JP2008119433A - How to save paper towels and hand towels - Google Patents
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- JP2008119433A JP2008119433A JP2006335093A JP2006335093A JP2008119433A JP 2008119433 A JP2008119433 A JP 2008119433A JP 2006335093 A JP2006335093 A JP 2006335093A JP 2006335093 A JP2006335093 A JP 2006335093A JP 2008119433 A JP2008119433 A JP 2008119433A
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- 229920001090 Polyaminopropyl biguanide Polymers 0.000 claims description 7
- 229940093424 polyaminopropyl biguanide Drugs 0.000 claims description 6
- 150000003242 quaternary ammonium salts Chemical class 0.000 claims description 6
- 229960000686 benzalkonium chloride Drugs 0.000 claims description 3
- XIWFQDBQMCDYJT-UHFFFAOYSA-M benzyl-dimethyl-tridecylazanium;chloride Chemical compound [Cl-].CCCCCCCCCCCCC[N+](C)(C)CC1=CC=CC=C1 XIWFQDBQMCDYJT-UHFFFAOYSA-M 0.000 claims description 3
- 229960001927 cetylpyridinium chloride Drugs 0.000 claims description 3
- YMKDRGPMQRFJGP-UHFFFAOYSA-M cetylpyridinium chloride Chemical compound [Cl-].CCCCCCCCCCCCCCCC[N+]1=CC=CC=C1 YMKDRGPMQRFJGP-UHFFFAOYSA-M 0.000 claims description 3
- WOWHHFRSBJGXCM-UHFFFAOYSA-M cetyltrimethylammonium chloride Chemical compound [Cl-].CCCCCCCCCCCCCCCC[N+](C)(C)C WOWHHFRSBJGXCM-UHFFFAOYSA-M 0.000 claims description 3
- NLGPPMLLUZWGGS-UHFFFAOYSA-N prop-1-ynyl n-butylcarbamate Chemical compound CCCCNC(=O)OC#CC NLGPPMLLUZWGGS-UHFFFAOYSA-N 0.000 claims description 3
- VBIIFPGSPJYLRR-UHFFFAOYSA-M Stearyltrimethylammonium chloride Chemical compound [Cl-].CCCCCCCCCCCCCCCCCC[N+](C)(C)C VBIIFPGSPJYLRR-UHFFFAOYSA-M 0.000 claims description 2
- UREZNYTWGJKWBI-UHFFFAOYSA-M benzethonium chloride Chemical compound [Cl-].C1=CC(C(C)(C)CC(C)(C)C)=CC=C1OCCOCC[N+](C)(C)CC1=CC=CC=C1 UREZNYTWGJKWBI-UHFFFAOYSA-M 0.000 claims description 2
- 229960001950 benzethonium chloride Drugs 0.000 claims description 2
- 230000000844 anti-bacterial effect Effects 0.000 abstract description 8
- 239000004615 ingredient Substances 0.000 abstract description 7
- 230000000843 anti-fungal effect Effects 0.000 abstract description 6
- 230000002195 synergetic effect Effects 0.000 abstract description 2
- 239000008406 cosmetic ingredient Substances 0.000 abstract 1
- 238000000034 method Methods 0.000 description 7
- 238000013329 compounding Methods 0.000 description 6
- 239000000203 mixture Substances 0.000 description 5
- XLYOFNOQVPJJNP-UHFFFAOYSA-N water Substances O XLYOFNOQVPJJNP-UHFFFAOYSA-N 0.000 description 5
- 241000894006 Bacteria Species 0.000 description 3
- DNIAPMSPPWPWGF-UHFFFAOYSA-N Propylene glycol Chemical compound CC(O)CO DNIAPMSPPWPWGF-UHFFFAOYSA-N 0.000 description 3
- 229940121375 antifungal agent Drugs 0.000 description 3
- 239000003795 chemical substances by application Substances 0.000 description 3
- 239000004744 fabric Substances 0.000 description 3
- 239000000835 fiber Substances 0.000 description 3
- 239000007788 liquid Substances 0.000 description 3
- 239000000126 substance Substances 0.000 description 3
- 241000588724 Escherichia coli Species 0.000 description 2
- 241000191967 Staphylococcus aureus Species 0.000 description 2
- CEBAWORGZDCFQS-UHFFFAOYSA-N butylcarbamic acid 1-iodoprop-1-yne Chemical compound C(#CC)I.C(CCC)NC(O)=O CEBAWORGZDCFQS-UHFFFAOYSA-N 0.000 description 2
- 239000002537 cosmetic Substances 0.000 description 2
- OSVXSBDYLRYLIG-UHFFFAOYSA-N dioxidochlorine(.) Chemical compound O=Cl=O OSVXSBDYLRYLIG-UHFFFAOYSA-N 0.000 description 2
- 230000000694 effects Effects 0.000 description 2
- 230000002538 fungal effect Effects 0.000 description 2
