GB995940A - Manufacture of detergent tablets - Google Patents
Manufacture of detergent tabletsInfo
- Publication number
- GB995940A GB995940A GB29355/63A GB2935563A GB995940A GB 995940 A GB995940 A GB 995940A GB 29355/63 A GB29355/63 A GB 29355/63A GB 2935563 A GB2935563 A GB 2935563A GB 995940 A GB995940 A GB 995940A
- Authority
- GB
- United Kingdom
- Prior art keywords
- water
- sodium
- specified
- detergent
- soluble
- Prior art date
- Legal status (The legal status is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the status listed.)
- Expired
Links
- 239000003599 detergent Substances 0.000 title abstract 8
- 238000004519 manufacturing process Methods 0.000 title 1
- XLYOFNOQVPJJNP-UHFFFAOYSA-N water Substances O XLYOFNOQVPJJNP-UHFFFAOYSA-N 0.000 abstract 6
- -1 alkyl phenols Chemical class 0.000 abstract 4
- 239000002245 particle Substances 0.000 abstract 4
- DGAQECJNVWCQMB-PUAWFVPOSA-M Ilexoside XXIX Chemical compound C[C@@H]1CC[C@@]2(CC[C@@]3(C(=CC[C@H]4[C@]3(CC[C@@H]5[C@@]4(CC[C@@H](C5(C)C)OS(=O)(=O)[O-])C)C)[C@@H]2[C@]1(C)O)C)C(=O)O[C@H]6[C@@H]([C@H]([C@@H]([C@H](O6)CO)O)O)O.[Na+] DGAQECJNVWCQMB-PUAWFVPOSA-M 0.000 abstract 3
- KWYUFKZDYYNOTN-UHFFFAOYSA-M Potassium hydroxide Chemical compound [OH-].[K+] KWYUFKZDYYNOTN-UHFFFAOYSA-M 0.000 abstract 3
- 229910052708 sodium Inorganic materials 0.000 abstract 3
- SUZRRICLUFMAQD-UHFFFAOYSA-N N-Methyltaurine Chemical compound CNCCS(O)(=O)=O SUZRRICLUFMAQD-UHFFFAOYSA-N 0.000 abstract 2
- 229920000388 Polyphosphate Polymers 0.000 abstract 2
- VYPSYNLAJGMNEJ-UHFFFAOYSA-N Silicium dioxide Chemical compound O=[Si]=O VYPSYNLAJGMNEJ-UHFFFAOYSA-N 0.000 abstract 2
- DPXJVFZANSGRMM-UHFFFAOYSA-N acetic acid;2,3,4,5,6-pentahydroxyhexanal;sodium Chemical compound [Na].CC(O)=O.OCC(O)C(O)C(O)C(O)C=O DPXJVFZANSGRMM-UHFFFAOYSA-N 0.000 abstract 2
- 125000000217 alkyl group Chemical group 0.000 abstract 2
- 125000002947 alkylene group Chemical group 0.000 abstract 2
- 239000001768 carboxy methyl cellulose Substances 0.000 abstract 2
- 239000001205 polyphosphate Substances 0.000 abstract 2
- 235000011176 polyphosphates Nutrition 0.000 abstract 2
- 239000011734 sodium Substances 0.000 abstract 2
- 235000019812 sodium carboxymethyl cellulose Nutrition 0.000 abstract 2
- 229920001027 sodium carboxymethylcellulose Polymers 0.000 abstract 2
- LDVVTQMJQSCDMK-UHFFFAOYSA-N 1,3-dihydroxypropan-2-yl formate Chemical compound OCC(CO)OC=O LDVVTQMJQSCDMK-UHFFFAOYSA-N 0.000 abstract 1
- 238000012935 Averaging Methods 0.000 abstract 1
- FBPFZTCFMRRESA-FSIIMWSLSA-N D-Glucitol Natural products OC[C@H](O)[C@H](O)[C@@H](O)[C@H](O)CO FBPFZTCFMRRESA-FSIIMWSLSA-N 0.000 abstract 1
- FBPFZTCFMRRESA-KVTDHHQDSA-N D-Mannitol Chemical compound OC[C@@H](O)[C@@H](O)[C@H](O)[C@H](O)CO FBPFZTCFMRRESA-KVTDHHQDSA-N 0.000 abstract 1
- FBPFZTCFMRRESA-JGWLITMVSA-N D-glucitol Chemical compound OC[C@H](O)[C@@H](O)[C@H](O)[C@H](O)CO FBPFZTCFMRRESA-JGWLITMVSA-N 0.000 abstract 1
- 239000004150 EU approved colour Substances 0.000 abstract 1
- 229930195725 Mannitol Natural products 0.000 abstract 1
- IGFHQQFPSIBGKE-UHFFFAOYSA-N Nonylphenol Natural products CCCCCCCCCC1=CC=C(O)C=C1 IGFHQQFPSIBGKE-UHFFFAOYSA-N 0.000 abstract 1
- 239000004372 Polyvinyl alcohol Substances 0.000 abstract 1
- GOOHAUXETOMSMM-UHFFFAOYSA-N Propylene oxide Chemical class CC1CO1 GOOHAUXETOMSMM-UHFFFAOYSA-N 0.000 abstract 1
