JPS54100323A - Preparation of organic polyisocyanate having improved long-term storage stability - Google Patents
Preparation of organic polyisocyanate having improved long-term storage stabilityInfo
- Publication number
- JPS54100323A JPS54100323A JP505378A JP505378A JPS54100323A JP S54100323 A JPS54100323 A JP S54100323A JP 505378 A JP505378 A JP 505378A JP 505378 A JP505378 A JP 505378A JP S54100323 A JPS54100323 A JP S54100323A
- Authority
- JP
- Japan
- Prior art keywords
- storage stability
- term storage
- organic polyisocyanate
- improved long
- aliphatic
- Prior art date
- Legal status (The legal status is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the status listed.)
- Granted
Links
- 230000007774 longterm Effects 0.000 title abstract 2
- 239000005056 polyisocyanate Substances 0.000 title abstract 2
- 229920001228 polyisocyanate Polymers 0.000 title abstract 2
- 125000002723 alicyclic group Chemical group 0.000 abstract 2
- 125000001931 aliphatic group Chemical group 0.000 abstract 2
- XLLIQLLCWZCATF-UHFFFAOYSA-N ethylene glycol monomethyl ether acetate Natural products COCCOC(C)=O XLLIQLLCWZCATF-UHFFFAOYSA-N 0.000 abstract 2
- 239000012046 mixed solvent Substances 0.000 abstract 2
- XLYOFNOQVPJJNP-UHFFFAOYSA-N water Substances O XLYOFNOQVPJJNP-UHFFFAOYSA-N 0.000 abstract 2
- LYCAIKOWRPUZTN-UHFFFAOYSA-N Ethylene glycol Chemical class OCCO LYCAIKOWRPUZTN-UHFFFAOYSA-N 0.000 abstract 1
- 239000005057 Hexamethylene diisocyanate Substances 0.000 abstract 1
- 229920002396 Polyurea Polymers 0.000 abstract 1
- 125000002777 acetyl group Chemical group [H]C([H])([H])C(*)=O 0.000 abstract 1
- 239000000853 adhesive Substances 0.000 abstract 1
- 230000001070 adhesive effect Effects 0.000 abstract 1
- 125000000217 alkyl group Chemical group 0.000 abstract 1
- 230000015572 biosynthetic process Effects 0.000 abstract 1
- 239000006227 byproduct Substances 0.000 abstract 1
- 239000011248 coating agent Substances 0.000 abstract 1
- 238000000576 coating method Methods 0.000 abstract 1
- 150000001875 compounds Chemical class 0.000 abstract 1
- 230000000694 effects Effects 0.000 abstract 1
- RRAMGCGOFNQTLD-UHFFFAOYSA-N hexamethylene diisocyanate Chemical compound O=C=NCCCCCCN=C=O RRAMGCGOFNQTLD-UHFFFAOYSA-N 0.000 abstract 1
- 239000000203 mixture Substances 0.000 abstract 1
- 239000003607 modifier Substances 0.000 abstract 1
- 239000000178 monomer Substances 0.000 abstract 1
- 229920000642 polymer Polymers 0.000 abstract 1
- 239000002994 raw material Substances 0.000 abstract 1
- 239000004753 textile Substances 0.000 abstract 1
- DQWPFSLDHJDLRL-UHFFFAOYSA-N triethyl phosphate Chemical compound CCOP(=O)(OCC)OCC DQWPFSLDHJDLRL-UHFFFAOYSA-N 0.000 abstract 1
- WVLBCYQITXONBZ-UHFFFAOYSA-N trimethyl phosphate Chemical compound COP(=O)(OC)OC WVLBCYQITXONBZ-UHFFFAOYSA-N 0.000 abstract 1
Landscapes
- Organic Low-Molecular-Weight Compounds And Preparation Thereof (AREA)
Abstract
PURPOSE: To obtain an organic polyisocyanate useful as a raw material for coating meterials, having improved long-term storage stability, by reacting an excess of an aliphatic, alicyclic, or aromatic aliphatic diisocyanate with water in a specific mixed solvent.
CONSTITUTION: An excess of an aliphatic, alicyclic, or aromatic aliphatic diisocyanate, e.g. hexamethylene diisocyanate, is reacted with water in a mixed solvent consisting of a combination of (a) at least one type of an ethylene glycol derivative of formula (R1 and R2 are 1W4C alkyl or acetyl groups; n is 1 or 2), e.g. ethylene glycol monomethyl ether acetate, and (b) triethyl phosphate alone or its mixture with trimethyl phosphate to give the objective compound.
EFFECT: Formation of polyurea as a byproduct is suppressed, and liberation of monomers is prevented.
USE: High polymer modifiers, textile finishes, adhesives, etc.