- 238000005470 impregnation Methods 0.000 description 2
- 239000004745 nonwoven fabric Substances 0.000 description 2
- VAZJLPXFVQHDFB-UHFFFAOYSA-N 1-(diaminomethylidene)-2-hexylguanidine Chemical compound CCCCCCN=C(N)N=C(N)N VAZJLPXFVQHDFB-UHFFFAOYSA-N 0.000 description 1
- OMNGRPHPKWAMSY-UHFFFAOYSA-N 1-chloroprop-1-yne Chemical compound CC#CCl OMNGRPHPKWAMSY-UHFFFAOYSA-N 0.000 description 1
- 241000228245 Aspergillus niger Species 0.000 description 1
- 241001515917 Chaetomium globosum Species 0.000 description 1
- 239000004155 Chlorine dioxide Substances 0.000 description 1
- 241000233866 Fungi Species 0.000 description 1
- 240000001194 Heliotropium europaeum Species 0.000 description 1
- FBOUJVVNFRBCHQ-UHFFFAOYSA-N N-butylcarbamoyl iodide Chemical compound C(CCC)NC(=O)I FBOUJVVNFRBCHQ-UHFFFAOYSA-N 0.000 description 1
- 241000228153 Penicillium citrinum Species 0.000 description 1
- 230000002421 anti-septic effect Effects 0.000 description 1
- -1 butyl carbamate bromide iodide Chemical compound 0.000 description 1
- 150000001768 cations Chemical class 0.000 description 1
- 235000019398 chlorine dioxide Nutrition 0.000 description 1
- 125000001495 ethyl group Chemical group [H]C([H])([H])C([H])([H])* 0.000 description 1
- 239000012530 fluid Substances 0.000 description 1
- 238000009472 formulation Methods 0.000 description 1
- 239000003205 fragrance Substances 0.000 description 1
- 125000002496 methyl group Chemical group [H]C([H])([H])* 0.000 description 1
- 244000005700 microbiome Species 0.000 description 1
- 238000002156 mixing Methods 0.000 description 1
- 238000004806 packaging method and process Methods 0.000 description 1
- 230000035699 permeability Effects 0.000 description 1
- 238000004321 preservation Methods 0.000 description 1
- 239000003755 preservative agent Substances 0.000 description 1
- 230000002335 preservative effect Effects 0.000 description 1
- 230000002265 prevention Effects 0.000 description 1
- 238000003672 processing method Methods 0.000 description 1
- 239000008213 purified water Substances 0.000 description 1
- 239000002994 raw material Substances 0.000 description 1
- 239000007921 spray Substances 0.000 description 1
- 238000005507 spraying Methods 0.000 description 1
- 230000001954 sterilising effect Effects 0.000 description 1
- 238000010998 test method Methods 0.000 description 1
Landscapes
- Body Washing Hand Wipes And Brushes (AREA)
- Apparatus For Disinfection Or Sterilisation (AREA)
- Agricultural Chemicals And Associated Chemicals (AREA)
Abstract
【課題】 手指の清拭に際し、皮膚に対する安全性を確保し、かつ充分な抗菌・防カビ効果を持った紙おしぼり・お手ふきを製造する。
【解決手段】 本発明は、配合成分およびその配合量を化粧品基準に準ずることにより皮膚に対する安全性を確保し、複数成分の配合による相乗効果により充分な抗菌・防カビ効果を付与する。PROBLEM TO BE SOLVED: To produce a paper towel / hand wipe having a sufficient antibacterial / antifungal effect while ensuring safety for skin when wiping fingers.
SOLUTION: The present invention ensures skin safety by complying with cosmetic ingredients according to the ingredients and amounts of the ingredients, and provides a sufficient antibacterial and antifungal effect due to the synergistic effect of the combination of a plurality of ingredients.
Description
本発明は、パルプまたは不織布等の紙おしぼり・お手ふきの保存方法に関する。詳しくはポリアミノプロピルビグアナイド、第四級アンモニウム塩およびブチルカルバミン酸ヨウ化プロピニルなどの配合加工液で処理する紙おしぼり・お手ふきの保存方法である。 The present invention relates to a method for preserving paper towels and hand towels such as pulp or nonwoven fabric. Specifically, it is a method for preserving paper towels and hand towels that are treated with a compounding processing solution such as polyaminopropyl biguanide, quaternary ammonium salt and propynyl iodide butylcarbamate.
