を50′Cに加熱し、攪拌しつつ、これに60℃に
加熱した食用米油10重量部を少しずつ加え、水中油型
に乳化させ、水中油型予備乳化物を得た。この水中油型
予備乳化物をso’c前後に保持しながら、KRCニー
ダにて100′Cで15秒間加熱処理を行い、40℃に
冷却して高粘性水中油型乳化物を得た。このものを食パ
ンに塗り、180℃で5分間焼成しても、形くずれは見
られず、しょうゆ風味も良好であった。
The aqueous phase was heated to 50'C, and while stirring, 10 parts by weight of edible rice oil heated to 60C was added little by little to emulsify it into an oil-in-water type to obtain an oil-in-water type pre-emulsion. This oil-in-water preliminary emulsion was heated at 100'C for 15 seconds in a KRC kneader while being maintained at around SO'C, and then cooled to 40°C to obtain a highly viscous oil-in-water emulsion. Even when this product was spread on bread and baked at 180°C for 5 minutes, it did not lose its shape and had a good soy sauce flavor.

実施例9 ウスターソース(水溶性蛋白質含有量0.8重量%)4
0M量部、ソルビトール(水分30%)20重量部、麦
芽糖水飴10重量部、米デンプン8重量部、ラクトアル
ブミン0.12重量部、トリポリリン酸ナトリウム0.
05iffit部、ヘキサメタリン酸ナトリウム0.0
:l置部、キサンタンガム0゜03重量部、ローカスト
ビーンガム0.02ffiLfB及び水1.66重量部
を混合し、水相を調製した。
Example 9 Worcestershire sauce (water-soluble protein content 0.8% by weight) 4
0M parts, 20 parts by weight of sorbitol (30% water), 10 parts by weight of maltose syrup, 8 parts by weight of rice starch, 0.12 parts by weight of lactalbumin, 0.0 parts by weight of sodium tripolyphosphate.
05iffit part, sodium hexametaphosphate 0.0
:1 part by weight, 0.03 parts by weight of xanthan gum, 0.02 parts by weight of locust bean gum, and 1.66 parts by weight of water to prepare an aqueous phase.

別に、食用パームオレイン15重量部、食用なたね/l
i]5重量部及びHLB3以下のショ糖脂肪酸エステル
0.09宙量部を混合し、油相を調製した。
Separately, 15 parts by weight of edible palm olein, edible rapeseed/l
i] 5 parts by weight and 0.09 parts by weight of a sucrose fatty acid ester having an HLB of 3 or less were mixed to prepare an oil phase.

水相を45℃に保持しつつ、これに60℃に加熱した油
相を少しずつ加え、水中油型に乳化させ、更にホモミキ
サーにて均質化処理し、水中油型予備乳化物をiqだ。
While maintaining the aqueous phase at 45°C, add the oil phase heated to 60°C little by little to emulsify it into an oil-in-water type, and then homogenize it with a homomixer to obtain an oil-in-water pre-emulsion in iq. .

次いで、この水中油型予備乳化物を50℃前後に保持し
つつ、KRCニーグーにて102℃で6秒間加熱処理を
行い、高粘性水中油型乳化物を得た。このものをビスケ
ット生地ではさみ、200℃で15分間焼成しても、形
くずれは見られず、ソース風味も良好であった。
Next, this oil-in-water pre-emulsion was heated at 102°C for 6 seconds at KRC Negoo while being maintained at around 50°C to obtain a highly viscous oil-in-water emulsion. Even when this product was sandwiched between biscuit dough and baked at 200° C. for 15 minutes, no deformation was observed and the sauce flavor was good.

〔発明の効果〕〔Effect of the invention〕

本発明によれば、耐熱性に優れ、且つ風味が良好で、製
菓・製パン用のフィリング・ドアピング材として好′J
!it高粘性水中曲型乳化物を製造することができる。
According to the present invention, it has excellent heat resistance and good flavor, and is suitable as a filling/dooring material for confectionery and bread making.
! It is possible to produce a highly viscous bent-in-water emulsion.