- DBMJMQXJHONAFJ-UHFFFAOYSA-M Sodium laurylsulphate Chemical compound [Na+].CCCCCCCCCCCCOS([O-])(=O)=O DBMJMQXJHONAFJ-UHFFFAOYSA-M 0.000 abstract 1
- 239000004141 Sodium laurylsulphate Substances 0.000 abstract 1
- QAOWNCQODCNURD-UHFFFAOYSA-L Sulfate Chemical compound [O-]S([O-])(=O)=O QAOWNCQODCNURD-UHFFFAOYSA-L 0.000 abstract 1
- 125000002252 acyl group Chemical group 0.000 abstract 1
- 238000005054 agglomeration Methods 0.000 abstract 1
- 230000002776 aggregation Effects 0.000 abstract 1
- 229910052783 alkali metal Inorganic materials 0.000 abstract 1
- 125000003545 alkoxy group Chemical group 0.000 abstract 1
- 150000004996 alkyl benzenes Chemical class 0.000 abstract 1
- 125000000129 anionic group Chemical group 0.000 abstract 1
- 239000007795 chemical reaction product Substances 0.000 abstract 1
- 239000003795 chemical substances by application Substances 0.000 abstract 1
- 239000000470 constituent Substances 0.000 abstract 1
- 238000001816 cooling Methods 0.000 abstract 1
- 235000014113 dietary fatty acids Nutrition 0.000 abstract 1
- POULHZVOKOAJMA-UHFFFAOYSA-N dodecanoic acid Chemical class CCCCCCCCCCCC(O)=O POULHZVOKOAJMA-UHFFFAOYSA-N 0.000 abstract 1
- 150000002148 esters Chemical class 0.000 abstract 1
- 150000002170 ethers Chemical class 0.000 abstract 1
- 229920005676 ethylene-propylene block copolymer Polymers 0.000 abstract 1
- 239000000194 fatty acid Substances 0.000 abstract 1
- 229930195729 fatty acid Natural products 0.000 abstract 1
- 150000004665 fatty acids Chemical class 0.000 abstract 1
- 150000002191 fatty alcohols Chemical class 0.000 abstract 1
- 239000012467 final product Substances 0.000 abstract 1
- 239000007850 fluorescent dye Substances 0.000 abstract 1
- 239000004615 ingredient Substances 0.000 abstract 1
- 239000000594 mannitol Substances 0.000 abstract 1
- 235000010355 mannitol Nutrition 0.000 abstract 1
- 229910044991 metal oxide Inorganic materials 0.000 abstract 1
- 150000004706 metal oxides Chemical class 0.000 abstract 1
- 229910052914 metal silicate Inorganic materials 0.000 abstract 1
- SNQQPOLDUKLAAF-UHFFFAOYSA-N nonylphenol Chemical compound CCCCCCCCCC1=CC=CC=C1O SNQQPOLDUKLAAF-UHFFFAOYSA-N 0.000 abstract 1
- 229940006093 opthalmologic coloring agent diagnostic Drugs 0.000 abstract 1
- 125000005702 oxyalkylene group Chemical group 0.000 abstract 1
- 239000011236 particulate material Substances 0.000 abstract 1
- 239000002304 perfume Substances 0.000 abstract 1
- 229920002451 polyvinyl alcohol Polymers 0.000 abstract 1
- 235000011118 potassium hydroxide Nutrition 0.000 abstract 1
- 159000000001 potassium salts Chemical class 0.000 abstract 1
- OTYBMLCTZGSZBG-UHFFFAOYSA-L potassium sulfate Chemical class [K+].[K+].[O-]S([O-])(=O)=O OTYBMLCTZGSZBG-UHFFFAOYSA-L 0.000 abstract 1
- 239000001120 potassium sulphate Substances 0.000 abstract 1
- 235000011151 potassium sulphates Nutrition 0.000 abstract 1
- 238000003825 pressing Methods 0.000 abstract 1
- 238000012216 screening Methods 0.000 abstract 1
- 150000004760 silicates Chemical class 0.000 abstract 1
- 239000000377 silicon dioxide Substances 0.000 abstract 1
- FQENQNTWSFEDLI-UHFFFAOYSA-J sodium diphosphate Chemical compound [Na+].[Na+].[Na+].[Na+].[O-]P([O-])(=O)OP([O-])([O-])=O FQENQNTWSFEDLI-UHFFFAOYSA-J 0.000 abstract 1
- 235000019333 sodium laurylsulphate Nutrition 0.000 abstract 1
- 159000000000 sodium salts Chemical class 0.000 abstract 1