紙おしぼり・お手ふきは水を含むという性質上、微生物（細菌類・真菌類）の繁殖の危険性がある。このため加工液には防腐剤が配合されている。しかしその配合成分や配合量においては使用用途を考慮すると、安全性の高い物質でなければならない。 Paper towels and hand towels contain water, so there is a risk of propagation of microorganisms (bacteria and fungi). For this reason, a preservative is blended in the working fluid. However, in consideration of the intended use, the compounding component and the compounding amount must be a highly safe substance.
またウェットティシューとは異なり、簡易、個包装であるにもかかわらず３〜６ヶ月の保存期間が考えられ、その保管には夏季は冷たく、冬季は暖かくするなどの条件により、より強力な防腐効果が求められている。 Unlike wet tissue, it can be stored for 3 to 6 months despite its simple and individual packaging, and its storage is colder in summer and warmer in winter. Is required.
使用時においては、その使用感が問題であり、ぬめり感や臭気等があってはならない。
また紙おしぼり・お手ふきの加工に関しては、ほとんどがスプレー方式によるもので、均一に処理することがむずかしいため、加工液の浸透性及び分散性が重要になる。In use, the feeling of use is a problem, and there should be no sliminess or odor.
Also, with regard to the processing of paper towels and hand towels, most of them are based on the spray method, and it is difficult to uniformly treat them. Therefore, the permeability and dispersibility of the processing liquid are important.
本発明では、紙おしぼりやお手ふきへの加工液の配合成分及びその配合量について安全性を確保し、かつ十分な保存効果を付与することを目的とする。 In this invention, it aims at ensuring safety | security about the compounding component and the compounding quantity of the processing liquid to a paper towel and a hand towel, and providing sufficient preservation | save effect.
本発明者らは上記の課題を解決する為、安全性を考慮し、化粧品に配合できる成分の中から複数成分を使用することにより、その相乗効果をもって紙おしぼり・お手ふき保存時の細菌類・真菌類の増殖を抑制する配合を発見し、本発明を完成した。 In order to solve the above problems, the present inventors consider safety and use a plurality of ingredients from among ingredients that can be blended into cosmetics. A formulation that inhibits fungal growth was discovered and the present invention was completed.
化粧品に添加可能な薬剤の単独使用では弱かった紙おしぼり・お手ふきの防腐効果が、複数成分の配合による相乗効果によって十分な防腐効果が得られた。 The antiseptic effect of paper towels and hand towels, which was weak when using a single agent that can be added to cosmetics, was obtained by the synergistic effect of the combination of multiple ingredients.
本発明の配合組成物は、ポリアミノプロピルビグアナイドおよび第四級アンモニウム塩で、塩化ベンザルコニウム、塩化ベンゼトニウム、塩化セチルトリメチルアンモニウム、塩化ステアリルトリメチルアンモニウム、塩化セチルピリジニウムのうちの一種以上とブチルカルバミン酸ヨウ化プロピニルを含有する。 The blended composition of the present invention is a polyaminopropyl biguanide and a quaternary ammonium salt, and one or more of benzalkonium chloride, benzethonium chloride, cetyltrimethylammonium chloride, stearyltrimethylammonium chloride, cetylpyridinium chloride and butylcarbamic acid iodide. Contains propynyl chloride.
加工方法は加工する紙ならびに不織布等（以下、原反と称する）の重量に対し、１５０〜２５０％の加工液をスプレーまたは含浸等の方法で加工する。ただし加工する原反によって適切な加工量は異なる。 The processing method is to process 150 to 250% of the processing liquid by a method such as spraying or impregnation with respect to the weight of the paper to be processed and the nonwoven fabric (hereinafter referred to as the original fabric). However, the appropriate processing amount varies depending on the raw material to be processed.
本発明の組成物以外に水，原反の殺菌を目的として安定化二酸化塩素水を配合したり、使用時の清涼感を付与する目的で香料等の成分を配合することもできる。 In addition to the composition of the present invention, stabilized chlorine dioxide water can be blended for the purpose of sterilizing water and raw fabric, and ingredients such as fragrances can be blended for the purpose of imparting a refreshing feeling during use.
