JPS6186951A - １，２―ジクロルエタン合成用触媒の製造方法 - Google Patents
１，２―ジクロルエタン合成用触媒の製造方法Info
- Publication number
- JPS6186951A JPS6186951A JP60203592A JP20359285A JPS6186951A JP S6186951 A JPS6186951 A JP S6186951A JP 60203592 A JP60203592 A JP 60203592A JP 20359285 A JP20359285 A JP 20359285A JP S6186951 A JPS6186951 A JP S6186951A
- Authority
- JP
- Japan
- Prior art keywords
- catalyst
- copper
- amount
- concentration
- magnesium
- Prior art date
- Legal status (The legal status is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the status listed.)
- Granted
Links
- 239000003054 catalyst Substances 0.000 title claims description 40
- 238000004519 manufacturing process Methods 0.000 title claims description 6
- 230000015572 biosynthetic process Effects 0.000 title claims description 4
- 238000003786 synthesis reaction Methods 0.000 title claims description 4
- WSLDOOZREJYCGB-UHFFFAOYSA-N 1,2-Dichloroethane Chemical compound ClCCCl WSLDOOZREJYCGB-UHFFFAOYSA-N 0.000 title description 2
- 239000010949 copper Substances 0.000 claims description 21
- 238000000034 method Methods 0.000 claims description 16
- 229910052802 copper Inorganic materials 0.000 claims description 13
- RYGMFSIKBFXOCR-UHFFFAOYSA-N Copper Chemical compound [Cu] RYGMFSIKBFXOCR-UHFFFAOYSA-N 0.000 claims description 12
- 239000011777 magnesium Substances 0.000 claims description 7
- 238000005470 impregnation Methods 0.000 claims description 6
- YMWUJEATGCHHMB-UHFFFAOYSA-N dichloromethane Substances ClCCl YMWUJEATGCHHMB-UHFFFAOYSA-N 0.000 claims description 5
- FYYHWMGAXLPEAU-UHFFFAOYSA-N Magnesium Chemical compound [Mg] FYYHWMGAXLPEAU-UHFFFAOYSA-N 0.000 claims description 4
- 229910052749 magnesium Inorganic materials 0.000 claims description 4
- 239000010410 layer Substances 0.000 claims description 2
- 239000002344 surface layer Substances 0.000 claims description 2
- TWRXJAOTZQYOKJ-UHFFFAOYSA-L Magnesium chloride Chemical compound [Mg+2].[Cl-].[Cl-] TWRXJAOTZQYOKJ-UHFFFAOYSA-L 0.000 description 8
- 238000006243 chemical reaction Methods 0.000 description 6
- VEXZGXHMUGYJMC-UHFFFAOYSA-N Hydrochloric acid Chemical compound Cl VEXZGXHMUGYJMC-UHFFFAOYSA-N 0.000 description 5
- PNEYBMLMFCGWSK-UHFFFAOYSA-N aluminium oxide Inorganic materials [O-2].[O-2].[O-2].[Al+3].[Al+3] PNEYBMLMFCGWSK-UHFFFAOYSA-N 0.000 description 5
- SCYULBFZEHDVBN-UHFFFAOYSA-N 1,1-Dichloroethane Chemical compound CC(Cl)Cl SCYULBFZEHDVBN-UHFFFAOYSA-N 0.000 description 4
- VGGSQFUCUMXWEO-UHFFFAOYSA-N Ethene Chemical compound C=C VGGSQFUCUMXWEO-UHFFFAOYSA-N 0.000 description 4
- 239000005977 Ethylene Substances 0.000 description 4
- 238000005243 fluidization Methods 0.000 description 4
- 229910001629 magnesium chloride Inorganic materials 0.000 description 4
- 239000002245 particle Substances 0.000 description 4
- 238000005259 measurement Methods 0.000 description 3
- 239000011148 porous material Substances 0.000 description 3
- 238000003756 stirring Methods 0.000 description 3
- BYFGZMCJNACEKR-UHFFFAOYSA-N aluminium(i) oxide Chemical compound [Al]O[Al] BYFGZMCJNACEKR-UHFFFAOYSA-N 0.000 description 2