- PMZURENOXWZQFD-UHFFFAOYSA-L sodium sulphate Substances [Na+].[Na+].[O-]S([O-])(=O)=O PMZURENOXWZQFD-UHFFFAOYSA-L 0.000 abstract 1
- 235000011152 sodium sulphate Nutrition 0.000 abstract 1
- 235000019832 sodium triphosphate Nutrition 0.000 abstract 1
- 239000002904 solvent Substances 0.000 abstract 1
- 239000000600 sorbitol Substances 0.000 abstract 1
- 239000007921 spray Substances 0.000 abstract 1
- 238000001694 spray drying Methods 0.000 abstract 1
- 150000005846 sugar alcohols Polymers 0.000 abstract 1
- 229910021653 sulphate ion Inorganic materials 0.000 abstract 1
- 235000019818 tetrasodium diphosphate Nutrition 0.000 abstract 1
- UNXRWKVEANCORM-UHFFFAOYSA-I triphosphate(5-) Chemical compound [O-]P([O-])(=O)OP([O-])(=O)OP([O-])([O-])=O UNXRWKVEANCORM-UHFFFAOYSA-I 0.000 abstract 1
Classifications
-
- C—CHEMISTRY; METALLURGY
- C11—ANIMAL OR VEGETABLE OILS, FATS, FATTY SUBSTANCES OR WAXES; FATTY ACIDS THEREFROM; DETERGENTS; CANDLES
- C11D—DETERGENT COMPOSITIONS; USE OF SINGLE SUBSTANCES AS DETERGENTS; SOAP OR SOAP-MAKING; RESIN SOAPS; RECOVERY OF GLYCEROL
- C11D3/00—Other compounding ingredients of detergent compositions covered in group C11D1/00
- C11D3/02—Inorganic compounds ; Elemental compounds
- C11D3/04—Water-soluble compounds
- C11D3/06—Phosphates, including polyphosphates
-
- C—CHEMISTRY; METALLURGY
- C11—ANIMAL OR VEGETABLE OILS, FATS, FATTY SUBSTANCES OR WAXES; FATTY ACIDS THEREFROM; DETERGENTS; CANDLES
- C11D—DETERGENT COMPOSITIONS; USE OF SINGLE SUBSTANCES AS DETERGENTS; SOAP OR SOAP-MAKING; RESIN SOAPS; RECOVERY OF GLYCEROL
- C11D17/00—Detergent materials or soaps characterised by their shape or physical properties
- C11D17/0047—Detergents in the form of bars or tablets
- C11D17/0065—Solid detergents containing builders
- C11D17/0073—Tablets
- C11D17/0086—Laundry tablets
-
- C—CHEMISTRY; METALLURGY
- C11—ANIMAL OR VEGETABLE OILS, FATS, FATTY SUBSTANCES OR WAXES; FATTY ACIDS THEREFROM; DETERGENTS; CANDLES
- C11D—DETERGENT COMPOSITIONS; USE OF SINGLE SUBSTANCES AS DETERGENTS; SOAP OR SOAP-MAKING; RESIN SOAPS; RECOVERY OF GLYCEROL
- C11D3/00—Other compounding ingredients of detergent compositions covered in group C11D1/00
- C11D3/02—Inorganic compounds ; Elemental compounds
- C11D3/04—Water-soluble compounds
- C11D3/08—Silicates
Landscapes
- Chemical & Material Sciences (AREA)
- Life Sciences & Earth Sciences (AREA)
- Engineering & Computer Science (AREA)
- Chemical Kinetics & Catalysis (AREA)
- Oil, Petroleum & Natural Gas (AREA)
- Wood Science & Technology (AREA)
- Organic Chemistry (AREA)
- Inorganic Chemistry (AREA)
- Detergent Compositions (AREA)
Abstract
Detergent tablets, in the form of lightly compacted particles which are disintegrable in and soluble in water and are form retaining and resistant to breakage during shipment, comprise by weight 2% to 20% of an anionic and/or nonionic synthetic organic detergent, 20% to 50% of a water-soluble polyphosphate, 20% to 50% of a water-soluble metal silicate and 15% to 35% of water. Specified anionic detergents are: the sodium and potassium salts of C12-C18 alkyl benzene sulphonates; sodium lauryl sulphate, sodium coconut oil fatty acids monoglyceride sulphate and sodium salts of higher fatty acid amide of N-methyltaurine which contain a C10-C18 alkyl or acyl group. Specified nonionic detergents are condensates of C2-C4 alkylene oxides with alkyl phenols containing C6-C14 alkyl groups, each molecule containing 4 to 