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JPH0480305A - Manufacture of powder high speed steel product - Google Patents

Manufacture of powder high speed steel product

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Publication number
JPH0480305A
JPH0480305A JP19525590A JP19525590A JPH0480305A JP H0480305 A JPH0480305 A JP H0480305A JP 19525590 A JP19525590 A JP 19525590A JP 19525590 A JP19525590 A JP 19525590A JP H0480305 A JPH0480305 A JP H0480305A
Authority
JP
Japan
Prior art keywords
hip
heating
time
temp
speed steel
Prior art date
Legal status (The legal status is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the status listed.)
Pending
Application number
JP19525590A
Other languages
Japanese (ja)
Inventor
Yukinori Matsuda
幸紀 松田
Kozo Ozaki
公造 尾崎
Current Assignee (The listed assignees may be inaccurate. Google has not performed a legal analysis and makes no representation or warranty as to the accuracy of the list.)
Daido Steel Co Ltd
Original Assignee
Daido Steel Co Ltd
Priority date (The priority date is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the date listed.)
Filing date
Publication date
Application filed by Daido Steel Co Ltd filed Critical Daido Steel Co Ltd
Priority to JP19525590A priority Critical patent/JPH0480305A/en
Publication of JPH0480305A publication Critical patent/JPH0480305A/en
Pending legal-status Critical Current

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  • Powder Metallurgy (AREA)

Abstract

PURPOSE:To improve grindability and machinability without lowering mechanical property by making value in the specific range of high temp. heating and parameter at the time of HIP treatment. CONSTITUTION:In the manufacturing method of powder high speed steel product with the hot isostatic pressing (HIP) and forging, to the high speed steed powder containing >=0.01 vol% improving component for machinability, whose shape is varied under hot machining condition, the HIP is executed so as to be in the range of P = (4.0 - 5.6) X 10<4> at the time of using P = T(log t + 37), wherein, T: temp. ( deg.K), t: time (sec) for high temp. heating parameter P at the time of executing the HIP. The heating at higher temp. and for longer time which causes P to exceed the value of P = 5.6 X 10<4> the upper limit value of the high temp. heating parameter P, brings about coarsening of machinable inclusion. In the heating, which does not reach the lower limit value 4.0 X 10<4>, the density after executing the HIP is far from the true density, and even this is forged, the remaining voids are extended and anisotropy is made to high and mechanical property in the product is deteriorated.

Description

【発明の詳細な説明】[Detailed description of the invention]