- 238000004458 analytical method Methods 0.000 description 2
- 238000010438 heat treatment Methods 0.000 description 2
- 239000012071 phase Substances 0.000 description 2
- 238000002360 preparation method Methods 0.000 description 2
- 239000000376 reactant Substances 0.000 description 2
- XLYOFNOQVPJJNP-UHFFFAOYSA-N water Chemical compound O XLYOFNOQVPJJNP-UHFFFAOYSA-N 0.000 description 2
- 102100024630 Asc-type amino acid transporter 1 Human genes 0.000 description 1
- 229910021592 Copper(II) chloride Inorganic materials 0.000 description 1
- 108091006242 SLC7A10 Proteins 0.000 description 1
- 230000002411 adverse Effects 0.000 description 1
- 230000003197 catalytic effect Effects 0.000 description 1
- 239000003795 chemical substances by application Substances 0.000 description 1
- 230000006835 compression Effects 0.000 description 1
- 238000007906 compression Methods 0.000 description 1
- 238000009833 condensation Methods 0.000 description 1
- 230000005494 condensation Effects 0.000 description 1
- 238000010276 construction Methods 0.000 description 1
- ORTQZVOHEJQUHG-UHFFFAOYSA-L copper(II) chloride Chemical compound Cl[Cu]Cl ORTQZVOHEJQUHG-UHFFFAOYSA-L 0.000 description 1
- 238000005260 corrosion Methods 0.000 description 1
- 230000007797 corrosion Effects 0.000 description 1
- 239000008367 deionised water Substances 0.000 description 1
- 229910021641 deionized water Inorganic materials 0.000 description 1
- 238000004090 dissolution Methods 0.000 description 1
- 238000009826 distribution Methods 0.000 description 1
- 230000000694 effects Effects 0.000 description 1
- 238000005265 energy consumption Methods 0.000 description 1
- 239000011521 glass Substances 0.000 description 1
- 238000011065 in-situ storage Methods 0.000 description 1
- 229910052738 indium Inorganic materials 0.000 description 1
- APFVFJFRJDLVQX-UHFFFAOYSA-N indium atom Chemical compound [In] APFVFJFRJDLVQX-UHFFFAOYSA-N 0.000 description 1
- 230000010354 integration Effects 0.000 description 1
- 210000003127 knee Anatomy 0.000 description 1
- 239000000203 mixture Substances 0.000 description 1
- 239000003607 modifier Substances 0.000 description 1
- 238000004838 photoelectron emission spectroscopy Methods 0.000 description 1
- 230000005855 radiation Effects 0.000 description 1
- 150000003839 salts Chemical class 0.000 description 1
- 230000035945 sensitivity Effects 0.000 description 1
- 239000007790 solid phase Substances 0.000 description 1
- 238000001228 spectrum Methods 0.000 description 1
- 239000000126 substance Substances 0.000 description 1
- 229910001868 water Inorganic materials 0.000 description 1
Classifications
-
- B—PERFORMING OPERATIONS; TRANSPORTING
- B01—PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
- B01J—CHEMICAL OR PHYSICAL PROCESSES, e.g. CATALYSIS OR COLLOID CHEMISTRY; THEIR RELEVANT APPARATUS
- B01J27/00—Catalysts comprising the elements or compounds of halogens, sulfur, selenium, tellurium, phosphorus or nitrogen; Catalysts comprising carbon compounds
- B01J27/06—Halogens; Compounds thereof
- B01J27/08—Halides
