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GB816398A - Preparation of metals and silicon and germanium from compounds thereof - Google Patents

Preparation of metals and silicon and germanium from compounds thereof

Info

Publication number
GB816398A
GB816398A GB2720/56A GB272056A GB816398A GB 816398 A GB816398 A GB 816398A GB 2720/56 A GB2720/56 A GB 2720/56A GB 272056 A GB272056 A GB 272056A GB 816398 A GB816398 A GB 816398A
Authority
GB
United Kingdom
Prior art keywords
hydrogen
germanium
metals
carbides
iron
Prior art date
Legal status (The legal status is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the status listed.)
Expired
Application number
GB2720/56A
Current Assignee (The listed assignees may be inaccurate. Google has not performed a legal analysis and makes no representation or warranty as to the accuracy of the list.)
Eltro GmbH and Co
Original Assignee
Eltro GmbH and Co
Priority date (The priority date is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the date listed.)
Filing date
Publication date
Application filed by Eltro GmbH and Co filed Critical Eltro GmbH and Co
Publication of GB816398A publication Critical patent/GB816398A/en
Expired legal-status Critical Current

Links

Classifications

    • C—CHEMISTRY; METALLURGY
    • C22—METALLURGY; FERROUS OR NON-FERROUS ALLOYS; TREATMENT OF ALLOYS OR NON-FERROUS METALS
    • C22B—PRODUCTION AND REFINING OF METALS; PRETREATMENT OF RAW MATERIALS
    • C22B41/00—Obtaining germanium
    • C—CHEMISTRY; METALLURGY
    • C01—INORGANIC CHEMISTRY
    • C01B—NON-METALLIC ELEMENTS; COMPOUNDS THEREOF; METALLOIDS OR COMPOUNDS THEREOF NOT COVERED BY SUBCLASS C01C
    • C01B33/00—Silicon; Compounds thereof
    • C01B33/02—Silicon
    • C01B33/021—Preparation

Landscapes

  • Chemical & Material Sciences (AREA)
  • Organic Chemistry (AREA)
  • Engineering & Computer Science (AREA)
  • Manufacturing & Machinery (AREA)
  • Materials Engineering (AREA)
  • Mechanical Engineering (AREA)
  • Metallurgy (AREA)
  • Inorganic Chemistry (AREA)
  • Carbon And Carbon Compounds (AREA)

Abstract

Germanium and other metals are produced from their refractory nitrides or carbides or from organic compounds thereof by subjecting the starting materials to the action of an atmosphere of hydrogen at a pressure of at least 100 atmospheres while heated to a temperature of at least 400 DEG C., these conditions being maintained for a period of about 50 minutes to 3 hours. The hydrogen may be mixed with nitrogen or a rare gas, at least 1 per cent of hydrogen being present in the gas mixture. Examples are given of the treatment of titanium carbide, vanadium nitride, iron oxalate and iron formate, uranyl acetate, beryllium acetate, and of a mixture of iron oxalate and nickel oxalate. Reference is also made to the treatment of the carbides or nitrides of zirconium, thorium, niobium, tantalum, chromium and uranium. The hydrogen may be circulated through a high-pressure autoclave containing the starting material, gaseous by-products of reaction being removed e.g. by freezing out with liquid air.
GB2720/56A 1955-02-04 1956-01-27 Preparation of metals and silicon and germanium from compounds thereof Expired GB816398A (en)

Applications Claiming Priority (1)

Application Number Priority Date Filing Date Title
DE816398X 1955-02-04

Publications (1)

Publication Number Publication Date
GB816398A true GB816398A (en) 1959-07-15

Family

ID=6734987

Family Applications (1)

Application Number Title Priority Date Filing Date
GB2720/56A Expired GB816398A (en) 1955-02-04 1956-01-27 Preparation of metals and silicon and germanium from compounds thereof

Country Status (1)

Country Link
GB (1) GB816398A (en)

Cited By (2)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
US4933003A (en) * 1989-07-18 1990-06-12 The United States Of America As Represented By The Secretary Of The Army Metal alloy formation by reduction of polyheterometallic complexes
US5061313A (en) * 1990-09-07 1991-10-29 Northeastern University Direct alloy synthesis from heteropolymetallic precursors

Cited By (2)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
US4933003A (en) * 1989-07-18 1990-06-12 The United States Of America As Represented By The Secretary Of The Army Metal alloy formation by reduction of polyheterometallic complexes
US5061313A (en) * 1990-09-07 1991-10-29 Northeastern University Direct alloy synthesis from heteropolymetallic precursors

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