(産業上の利用分野] 本発明は、機械的性質を低下させることなく被研削性、
被切削性を向上させた粉末高速度鋼製品の製造方法に関
する。 (従来の技術] 粉末高速度鋼から工具などの製品を製造するには、熱間
静水圧プレス(HIP)−鍛造−切削または研削による
仕上げ−の工程を経ることが多い。 従来、粉末高速度鋼の切削性を向上させる目的で、Sや
3eのような快削元素を添加し、主としてMn5(Se
)からなる介在物を生成させる手段がとられて来た。 このような介在物は、溶湯噴霧により得た段階の高速度
鋼粉末中では、微細かつ均一に分散している。 しかし
、その後の加熱工程で、粉末内部において介在物が凝集
したり、粉末表面において濃化したS成分のもたらす介
在物の凝集粗大化が起り、大型化した介在物が鍛伸工程
で延伸されて異方性を高めるとともに、熱間加工性を悪
くしていた。 このため、被削性は期待したほどは向上
せず、また機械的性質の低下が工具の性能の低下を招い
ていた。 事実、HIP−鍛造による粉末高速度鋼製品中には、長
さ1μIrLを越える介在物の存在がしばしば観察され
る。 [発明が解決しようとする課題] 本発明の目的は、粉末高速度鋼製品の製造技術の現状を
改善し、加熱工程において快削化介在物の粗大化が進ま
ず、かつ鍛伸工程における介在物のアスペクト比(縦、
横の比)の増大が押えられ、したがって機械的特性が低
下せず、しかも被削性向上効果を十分に享受できる製品
を製造する方法を提供することにある。 [課題を解決するための手段] 本発明の粉末高速度鋼製品の製造方法は、熱間静水圧プ
レス(HIP>および鍛造により粉末高速度鋼製品を製
造する方法において、熱間加工条件下にその形状が変化
する被削性改善成分を0゜01体積%以上含有する高速
度鋼粉末を、HIP時高温加熱パラメータPを P=T (lop t+37> (ただし、Tは温度(゜K)、tは時間(sec))と
するとき、P= (4,0〜5.6)X104の範囲に
あるようにHIPを実施することを特徴とする。 この方法を適用できる粉末高速度鋼は、JIS鋼種記号
でいえば、つぎのような鋼である。 5KH51,52,53,55,56,58゜59.5
KH2,3,4,10 [作 用] 発明者らは、研究の結果、粉末高速度鋼製品の製造工程
の中では、とくに粉末の粒子界面における快削化介在物
の凝集粗大化が、実質上真密度(99,99%以上)に
至らない段階で高温に加熱されたときに進行すること、
そしてこの粗大化の進行は加熱条件によって異なること
を見出した。 さらに、快削化介在物が比較的大型(平均粒径にして0
.5μ■以上)の場合に、その後の鍛造工程においてそ
のアスペクト比が増大しやすいことを見出した。 そこで、粉末粒子界面を中心として快削性物質の粗大化
が進まず、したがって鍛伸後の7スペクト比の増大も少
ない加熱条件を探求したところ、前記したように、高温
加熱パラメータPを特定の範囲になるよう条件をえらべ
ばよいことを知って本発明に至った。 高温加熱パラメータPが上限値5.6X104を超える
高温および(または)長時間の加熱は、快削化介在物の
粗大化を招く。 一方、下限値4.0X10’に達しな
い加熱では、HIP後の密度が真密度に遠く(90%)
、これを鍛造しても残存していた空隙が延伸されて異方
性が高まり、製品の機械的特性が劣る。
(Industrial Application Field) The present invention improves grindability without reducing mechanical properties.
This invention relates to a method for manufacturing powdered high-speed steel products with improved machinability. (Prior Art) To manufacture products such as tools from powdered high-speed steel, it often goes through the process of hot isostatic pressing (HIP) - forging - finishing by cutting or grinding. In order to improve the machinability of steel, free-cutting elements such as S and 3e are added, and mainly Mn5 (Se
) measures have been taken to generate inclusions consisting of Such inclusions are finely and uniformly dispersed in the high-speed steel powder obtained by molten metal spraying. However, in the subsequent heating process, inclusions agglomerate inside the powder, and inclusions aggregate and coarsen due to the concentrated S component on the powder surface, and the enlarged inclusions are stretched in the forging process. While increasing anisotropy, hot workability was worsened. For this reason, machinability did not improve as much as expected, and the decrease in mechanical properties led to a decrease in tool performance. In fact, the presence of inclusions with lengths exceeding 1 μIrL is often observed in HIP-forged powder high speed steel products. [Problems to be Solved by the Invention] An object of the present invention is to improve the current state of manufacturing technology for powdered high-speed steel products, to prevent the coarsening of free-cutting inclusions in the heating process, and to reduce the coarsening of free-cutting inclusions in the forging process. Aspect ratio of an object (vertical,
It is an object of the present invention to provide a method for manufacturing a product in which the increase in the lateral ratio (lateral ratio) is suppressed, the mechanical properties are not deteriorated, and the machinability improvement effect can be fully enjoyed. [Means for Solving the Problems] The method for manufacturing powdered high-speed steel products of the present invention is a method for manufacturing powdered high-speed steel products by hot isostatic pressing (HIP>) and forging, wherein A high-speed steel powder containing 0°01 volume % or more of machinability-improving components that change its shape is heated at high temperature during HIP by setting the heating parameter P to P=T (lop t+37> (where T is temperature (°K), When t is time (sec), HIP is performed in the range of P = (4,0 to 5.6) x 104. Powder high speed steel to which this method can be applied is: In terms of JIS steel type symbols, they are as follows: 5KH51, 52, 53, 55, 56, 58° 59.5
KH2, 3, 4, 10 [Function] As a result of research, the inventors found that in the manufacturing process of powdered high-speed steel products, the agglomeration and coarsening of free-cutting inclusions, especially at the particle interface of the powder, is a substantial problem. Proceeds when heated to a high temperature before reaching the upper true density (99.99% or more);
It was also found that the progress of this coarsening differs depending on the heating conditions. Furthermore, the free-cutting inclusions are relatively large (average particle size is 0).
.. It has been found that when the aspect ratio is 5μ or more), the aspect ratio tends to increase in the subsequent forging process. Therefore, we searched for heating conditions that would prevent the coarsening of the free-machining material centering on the powder particle interface and, therefore, less increase in the 7 spectral ratio after forging.As mentioned above, we found that the high temperature heating parameter P was The present invention was achieved by learning that conditions should be selected so as to fall within the range. High-temperature and/or long-term heating at which the high-temperature heating parameter P exceeds the upper limit of 5.6×104 causes coarsening of free-cutting inclusions. On the other hand, when heating does not reach the lower limit of 4.0X10', the density after HIP is far from the true density (90%).
Even if this is forged, the remaining voids are stretched, increasing the anisotropy and resulting in poor mechanical properties of the product.