本発明の紙おしぼり・お手ふき加工組成物は一種以上のポリアミノプロピルビグアナイドおよび第四級アンモニウム塩とブチルカルバミン酸ヨウ化プロピニルを配合した組成物で、手指の清拭用として使用するものである。 The paper towel / hand wipe composition of the present invention is a composition comprising one or more polyaminopropyl biguanides and a quaternary ammonium salt and propynyl butylcarbamate, and is used for wiping fingers.
以下、実施例により詳細説明する。しかし本発明はこれらの実施例に限定されるものではない。 Hereinafter, the embodiment will be described in detail. However, the present invention is not limited to these examples.
（実施例１）本発明に使用するポリアミノプロピルビグアナイドおよび第四級アンモニウム塩、ブチルカルバミン酸ヨウ化プロピニルの配合例を表１，２に記す。 (Example 1) Tables 1 and 2 show blending examples of polyaminopropyl biguanide, quaternary ammonium salt and propynyl butylcarbamate used in the present invention.
原反（ここではパルプを使用）に表１に記した配合薬剤を原反重量に対し２００％ムラなく含浸により処理した。比較として水のみを加工したものを作成した。 The compounding agents shown in Table 1 were processed by impregnation without any unevenness by 200% with respect to the weight of the original fabric (here, pulp was used). The thing which processed only water was created as a comparison.
使用薬剤
Ａ；塩化ベンザルコニウム（日本油脂（株）カチオンＭ２−１００）
Ｂ；塩化セチルトリメチルアンモニウム（日光ケミカルズ（株）ＣＡ−２３５０）
Ｃ；塩化セチルピリジニウム（メルク・ジャパン（株））
Ｄ；ポリアミノプロピルビグアナイド（アーチケミカル（株）Ｃｏｓｍｏｃｉｌ ＣＱ）
Ｅ；ブチルカルバミン酸ヨウ化プロピニル（三井化学（株）ヨートルＩＰ）
Ｆ；プロピレングリコール（昭和電工（株））
Ｇ；パラオキシ安息香酸メチル（上野製薬（株））
Ｈ；パラオキシ安息香酸エチル（上野製薬（株））
Ｉ；精製水Agent A: Benzalkonium chloride (Nippon Yushi Co., Ltd. Cation M2-100)
B: Cetyltrimethylammonium chloride (Nikko Chemicals CA-2350)
C: Cetylpyridinium chloride (Merck Japan Co., Ltd.)
D: Polyaminopropyl biguanide (Arco Chemical Co., Ltd. Cosmocil CQ)
E: propynyl iodide butylcarbamate (Yottle IP, Mitsui Chemicals, Inc.)
F: Propylene glycol (Showa Denko KK)
G: Methyl paraoxybenzoate (Ueno Pharmaceutical Co., Ltd.)
H: Ethyl paraoxybenzoate (Ueno Pharmaceutical Co., Ltd.)
I: Purified water
（試験１：抗菌・防カビ試験）
試験方法
抗菌試験：ＪＩＳ Ｌ−１９０２繊維製品の抗菌性試験に準じた。
供試細菌
Ａ：Ｅｓｃｈｅｒｉｃｈｉａ ｃｏｌｉ ＮＢＲＣ ３３０１（大腸菌）
Ｂ：Ｓｔａｐｈｙｌｏｃｏｃｃｕｓ ａｕｒｅｕｓ ＮＢＲＣ １２７３２（黄色ブドウ球菌）
防カビ試験：ＪＩＳ Ｚ−２９１１カビ抵抗性試験 繊維試験指定繊維カビ
Ａ：Ａｓｐｅｒｇｉｌｌｕｓ ｎｉｇｅｒ ＦＥＲＭ Ｓ−１
Ｂ：Ｐｅｎｉｃｉｌｌｉｕｍ ｃｉｔｒｉｎｕｍ ＦＥＲＭ Ｓ−５
Ｃｈａｅｔｏｍｉｕｍ ｇｌｏｂｏｓｕｍ ＦＥＲＭ Ｓ−１１
Ｍｙｒｏｔｈｅｃｉｕｍ ｖｅｒｒｕｃａｒｉａ ＦＥＲＭ Ｓ−１３ 以上３種の混合(Test 1: Antibacterial / antifungal test)
Test method Antibacterial test: According to JIS L-1902 fiber product antibacterial test.