Claims (11)

【特許請求の範囲】[Claims] (1)食用油脂を主たる成分とする油相5〜45重量部
と、水溶性蛋白質素材、デンプン類、糊料、及び水を主
たる成分とする水相55〜95重量部とから、水相を連
続相とする水中油型予備乳化物を調整し、得られた水中
油型予備乳化物を加熱処理することを特徴とする高粘性
水中油型乳化物の製造法。
(1) An aqueous phase is prepared from 5 to 45 parts by weight of an oil phase whose main components are edible fats and oils, and 55 to 95 parts by weight of an aqueous phase whose main components are water-soluble protein materials, starches, thickeners, and water. A method for producing a highly viscous oil-in-water emulsion, which comprises preparing an oil-in-water pre-emulsion as a continuous phase and heat-treating the obtained oil-in-water pre-emulsion.
(2)油相又は水相が、乳化剤0.01〜5重量%(水
中油型予備乳化物に対する使用量)を含有する特許請求
の範囲第(1)項記載の高粘性水中油型乳化物の製造法
(2) The high viscosity oil-in-water emulsion according to claim (1), wherein the oil phase or the aqueous phase contains 0.01 to 5% by weight of an emulsifier (amount used relative to the oil-in-water pre-emulsion). manufacturing method.
(3)乳化剤が、重合度7以上のポリグリセリン脂肪酸
エステルを含有する特許請求の範囲第(2)項記載の高
粘性水中油型乳化物の製造法。
(3) The method for producing a highly viscous oil-in-water emulsion according to claim (2), wherein the emulsifier contains a polyglycerin fatty acid ester having a degree of polymerization of 7 or more.
(4)乳化剤が、HLB3以下のショ糖脂肪酸エステル
を含有する特許請求の範囲第(2)項記載の高粘性水中
油型乳化物の製造法。
(4) The method for producing a highly viscous oil-in-water emulsion according to claim (2), wherein the emulsifier contains a sucrose fatty acid ester with an HLB of 3 or less.
(5)乳化剤の使用量が、水中油型予備乳化物に対して
0.01〜2重量%である特許請求の範囲第(3)項又
は第(4)項記載の高粘性水中油型乳化物の製造法。
(5) High viscosity oil-in-water emulsion according to claim (3) or (4), wherein the amount of emulsifier used is 0.01 to 2% by weight based on the oil-in-water pre-emulsion. How things are manufactured.
(6)食用油脂の固体脂指数(SFI)が、25℃で7
未満、20℃で10未満である特許請求の範囲第(1)
〜(5)項の何れかに記載の高粘性水中油型乳化物の製
造法。
(6) The solid fat index (SFI) of edible oil and fat is 7 at 25°C.
Claim No. (1) which is less than 10 at 20°C
A method for producing a highly viscous oil-in-water emulsion according to any one of items 1 to 5.
(7)水相が呈味物質を含有する特許請求の範囲第(1
)〜(6)項の何れかに記載の高粘性水中油型乳化物の
製造法。
(7) Claim No. 1 in which the aqueous phase contains a taste substance
) to (6).
(8)水相中の水溶性蛋白質素材に含まれている水溶性
蛋白質の含有量が、0.005重量%以上、5重量%未
満である特許請求の範囲第(1)〜(7)項の何れかに
記載の高粘性水中油型乳化物の製造法。
(8) Claims (1) to (7) in which the content of water-soluble protein contained in the water-soluble protein material in the aqueous phase is 0.005% by weight or more and less than 5% by weight. A method for producing a highly viscous oil-in-water emulsion according to any one of the above.
(9)水相中のデンプン類の含有量が2〜30重量%で
ある特許請求の範囲第(1)〜(8)項の何れかに記載
の高粘性水中油型乳化物の製造法。
(9) The method for producing a highly viscous oil-in-water emulsion according to any one of claims (1) to (8), wherein the content of starches in the aqueous phase is 2 to 30% by weight.
(10)糊料が、ペクチン類、ローカストビーンガム、
キサンタンガム、カラギーナン、ファーセレラン、寒天
、及びタマリンド種子多糖類からなる群から選ばれた一
種又は二種以上である特許請求の範囲第(1)〜(9)
項の何れかに記載の高粘性水中油型乳化物の製造法。
(10) The thickening agent is pectin, locust bean gum,
Claims Nos. (1) to (9) are one or more selected from the group consisting of xanthan gum, carrageenan, farcellan, agar, and tamarind seed polysaccharide.
A method for producing a highly viscous oil-in-water emulsion according to any one of paragraphs.
(11)加熱処理が、水中油型予備乳化物を90℃以上
に加熱することによって行われる特許請求の範囲第(1
)〜(10)項の何れかに記載の高粘性水中油型乳化物
の製造法。
(11) Claim No. 1 in which the heat treatment is performed by heating the oil-in-water pre-emulsion to 90°C or higher.
) to (10), the method for producing a highly viscous oil-in-water emulsion.
JP62024396A 1986-02-04 1987-02-04 Production of high-viscosity oil-in-water type emulsion Granted JPS62275646A (en)

