JPS5669212A - Synthesis of diamond - Google Patents
Synthesis of diamondInfo
- Publication number
- JPS5669212A JPS5669212A JP14191479A JP14191479A JPS5669212A JP S5669212 A JPS5669212 A JP S5669212A JP 14191479 A JP14191479 A JP 14191479A JP 14191479 A JP14191479 A JP 14191479A JP S5669212 A JPS5669212 A JP S5669212A
- Authority
- JP
- Japan
- Prior art keywords
- seed crystal
- diamond
- crystal
- metal
- solvent
- Prior art date
- Legal status (The legal status is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the status listed.)
- Granted
Links
- 229910003460 diamond Inorganic materials 0.000 title abstract 5
- 239000010432 diamond Substances 0.000 title abstract 5
- 230000015572 biosynthetic process Effects 0.000 title 1
- 238000003786 synthesis reaction Methods 0.000 title 1
- 239000013078 crystal Substances 0.000 abstract 9
- 239000002184 metal Substances 0.000 abstract 5
- 239000002904 solvent Substances 0.000 abstract 5
- OKTJSMMVPCPJKN-UHFFFAOYSA-N Carbon Chemical compound [C] OKTJSMMVPCPJKN-UHFFFAOYSA-N 0.000 abstract 4
- 229910052799 carbon Inorganic materials 0.000 abstract 4
- 238000000034 method Methods 0.000 abstract 2
- 239000011247 coating layer Substances 0.000 abstract 1
- 238000004090 dissolution Methods 0.000 abstract 1
- 230000000694 effects Effects 0.000 abstract 1
- 230000005496 eutectics Effects 0.000 abstract 1
- 239000010410 layer Substances 0.000 abstract 1
- 150000002736 metal compounds Chemical class 0.000 abstract 1
- 150000004767 nitrides Chemical class 0.000 abstract 1
- 230000000737 periodic effect Effects 0.000 abstract 1
Classifications
-
- B—PERFORMING OPERATIONS; TRANSPORTING
- B01—PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
- B01J—CHEMICAL OR PHYSICAL PROCESSES, e.g. CATALYSIS OR COLLOID CHEMISTRY; THEIR RELEVANT APPARATUS
- B01J3/00—Processes of utilising sub-atmospheric or super-atmospheric pressure to effect chemical or physical change of matter; Apparatus therefor
- B01J3/06—Processes using ultra-high pressure, e.g. for the formation of diamonds; Apparatus therefor, e.g. moulds or dies
- B01J3/062—Processes using ultra-high pressure, e.g. for the formation of diamonds; Apparatus therefor, e.g. moulds or dies characterised by the composition of the materials to be processed
-
- B—PERFORMING OPERATIONS; TRANSPORTING
- B01—PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
- B01J—CHEMICAL OR PHYSICAL PROCESSES, e.g. CATALYSIS OR COLLOID CHEMISTRY; THEIR RELEVANT APPARATUS
- B01J2203/00—Processes utilising sub- or super atmospheric pressure
- B01J2203/06—High pressure synthesis
- B01J2203/065—Composition of the material produced
- B01J2203/0655—Diamond
-
- B—PERFORMING OPERATIONS; TRANSPORTING
- B01—PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
- B01J—CHEMICAL OR PHYSICAL PROCESSES, e.g. CATALYSIS OR COLLOID CHEMISTRY; THEIR RELEVANT APPARATUS
- B01J2203/00—Processes utilising sub- or super atmospheric pressure
- B01J2203/06—High pressure synthesis
- B01J2203/0675—Structural or physico-chemical features of the materials processed
- B01J2203/068—Crystal growth
Landscapes
- Chemical & Material Sciences (AREA)
- Organic Chemistry (AREA)
- Chemical Kinetics & Catalysis (AREA)
- Carbon And Carbon Compounds (AREA)
Abstract
PURPOSE:To prevent the dissolution of a seed crystal in a process for growing a diamond crystal in a reactor having a temperature gradient under high temperature and pressure taking advantage of the solubility difference of carbon to the solvent metal, by separating the solvent metal from the seed crystal with a covering layer composed of a specific metal compound. CONSTITUTION:A diamond seed crystal 1, a solvent metal 2 and a carbon source 3 are combined together to a unit with a pressure medium 4, and the unit is inserted into a uniaxially compressing superhigh pressure generator, and heated above the eutectic temperature of the solvent metal and carbon with a heater 5 under high pressure under which diamond exists as the stable phase, while controlling the temperature near the seed crystal 1 below that of the carbon source 3, to effect the growth of diamond crystal on the seed crystal 1. In the above process, a coating layer composed of a carbide, nitride, or carbonitride of a metal of the 4a, 5a, or 6a group of the periodic table and having a thickness of 1-50mu is formed to the interface between the seed crystal 1 and the solvent crystal 2 (or vice versa).
Priority Applications (1)
Application Number | Priority Date | Filing Date | Title |
---|---|---|---|
JP14191479A JPS5669212A (en) | 1979-11-01 | 1979-11-01 | Synthesis of diamond |
Applications Claiming Priority (1)
Application Number | Priority Date | Filing Date | Title |
---|---|---|---|
JP14191479A JPS5669212A (en) | 1979-11-01 | 1979-11-01 | Synthesis of diamond |
Publications (2)
Publication Number | Publication Date |
---|---|
JPS5669212A true JPS5669212A (en) | 1981-06-10 |
JPS6317492B2 JPS6317492B2 (en) | 1988-04-14 |
Family
ID=15303095
Family Applications (1)
Application Number | Title | Priority Date | Filing Date |
---|---|---|---|
JP14191479A Granted JPS5669212A (en) | 1979-11-01 | 1979-11-01 | Synthesis of diamond |
Country Status (1)
Country | Link |
---|---|
JP (1) | JPS5669212A (en) |
Cited By (1)
Publication number | Priority date | Publication date | Assignee | Title |
---|---|---|---|---|
JPS59164608A (en) * | 1983-03-11 | 1984-09-17 | Showa Denko Kk | Method for synthesizing diamond |
Families Citing this family (1)
Publication number | Priority date | Publication date | Assignee | Title |
---|---|---|---|---|
DE69215021T2 (en) * | 1991-02-15 | 1997-04-03 | Sumitomo Electric Industries | DIAMOND SYNTHESIS PROCEDURE |
-
1979
- 1979-11-01 JP JP14191479A patent/JPS5669212A/en active Granted
Cited By (2)
Publication number | Priority date | Publication date | Assignee | Title |
---|---|---|---|---|
JPS59164608A (en) * | 1983-03-11 | 1984-09-17 | Showa Denko Kk | Method for synthesizing diamond |
JPH0380535B2 (en) * | 1983-03-11 | 1991-12-25 | Showa Denko Kk |
Also Published As
Publication number | Publication date |
---|---|
JPS6317492B2 (en) | 1988-04-14 |
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