12 and an average of 9 to 10 alkoxy groups per molecule e.g. nonyl phenol polyoxyethylene ethanol averaging 9.5 oxyalkylene groups. Other nonionics specified are block copolymers of ethylene and propylene oxides, reaction products of higher fatty alcohols and lower alkylene oxides polyethoxy and polyalkoxy esters and ethers of polyalcohols e.g. of sorbitol and mannitol. Specified polyphosphates are pentasodium tripolyphosphate and tetrasodium pyrophosphate. Specified water soluble silicates used are alkali metal salts having a metal oxide to silica ratio, by weight, of 0.3 to 1.0. Other ingredients include potassium hydroxide, sodium and potassium sulphates, sodium carboxy methyl cellulose, colouring agents, fluorescent dyes, perfumes, bleaches, solvents and anti-redeposition agents. The detergent tablets may be made by (1) mixing the components of the tablet, moving and circulating the moistened detergent particles and finally compacting at pressures of 3 to 25 p.s.i. (2) Adding only a portion of the water to the other constituents, spray drying to produce particulate material, adding water to bring the water content up to the required level and finally pressing into tablet form as in (1). The detergent particles may also be prepared by spray cooling, agglomeration and crushing followed by screening and classification of particle size. The final product may be coated with moisture, sodium carboxy methyl cellulose or polyvinyl alcohol.
Applications Claiming Priority (2)
Application Number | Priority Date | Filing Date | Title |
---|---|---|---|
US213117A US3247123A (en) | 1962-07-30 | 1962-07-30 | Manufacture of detergent tablets |
US213116A US3247122A (en) | 1962-07-30 | 1962-07-30 | Detergent tablet and process of preparing same |
Publications (1)
Publication Number | Publication Date |
---|---|
GB995940A true GB995940A (en) | 1965-06-23 |
Family
ID=26907784
Family Applications (1)
Application Number | Title | Priority Date | Filing Date |
---|---|---|---|
GB29355/63A Expired GB995940A (en) | 1962-07-30 | 1963-07-24 | Manufacture of detergent tablets |
Country Status (13)
Country | Link |
---|---|
US (2) | US3247122A (en) |
AU (1) | AU3279063A (en) |
BE (1) | BE635589A (en) |
BR (1) | BR6351230D0 (en) |
CA (2) | CA718384A (en) |
CH (1) | CH439554A (en) |
DE (1) | DE1467564A1 (en) |
DK (1) | DK117972B (en) |
ES (1) | ES290152A1 (en) |
FR (1) | FR1387029A (en) |
GB (1) | GB995940A (en) |
MY (1) | MY6600098A (en) |
NL (1) | NL295937A (en) |
Families Citing this family (20)
Publication number | Priority date | Publication date | Assignee | Title |
---|---|---|---|---|
US3455834A (en) * | 1964-01-22 | 1969-07-15 | Colgate Palmolive Co | Process for production of detergent tablets |
US3370015A (en) * | 1964-01-30 | 1968-02-20 | Lever Brothers Ltd | Process for preparing detergent compositions |
US3392120A (en) * | 1964-03-19 | 1968-07-09 | Fmc Corp | Dry detergent mixtures |
CA795287A (en) * | 1965-03-09 | 1968-09-24 | P. Davis Robert | Detergent tablets |
US3360469A (en) * | 1965-06-07 | 1967-12-26 | Fmc Corp | Dry-mixed detergent compositions |
US3361675A (en) * | 1965-08-23 | 1968-01-02 | Fmc Corp | Dry-mixed detergent compositions |
US3408300A (en) * | 1965-12-13 | 1968-10-29 | Henkel & Cie Gmbh | Stable,alkaline,non-forming cleansing agents |
US3709837A (en) * | 1970-12-30 | 1973-01-09 | Philadelphia Quartz Co | Spray dried detergents containing sodium-potassium double silicate |
