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GB839172A - Preparation of organic lead compounds - Google Patents

Preparation of organic lead compounds

Info

Publication number
GB839172A
GB839172A GB24186/58A GB2418658A GB839172A GB 839172 A GB839172 A GB 839172A GB 24186/58 A GB24186/58 A GB 24186/58A GB 2418658 A GB2418658 A GB 2418658A GB 839172 A GB839172 A GB 839172A
Authority
GB
United Kingdom
Prior art keywords
lead
july
diethyl ether
organic solvent
aryl
Prior art date
Legal status (The legal status is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the status listed.)
Expired
Application number
GB24186/58A
Current Assignee (The listed assignees may be inaccurate. Google has not performed a legal analysis and makes no representation or warranty as to the accuracy of the list.)
ChampionX LLC
Original Assignee
National Aluminate Corp
Priority date (The priority date is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the date listed.)
Filing date
Publication date
Application filed by National Aluminate Corp filed Critical National Aluminate Corp
Publication of GB839172A publication Critical patent/GB839172A/en
Expired legal-status Critical Current

Links

Classifications

    • C—CHEMISTRY; METALLURGY
    • C25—ELECTROLYTIC OR ELECTROPHORETIC PROCESSES; APPARATUS THEREFOR
    • C25B—ELECTROLYTIC OR ELECTROPHORETIC PROCESSES FOR THE PRODUCTION OF COMPOUNDS OR NON-METALS; APPARATUS THEREFOR
    • C25B3/00—Electrolytic production of organic compounds
    • C25B3/01—Products
    • C25B3/13—Organo-metallic compounds

Landscapes

  • Chemical & Material Sciences (AREA)
  • Organic Chemistry (AREA)
  • Engineering & Computer Science (AREA)
  • Chemical Kinetics & Catalysis (AREA)
  • Electrochemistry (AREA)
  • Materials Engineering (AREA)
  • Metallurgy (AREA)
  • Electrolytic Production Of Non-Metals, Compounds, Apparatuses Therefor (AREA)
  • Organic Low-Molecular-Weight Compounds And Preparation Thereof (AREA)

Abstract

839,172. Lead organic compounds. NATIONAL ALUMINATE CORPORATION. July 28, 1958 [July 31, 1957], No. 24186/58. Class 41. Lead alkyl or aryl compounds are made by electrolysing a solution of a Grignard reagent dissolved in an organic solvent, using a lead anode which is consumed during the process. Diethyl ether or its homologues or tetra hydrofuran may be used as organic solvent, in which the lead alkyl or aryl produced is soluble and is separated by distillation. Polyoxyalkylene ethers may also be used as solvents when the lead compound forms a separate layer. In examples, ethyl magnesium bromide is dissolved in diethyl ether, and the electrodes are well separated, or the cathode of platinum is provided with spacers. The temperature of electrolysis is about the boiling point of the solvent and a reflux condenser is provided; alternatively the process is conducted under pressure.
GB24186/58A 1957-07-31 1958-07-28 Preparation of organic lead compounds Expired GB839172A (en)

Applications Claiming Priority (1)

Application Number Priority Date Filing Date Title
US675260A US3007857A (en) 1957-07-31 1957-07-31 Preparation of organic lead compounds

Publications (1)

Publication Number Publication Date
GB839172A true GB839172A (en) 1960-06-29

Family

ID=24709710

Family Applications (1)

Application Number Title Priority Date Filing Date
GB24186/58A Expired GB839172A (en) 1957-07-31 1958-07-28 Preparation of organic lead compounds

Country Status (5)

Country Link
US (1) US3007857A (en)
BE (1) BE569921A (en)
DE (1) DE1164406B (en)
FR (1) FR1201049A (en)
GB (1) GB839172A (en)

Cited By (5)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
US3079311A (en) * 1961-02-20 1963-02-26 Nalco Chemical Co Method of preparing tertiary phosphines
US3100181A (en) * 1961-02-16 1963-08-06 Nalco Chemical Co Preparation of organoboranes
US3234112A (en) * 1961-03-21 1966-02-08 Nalco Chemical Co Process of producing organic lead compounds
US3391066A (en) * 1959-05-06 1968-07-02 Nalco Chemical Co Preparation of organic compounds of metals
US3391067A (en) * 1959-05-06 1968-07-02 Nalco Chemical Co Electrolytic process for the preparation of mixed organic lead compounds and electrolyte therefor

Families Citing this family (5)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
NL262356A (en) * 1960-03-15 Merck & Co Inc
US3180810A (en) * 1961-07-31 1965-04-27 Standard Oil Co Electrolytic cell and method of operation
US3197392A (en) * 1961-11-30 1965-07-27 Du Pont Process for preparing organometal compounds
DE1226100B (en) * 1963-09-24 1966-10-06 Halco Chem Co Process for the production of tetraalkylene lead
DE1216303B (en) * 1963-09-24 1966-05-12 Nalco Chemical Co Electrolyte for the production of lead alkyl compounds

Family Cites Families (4)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
NL202273A (en) * 1954-11-26
BE534128A (en) * 1954-12-15
BE540052A (en) * 1955-06-13
US2944948A (en) * 1956-02-06 1960-07-12 Ethyl Corp Method of purifying organometallic complexes and their use in the preparation of organolead compounds

Cited By (5)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
US3391066A (en) * 1959-05-06 1968-07-02 Nalco Chemical Co Preparation of organic compounds of metals
US3391067A (en) * 1959-05-06 1968-07-02 Nalco Chemical Co Electrolytic process for the preparation of mixed organic lead compounds and electrolyte therefor
US3100181A (en) * 1961-02-16 1963-08-06 Nalco Chemical Co Preparation of organoboranes
US3079311A (en) * 1961-02-20 1963-02-26 Nalco Chemical Co Method of preparing tertiary phosphines
US3234112A (en) * 1961-03-21 1966-02-08 Nalco Chemical Co Process of producing organic lead compounds

Also Published As

Publication number Publication date
FR1201049A (en) 1959-12-28
US3007857A (en) 1961-11-07
DE1164406B (en) 1964-03-05
BE569921A (en)

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