GB647884A - Improvements in or relating to the purification of glycerol solutions - Google Patents
Improvements in or relating to the purification of glycerol solutionsInfo
- Publication number
- GB647884A GB647884A GB176947A GB176947A GB647884A GB 647884 A GB647884 A GB 647884A GB 176947 A GB176947 A GB 176947A GB 176947 A GB176947 A GB 176947A GB 647884 A GB647884 A GB 647884A
- Authority
- GB
- United Kingdom
- Prior art keywords
- esters
- soaps
- fatty acids
- glycerol
- splitting
- Prior art date
- Legal status (The legal status is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the status listed.)
- Expired
Links
Classifications
-
- C—CHEMISTRY; METALLURGY
- C11—ANIMAL OR VEGETABLE OILS, FATS, FATTY SUBSTANCES OR WAXES; FATTY ACIDS THEREFROM; DETERGENTS; CANDLES
- C11D—DETERGENT COMPOSITIONS; USE OF SINGLE SUBSTANCES AS DETERGENTS; SOAP OR SOAP-MAKING; RESIN SOAPS; RECOVERY OF GLYCEROL
- C11D19/00—Recovery of glycerol from a saponification liquor
Landscapes
- Chemical & Material Sciences (AREA)
- Life Sciences & Earth Sciences (AREA)
- Engineering & Computer Science (AREA)
- Chemical Kinetics & Catalysis (AREA)
- Oil, Petroleum & Natural Gas (AREA)
- Wood Science & Technology (AREA)
- Organic Chemistry (AREA)
- Organic Low-Molecular-Weight Compounds And Preparation Thereof (AREA)
Abstract
Alcoholic glycerol solutions containing soaps and esters resulting from the alcoholysis of glycerides are purified by splitting the soaps into fatty acids and extracting the resulting fatty acids and the esters by means of a selective solvent therefor such as aliphatic hydrocarbons (e.g. gasoline) and halogenated aliphatic hydrocarbons (e.g. trichlorethylene and carbon tetrachloride). The splitting of the soaps is preferably carried out by sulphuric acid. In cases where the alcoholic glycerol solution contains such a high proportion of soaps or esters as to cause the solvent to lose its selectivity, a proportion of the alcohol is evaporated after the solution has been treated with acid so as to increase the glycerol-alcohol ratio, whereby some of the esters and fatty acids become insoluble and settle out, after which the remainder of the esters and fatty acids are extracted by selective solvents as before. Specifications 587,523, 587,530, 587,532 and 587,533 are referred to.
Priority Applications (1)
Application Number | Priority Date | Filing Date | Title |
---|---|---|---|
GB176947A GB647884A (en) | 1947-01-20 | 1947-01-20 | Improvements in or relating to the purification of glycerol solutions |
Applications Claiming Priority (1)
Application Number | Priority Date | Filing Date | Title |
---|---|---|---|
GB176947A GB647884A (en) | 1947-01-20 | 1947-01-20 | Improvements in or relating to the purification of glycerol solutions |
Publications (1)
Publication Number | Publication Date |
---|---|
GB647884A true GB647884A (en) | 1950-12-28 |
Family
ID=9727654
Family Applications (1)
Application Number | Title | Priority Date | Filing Date |
---|---|---|---|
GB176947A Expired GB647884A (en) | 1947-01-20 | 1947-01-20 | Improvements in or relating to the purification of glycerol solutions |
Country Status (1)
Country | Link |
---|---|
GB (1) | GB647884A (en) |
-
1947
- 1947-01-20 GB GB176947A patent/GB647884A/en not_active Expired
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