- B01J27/10—Chlorides
-
- C—CHEMISTRY; METALLURGY
- C07—ORGANIC CHEMISTRY
- C07C—ACYCLIC OR CARBOCYCLIC COMPOUNDS
- C07C17/00—Preparation of halogenated hydrocarbons
- C07C17/093—Preparation of halogenated hydrocarbons by replacement by halogens
- C07C17/15—Preparation of halogenated hydrocarbons by replacement by halogens with oxygen as auxiliary reagent, e.g. oxychlorination
- C07C17/152—Preparation of halogenated hydrocarbons by replacement by halogens with oxygen as auxiliary reagent, e.g. oxychlorination of hydrocarbons
- C07C17/156—Preparation of halogenated hydrocarbons by replacement by halogens with oxygen as auxiliary reagent, e.g. oxychlorination of hydrocarbons of unsaturated hydrocarbons
Landscapes
- Chemical & Material Sciences (AREA)
- Organic Chemistry (AREA)
- Engineering & Computer Science (AREA)
- Materials Engineering (AREA)
- Chemical Kinetics & Catalysis (AREA)
- Organic Low-Molecular-Weight Compounds And Preparation Thereof (AREA)
- Catalysts (AREA)
- Low-Molecular Organic Synthesis Reactions Using Catalysts (AREA)
Applications Claiming Priority (2)
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| IT22717/84A IT1176719B (it) | 1984-09-19 | 1984-09-19 | Metodo per la preparazione di un catalizzatore per la sintesi di 1,2-dicloroetano |
| IT22717A/84 | 1984-09-19 |
Publications (2)
| Publication Number | Publication Date |
|---|---|
| JPS6186951A true JPS6186951A (ja) | 1986-05-02 |
| JPH0516904B2 JPH0516904B2 (it) | 1993-03-05 |
Family
ID=11199597
Family Applications (1)
| Application Number | Title | Priority Date | Filing Date |
|---|---|---|---|
| JP60203592A Granted JPS6186951A (ja) | 1984-09-19 | 1985-09-17 | １，２―ジクロルエタン合成用触媒の製造方法 |
Country Status (11)
| Country | Link |
|---|---|
| US (1) | US4871707A (it) |
| EP (1) | EP0176432B1 (it) |
| JP (1) | JPS6186951A (it) |
| AR (1) | AR241241A1 (it) |
| BR (1) | BR8504512A (it) |
| CA (1) | CA1248934A (it) |
| DE (1) | DE3564911D1 (it) |
| ES (1) | ES8708190A1 (it) |
| IT (1) | IT1176719B (it) |
| MX (1) | MX166997B (it) |
| NO (1) | NO162106C (it) |
Cited By (1)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| JP2002503536A (ja) * | 1998-01-08 | 2002-02-05 | イーヴィーシー・テクノロジー・アクチエン・ゲゼルシャフト | 触媒、その製造方法、および１，２−ジクロロエタンの合成におけるその使用 |
Families Citing this family (7)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| ES2026073A6 (es) * | 1991-01-03 | 1992-04-01 | Aiscondel Sa | Procedimiento para la preparacion de un catalizador para la oxicloracion del etileno. |
| CN1045727C (zh) * | 1994-07-05 | 1999-10-20 | 化学工业部北京化工研究院 | 流化床氧气法烃类氧氯化反应催化剂及其制造方法 |
| RU2139761C1 (ru) * | 1997-12-31 | 1999-10-20 | Институт нефтехимии и катализа АН Республики Башкортостан | Способ приготовления микросферического катализатора оксихлорирования углеводородов |
| RU2148432C1 (ru) * | 1999-04-23 | 2000-05-10 | Акционерное общество открытого типа "Катализатор" | Способ приготовления катализатора для оксихлорирования этилена в 1,2-дихлорэтан |
| ITMI20012241A1 (it) * | 2001-10-25 | 2003-04-25 | Sued Chemie Mt Srl | Catalizzatori per l'ossiclorurazione dell'etilene a 1,2-dicloroetano |