Applications Claiming Priority (2)

Application Number Priority Date Filing Date Title
JP61-22619 1986-02-04
JP2261986 1986-02-04

Publications (2)

Publication Number Publication Date
JPS62275646A true JPS62275646A (en) 1987-11-30
JPH051701B2 JPH051701B2 (en) 1993-01-08

Family

ID=12087846

Family Applications (1)

Application Number Title Priority Date Filing Date
JP62024396A Granted JPS62275646A (en) 1986-02-04 1987-02-04 Production of high-viscosity oil-in-water type emulsion

Country Status (1)

Country Link
JP (1) JPS62275646A (en)

Cited By (17)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
JPH03112457A (en) * 1989-09-28 1991-05-14 Meiji Milk Prod Co Ltd Custard creams and their manufacturing method
JPH0436150A (en) * 1990-05-31 1992-02-06 Q P Corp flower paste
JP2001302694A (en) * 2000-04-14 2001-10-31 Asahi Denka Kogyo Kk Method for modifying protein and / or carbohydrate
JP2001314149A (en) * 2000-05-09 2001-11-13 Sonton Food Industry Co Ltd Filling for hollow bread and method for producing the same
JP2002101822A (en) * 2000-10-02 2002-04-09 Kanegafuchi Chem Ind Co Ltd Method for producing filling material for confectionery and bakery
JP2002171926A (en) * 2000-12-08 2002-06-18 Mitsubishi Chemicals Corp Oil-in-water emulsion
JP2002335897A (en) * 2001-02-28 2002-11-26 Asahi Denka Kogyo Kk Oil-in-water emulsion composition and method for producing the same
JP2003070431A (en) * 2001-09-04 2003-03-11 Asahi Denka Kogyo Kk Food manufacturing method
JP2005537798A (en) * 2002-09-06 2005-12-15 リッチ プロダクツ コーポレイション Cooking cream
JP2009022253A (en) * 2007-07-24 2009-02-05 Fuji Oil Co Ltd Bingham fluid composition
JP2013090602A (en) * 2011-10-26 2013-05-16 Kaneka Corp Concentrated milk-like oil-in-water emulsified oil-and-fat composition
JP2015188358A (en) * 2014-03-27 2015-11-02 株式会社Adeka Acidic flour paste
JP2015202093A (en) * 2014-04-16 2015-11-16 日清オイリオグループ株式会社 Emulsified oil-and-fat composition
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JP2016189763A (en) * 2015-03-31 2016-11-10 不二製油株式会社 Source-shaped oil-in-water type emulsion having heating resistance
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Citations (1)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
JPS58212752A (en) * 1982-06-07 1983-12-10 Asahi Denka Kogyo Kk Preparation of high-viscosity oil-in-water emulsion

Patent Citations (1)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
JPS58212752A (en) * 1982-06-07 1983-12-10 Asahi Denka Kogyo Kk Preparation of high-viscosity oil-in-water emulsion

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JPH0436150A (en) * 1990-05-31 1992-02-06 Q P Corp flower paste
JP2001302694A (en) * 2000-04-14 2001-10-31 Asahi Denka Kogyo Kk Method for modifying protein and / or carbohydrate
JP2001314149A (en) * 2000-05-09 2001-11-13 Sonton Food Industry Co Ltd Filling for hollow bread and method for producing the same
JP2002101822A (en) * 2000-10-02 2002-04-09 Kanegafuchi Chem Ind Co Ltd Method for producing filling material for confectionery and bakery
JP2002171926A (en) * 2000-12-08 2002-06-18 Mitsubishi Chemicals Corp Oil-in-water emulsion
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JP2015188358A (en) * 2014-03-27 2015-11-02 株式会社Adeka Acidic flour paste
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JPWO2015178494A1 (en) * 2014-05-22 2017-04-20 株式会社カネカ Novel edible oil-in-water paste composition
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