【実施例】【Example】

下記の合金組成(重量%、残部Fe)をもつ工具用粉末
ハイス鋼rDEX80Jに、快削元素としてSを0.0
1〜1.5%の範囲で種々の量添加した鋼を溶製し、ガ
ス噴霧法により粉末化した。 CSi    Mn    Cr    M。 2.8 0.3 0.3 4.2   6V     
 W     C。 この粉末を軟鋼製の缶に充填し、真空下に密封して、種
々異なる高温加熱パラメータの下でHIP処理した。 
得られた焼結体について、A)そのまま、 B)1200℃において鍛造(鍛錬社10.23>に分
け、それぞれの試料について、快削化介在物の占める体
積%および平均アスペクト比(L/T>をしらべた。 
この測定は、大きさ0.1μm以上の粒子を対象に行な
った。 試料を焼入れ焼戻し処理した後、ホワイトアランダム砥
石を用いた研削、エンドミルを用いた切削、および衝撃
試験を行なって、下記の物性を測定した。 研 削 比 :研削量/砥石減耗量 切削性能指数:最良の結果を与えたNO3の値を100
としたときの相対値 抗 折 カニ最も低い方向の抗折力 比較のため、高温加熱パラメータPを本発明の範囲外と
した場合についても実験した。 それらのデータを、下
表に示す。 r発明の効果】 本発明の方法により粉末高速度m製品を製造すれば、快
削元素の添加がもたらす機械的性質の低下を避けて被削
性向上効果を享受することができる。 特許出願人   大同特殊鋼株式会社 代理人  弁理士  須 賀 総 夫 手続補正書 (自発) 平成3年IO月9
0.0 S as a free-cutting element was added to rDEX80J powdered high-speed steel for tools having the following alloy composition (weight %, remainder Fe).
Steels with various amounts added in the range of 1 to 1.5% were melted and powdered by a gas atomization method. CSi Mn Cr M. 2.8 0.3 0.3 4.2 6V
W.C. The powder was filled into mild steel cans, sealed under vacuum, and HIPed under different high temperature heating parameters.
The obtained sintered body was divided into A) as-is, B) forging at 1200°C (Kenryusha 10.23), and for each sample, the volume % occupied by free-cutting inclusions and the average aspect ratio (L/T > I looked into it.
This measurement was performed on particles having a size of 0.1 μm or more. After the sample was quenched and tempered, it was ground using a white alundum grindstone, cut using an end mill, and subjected to an impact test, and the following physical properties were measured. Grinding ratio: Grinding amount/Wheelstone wear amount Cutting performance index: The value of NO3 that gave the best result was set to 100
In order to compare the relative value of the transverse rupture force in the lowest direction, experiments were also carried out when the high temperature heating parameter P was outside the range of the present invention. The data are shown in the table below. [Effects of the Invention] By producing a powder high-speed m product by the method of the present invention, it is possible to enjoy the effect of improving machinability while avoiding the deterioration of mechanical properties caused by the addition of free-cutting elements. Patent Applicant Daido Steel Co., Ltd. Agent Patent Attorney Souo Suga Procedural Amendment (Voluntary) IO September 9, 1991

Claims (1)

【特許請求の範囲】 熱間静水圧プレス(HIP)および鍛造により粉末高速
度鋼製品を製造する方法において、熱間加工条件下にそ
の形状が変化する被削性改善成分を0.01体積%以上
含有する高速度鋼粉末を、HIP時高温加熱パラメータ
Pを P=T(logt+37) 〔ただし、Tは温度(゜K)、tは時間(sec)〕と
するとき、P=(4.0〜5.6)×10^4の範囲に
あるようにHIPを実施することを特徴とする製造方法
[Claims] In a method for manufacturing powdered high-speed steel products by hot isostatic pressing (HIP) and forging, a machinability-improving component whose shape changes under hot working conditions is 0.01% by volume. High-speed steel powder containing the above-mentioned high-temperature heating parameter P during HIP is P = T (logt + 37) [where T is temperature (°K) and t is time (sec)], P = (4.0 A manufacturing method characterized in that HIP is performed in the range of ~5.6)×10^4.
JP19525590A 1990-07-24 1990-07-24 Manufacture of powder high speed steel product Pending JPH0480305A (en)

Priority Applications (1)

Application Number Priority Date Filing Date Title
JP19525590A JPH0480305A (en) 1990-07-24 1990-07-24 Manufacture of powder high speed steel product

Applications Claiming Priority (1)

Application Number Priority Date Filing Date Title
JP19525590A JPH0480305A (en) 1990-07-24 1990-07-24 Manufacture of powder high speed steel product

Publications (1)

Publication Number Publication Date
JPH0480305A true JPH0480305A (en) 1992-03-13

Family

ID=16338095

Family Applications (1)

Application Number Title Priority Date Filing Date
JP19525590A Pending JPH0480305A (en) 1990-07-24 1990-07-24 Manufacture of powder high speed steel product

Country Status (1)

Country Link
JP (1) JPH0480305A (en)

Cited By (3)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
JPH07179908A (en) * 1993-09-27 1995-07-18 Crucible Materials Corp Sulfur-containing powder metallurgy tool steel object
CN104004956A (en) * 2014-05-29 2014-08-27 河冶科技股份有限公司 Manufacturing method of high-performance jet steel
CN104004955A (en) * 2014-05-29 2014-08-27 河冶科技股份有限公司 Manufacturing method of high-temperature jet steel

Cited By (3)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
JPH07179908A (en) * 1993-09-27 1995-07-18 Crucible Materials Corp Sulfur-containing powder metallurgy tool steel object
CN104004956A (en) * 2014-05-29 2014-08-27 河冶科技股份有限公司 Manufacturing method of high-performance jet steel
CN104004955A (en) * 2014-05-29 2014-08-27 河冶科技股份有限公司 Manufacturing method of high-temperature jet steel

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