| ITMI20030630A1 (it) * | 2003-03-31 | 2004-10-01 | Sued Chemie Mt Srl | Catalizzatori per ossiclorurazione dell'etilene a 1,2-dicloroetano. |
| ITMI20042317A1 (it) * | 2004-12-02 | 2005-03-02 | Sued Chemie Mt Srl | Catalizzatori per l'ossiclorurazione dell'etilene a 1,2-dicloroetano |
Family Cites Families (8)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| NL131716C (it) * | 1962-09-01 | 1900-01-01 | ||
| US3624170A (en) * | 1966-09-16 | 1971-11-30 | Toyo Soda Mfg Co Ltd | Process for oxychlorination of ethylene |
| FR2141452B1 (it) * | 1971-06-03 | 1973-06-29 | Pechiney Saint Gobain | |
| IT1030646B (it) * | 1974-10-04 | 1979-04-10 | Sir Soc Italiana Resine Spa | Procedimento er la produzione di dicloroetano |
| US4124534A (en) * | 1976-10-20 | 1978-11-07 | Diamond Shamrock Corporation | High temperature chlorination catalyst |
| US4460699A (en) * | 1982-08-04 | 1984-07-17 | Conoco Inc. | Fixed bed catalyst for oxychlorination |
| US4495308A (en) * | 1983-03-04 | 1985-01-22 | Chevron Research Company | Two-region spherical catalysts |
| IT1163160B (it) * | 1983-03-22 | 1987-04-08 | Montepolimeri Spa | Catalizzatori supportati per la sintesi di 1-2 dicloroetano per ossiclorurazione di etilene in letto fluidizzato |
-
1984
- 1984-09-19 IT IT22717/84A patent/IT1176719B/it active
-
1985
- 1985-09-13 NO NO853595A patent/NO162106C/no not_active IP Right Cessation
- 1985-09-16 CA CA000490819A patent/CA1248934A/en not_active Expired
- 1985-09-17 AR AR85301627A patent/AR241241A1/es active
- 1985-09-17 JP JP60203592A patent/JPS6186951A/ja active Granted
- 1985-09-17 BR BR8504512A patent/BR8504512A/pt not_active IP Right Cessation
- 1985-09-18 ES ES547073A patent/ES8708190A1/es not_active Expired
- 1985-09-18 DE DE8585401807T patent/DE3564911D1/de not_active Expired
- 1985-09-18 EP EP85401807A patent/EP0176432B1/en not_active Expired
- 1985-10-01 MX MX000020A patent/MX166997B/es unknown
-
1986
- 1986-12-15 US US06/940,204 patent/US4871707A/en not_active Expired - Lifetime
Cited By (1)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| JP2002503536A (ja) * | 1998-01-08 | 2002-02-05 | イーヴィーシー・テクノロジー・アクチエン・ゲゼルシャフト | 触媒、その製造方法、および１，２−ジクロロエタンの合成におけるその使用 |
Also Published As
| Publication number | Publication date |
|---|---|
| MX166997B (es) | 1993-02-22 |
| BR8504512A (pt) | 1986-07-15 |
| EP0176432A3 (en) | 1986-06-18 |
| CA1248934A (en) | 1989-01-17 |
| EP0176432B1 (en) | 1988-09-14 |
| NO162106C (no) | 1989-11-08 |
| AR241241A1 (es) | 1992-03-31 |
| EP0176432A2 (en) | 1986-04-02 |
| IT1176719B (it) | 1987-08-18 |
| ES547073A0 (es) | 1987-10-01 |
| NO162106B (no) | 1989-07-31 |
| JPH0516904B2 (it) | 1993-03-05 |
| IT8422717A0 (it) | 1984-09-19 |
| IT8422717A1 (it) | 1986-03-19 |
| ES8708190A1 (es) | 1987-10-01 |
| NO853595L (no) | 1986-03-20 |
| DE3564911D1 (en) | 1988-10-20 |
| US4871707A (en) | 1989-10-03 |
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Legal Events
| Date | Code | Title | Description |
|---|---|---|---|
| LAPS | Cancellation because of no payment of annual fees |