Test bacteria
A: Escherichia coli NBRC 3301 (E. coli)
B: Staphylococcus aureus NBRC 12732 (Staphylococcus aureus)
Antifungal test: JIS Z-2911 fungal resistance test Fiber test designated fiber mold
A: Aspergillus niger FERM S-1
B: Penicillium citrinum FERM S-5
Chaetomium globosum FERM S-11
Myrothecerium verrucaria FERM S-13
判定方法
抗菌試験 細菌・・・効果有り （−）
効果なし （＋）
防カビ試験・・・ＪＩＳ Ｚ−２９１１ カビ抵抗性試験 表示方法による
０・・・試料上にカビの発育なし
右側の数値は発育阻止ｍｍ数
１・・・試料上のカビの発育面積が全体の１／３以下
２・・・試料上のカビの発育面積が全体の１／３以上Judgment method Antibacterial test Bacteria ... Effective (-)
No effect (+)
Mold prevention test JIS Z-2911 Mold resistance test According to display method
0 ... No mold growth on the sample
The number on the right is the number of mm
1 ... Mold growth area on the sample is 1/3 or less of the whole
2 ... Mold growth area on the sample is 1/3 or more of the whole
抗菌防カビ試験の結果を表３，４に示す。 The results of the antibacterial and antifungal test are shown in Tables 3 and 4.
以上のごとく、ポリアミノプロピルビグアナイド、第四級アンモニウム塩およびブチルカルバミン酸ヨウ化ブロビニルなどの配合加工液で処理した紙おしぼりは、優れた抗菌・防カビ効果を発揮する。 As described above, paper towels treated with a blended processing solution such as polyaminopropyl biguanide, quaternary ammonium salt and butyl carbamate bromide iodide exhibit excellent antibacterial and antifungal effects.
Claims (1)
Priority Applications (1)
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| JP2006335093A JP2008119433A (en) | 2006-11-15 | 2006-11-15 | How to save paper towels and hand towels |
Applications Claiming Priority (1)
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| JP2006335093A JP2008119433A (en) | 2006-11-15 | 2006-11-15 | How to save paper towels and hand towels |
Publications (1)
| Publication Number | Publication Date |
|---|---|
| JP2008119433A true JP2008119433A (en) | 2008-05-29 |
Family
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Family Applications (1)
| Application Number | Title | Priority Date | Filing Date |
|---|---|---|---|
| JP2006335093A Pending JP2008119433A (en) | 2006-11-15 | 2006-11-15 | How to save paper towels and hand towels |
Country Status (1)
| Country | Link |
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| JP (1) | JP2008119433A (en) |
Cited By (7)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| JP2012024520A (en) * | 2010-07-28 | 2012-02-09 | Lec Inc | Wipe-cleaning sheet |
| WO2013115061A1 (en) * | 2012-01-31 | 2013-08-08 | Ｖｂジャパンテクノロジー株式会社 | Heated moist towelette and method for producing heated moist towelette |
| JP2016032646A (en) * | 2015-09-28 | 2016-03-10 | レック株式会社 | Manufacturing method of wipe sheet for wiping infant buttocks |
| JP2016097336A (en) * | 2014-11-19 | 2016-05-30 | 日揮ユニバーサル株式会社 | Filter medium for air filter and manufacturing method of the same |
| JP2017124060A (en) * | 2016-01-14 | 2017-07-20 | 日本製紙クレシア株式会社 | Wet tissue roll body |
| JP2018188368A (en) * | 2017-04-28 | 2018-11-29 | 日本製紙クレシア株式会社 | Wet wiper |
| WO2023228604A1 (en) * | 2022-05-24 | 2023-11-30 | 大王製紙株式会社 | Cleansing wet wipe |
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Cited By (10)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| JP2012024520A (en) * | 2010-07-28 | 2012-02-09 | Lec Inc | Wipe-cleaning sheet |
| WO2013115061A1 (en) * | 2012-01-31 | 2013-08-08 | Ｖｂジャパンテクノロジー株式会社 | Heated moist towelette and method for producing heated moist towelette |
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| JP2016097336A (en) * | 2014-11-19 | 2016-05-30 | 日揮ユニバーサル株式会社 | Filter medium for air filter and manufacturing method of the same |
| JP2016032646A (en) * | 2015-09-28 | 2016-03-10 | レック株式会社 | Manufacturing method of wipe sheet for wiping infant buttocks |
| JP2017124060A (en) * | 2016-01-14 | 2017-07-20 | 日本製紙クレシア株式会社 | Wet tissue roll body |
| JP2018188368A (en) * | 2017-04-28 | 2018-11-29 | 日本製紙クレシア株式会社 | Wet wiper |
| JP7078819B2 (en) | 2017-04-28 | 2022-06-01 | 日本製紙クレシア株式会社 | Wet wiper |
| WO2023228604A1 (en) * | 2022-05-24 | 2023-11-30 | 大王製紙株式会社 | Cleansing wet wipe |
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