US4022704A (en) * | 1971-06-21 | 1977-05-10 | Stauffer Chemical Company | Production of spray dried, high bulk density hydrous sodium silicate mixtures |
US4370250A (en) * | 1976-12-06 | 1983-01-25 | Colgate-Palmolive Company | Detergent tablet |
US4451386A (en) * | 1976-12-06 | 1984-05-29 | Colgate-Palmolive Company | Detergent tablet |
GB2041966A (en) * | 1977-11-29 | 1980-09-17 | Procter & Gamble | Detergent tablet having a hydrated salt coating and process for preparing the tablet |
DE3541145A1 (en) * | 1985-11-21 | 1987-05-27 | Henkel Kgaa | UNIFORMED DETERGENT TABLETS FOR MACHINE DISHWASHER |
US5234615A (en) * | 1987-10-02 | 1993-08-10 | Ecolab Inc. | Article comprising a water soluble bag containing a multiple use amount of a pelletized functional material and methods of its use |
US5078301A (en) * | 1987-10-02 | 1992-01-07 | Ecolab Inc. | Article comprising a water soluble bag containing a multiple use amount of a pelletized functional material and methods of its use |
DE4010533A1 (en) * | 1990-04-02 | 1991-10-10 | Henkel Kgaa | Prodn. of high-density detergent granules |
JPH09503799A (en) * | 1993-09-13 | 1997-04-15 | ディヴァーシィ コーポレーション | Tablet-like detergent, its manufacturing and use |
DE4432130A1 (en) * | 1994-09-09 | 1996-03-14 | Henkel Kgaa | Mild detergent mixtures |
DE19709411A1 (en) * | 1997-03-07 | 1998-09-10 | Henkel Kgaa | Detergent tablets |
EP3046887A1 (en) * | 2013-09-18 | 2016-07-27 | Technion Research & Development Foundation Ltd. | Concrete formulations and admixtures therefor |
Family Cites Families (3)
Publication number | Priority date | Publication date | Assignee | Title |
---|---|---|---|---|
CA510555A (en) * | 1955-03-01 | C. Miller Robert | Detergent compositions | |
US2875155A (en) * | 1954-12-09 | 1959-02-24 | Colgate Palmolive Co | Detergent briquette and process for the production thereof |
BE632373A (en) * | 1959-12-31 |
-
0
- CA CA718383A patent/CA718383A/en not_active Expired
- CA CA718384A patent/CA718384A/en not_active Expired
- NL NL295937D patent/NL295937A/xx unknown
- BE BE635589D patent/BE635589A/xx unknown
-
1962
- 1962-07-30 US US213116A patent/US3247122A/en not_active Expired - Lifetime
- 1962-07-30 US US213117A patent/US3247123A/en not_active Expired - Lifetime
-
1963
- 1963-07-09 AU AU32790/63A patent/AU3279063A/en not_active Expired
- 1963-07-20 ES ES290152A patent/ES290152A1/en not_active Expired
- 1963-07-22 DE DE19631467564 patent/DE1467564A1/en active Pending
- 1963-07-22 DK DK348663AA patent/DK117972B/en unknown
- 1963-07-24 GB GB29355/63A patent/GB995940A/en not_active Expired
- 1963-07-25 FR FR942621A patent/FR1387029A/en not_active Expired
- 1963-07-25 CH CH928563A patent/CH439554A/en unknown
- 1963-07-29 BR BR151230/63A patent/BR6351230D0/en unknown
-
1966
- 1966-12-31 MY MY196698A patent/MY6600098A/en unknown
Also Published As
Publication number | Publication date |
---|---|
US3247123A (en) | 1966-04-19 |
BE635589A (en) | |
CH439554A (en) | 1967-07-15 |
AU3279063A (en) | 1965-01-14 |
BR6351230D0 (en) | 1973-08-28 |
US3247122A (en) | 1966-04-19 |
CA718383A (en) | 1965-09-21 |
CA718384A (en) | 1965-09-21 |
MY6600098A (en) | 1966-12-31 |
NL295937A (en) | |
DK117972B (en) | 1970-06-22 |
FR1387029A (en) | 1965-01-29 |
ES290152A1 (en) | 1963-10-16 |
DE1467564A1 (en) | 1969-10-09 |
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