COPYRIGHT: (C)1979,JPO&Japio
Priority Applications (10)
Application Number | Priority Date | Filing Date | Title |
---|---|---|---|
JP505378A JPS54100323A (en) | 1978-01-20 | 1978-01-20 | Preparation of organic polyisocyanate having improved long-term storage stability |
BE185485A BE864326A (en) | 1977-03-01 | 1978-02-27 | PROCESS FOR PREPARING AN ORGANIC POLYISOCYANATE |
GB7862/78A GB1564690A (en) | 1977-03-01 | 1978-02-28 | Process for producing organic polysocyanate having good stability on long storage |
CA297,866A CA1128246A (en) | 1977-03-01 | 1978-02-28 | Process for producing organic polyisocyanate having good stability on long storage |
AR271269A AR228831A1 (en) | 1977-03-01 | 1978-02-28 | PROCEDURE FOR PREPARING AN ORGANIC POLYISOCYANATE |
IT48215/78A IT1155849B (en) | 1977-03-01 | 1978-02-28 | PROCEDURE FOR PRODUCING ORGANIC POLYISOCYANATES OF GOOD STABILITY FOR LONG STORAGE |
FR7805700A FR2382468A1 (en) | 1977-03-01 | 1978-02-28 | PROCESS FOR PREPARING AN ORGANIC POLYISOCYANATE |
CH221478A CH632489A5 (en) | 1977-03-01 | 1978-03-01 | METHOD FOR PRODUCING AN ORGANIC POLYISOCYANATE. |
DE2808801A DE2808801C3 (en) | 1977-03-01 | 1978-03-01 | Process for the preparation of an organic polyisocyanate with a long shelf life |
US05/882,466 US4176132A (en) | 1977-03-01 | 1978-03-01 | Reaction of organic diisocyanates with water |
Applications Claiming Priority (1)
Application Number | Priority Date | Filing Date | Title |
---|---|---|---|
JP505378A JPS54100323A (en) | 1978-01-20 | 1978-01-20 | Preparation of organic polyisocyanate having improved long-term storage stability |
Publications (2)
Publication Number | Publication Date |
---|---|
JPS54100323A true JPS54100323A (en) | 1979-08-08 |
JPS6126778B2 JPS6126778B2 (en) | 1986-06-21 |
Family
ID=11600648
Family Applications (1)
Application Number | Title | Priority Date | Filing Date |
---|---|---|---|
JP505378A Granted JPS54100323A (en) | 1977-03-01 | 1978-01-20 | Preparation of organic polyisocyanate having improved long-term storage stability |
Country Status (1)
Country | Link |
---|---|
JP (1) | JPS54100323A (en) |
Families Citing this family (1)
Publication number | Priority date | Publication date | Assignee | Title |
---|---|---|---|---|
JPS62268439A (en) * | 1986-05-14 | 1987-11-21 | 松下電工株式会社 | Nozzle driving apparatus of hot water washing apparatus |
-
1978
- 1978-01-20 JP JP505378A patent/JPS54100323A/en active Granted
Also Published As
Publication number | Publication date |
---|---|
JPS6126778B2 (en) | 1986-06-21 |
Similar Documents
Publication | Publication Date | Title |
---|---|---|
JPS5736115A (en) | Curing agent composition for polyurethane | |
GB1491695A (en) | Photopolymerizable copying compositions and photopolymerizable compounds for use therein | |
JPS5747319A (en) | Preparation of aliphatic isocyanurate compound | |
JPS54100323A (en) | Preparation of organic polyisocyanate having improved long-term storage stability | |
GB852988A (en) | Alkylbenzene diisocyanates | |
JPS5647431A (en) | Photoconductive polymer and photoconductive material | |
JPS5730717A (en) | Preparation of thermosetting resin | |
US3142653A (en) | Plasticized urea-formaldehyde resins | |
JPS55167273A (en) | Novel bis(n-carboalkoxy-anilino)methane and its preparation | |
GB1273376A (en) | Process for the preparation of physiologically harmless aliphatic polyisocyanates | |
JPS53106797A (en) | Preparation of organic polyisocyanate having improved storage stability | |
JPS5350187A (en) | Preparation of plyisocyanates | |
JPS557832A (en) | Preparation of fibrous zr-containing phosphoric acid compound | |
GB1199810A (en) | Improvements in or relating to Polyurethane Resins | |
JPS56814A (en) | Oligomer composition composed of isoxazolidine derivative | |
JPS5536240A (en) | Preparation of substance having photosensitivity- promoting activity | |
JPS5569614A (en) | Quick-drying, urethane-forming composition | |
JPS54125633A (en) | 4-chloro-3,5-diaminophenyl acetate, its preparation, and hardeners for preparing polyurethane elastomers | |
JPS54110296A (en) | Polyurethane resin and coating composition | |
JPS54105199A (en) | Preparation of organic polyisocyanate having improved storage stability | |
JPS5767626A (en) | Water-soluble blocked isocyanate compound | |
JPS5476697A (en) | Epoxy resin composition | |
JPS54154427A (en) | Polyurethane coating composition | |
JPS57165416A (en) | Photo-setting urethane acrylic resin composition | |
JPS55120591A (en) | Phosphinoethylmalonic acid derivative, and preparation thereof |