GB445405A - Process for the manufacture of n-aryl-glucamines - Google Patents
Process for the manufacture of n-aryl-glucaminesInfo
- Publication number
- GB445405A GB445405A GB26954/35A GB2695435A GB445405A GB 445405 A GB445405 A GB 445405A GB 26954/35 A GB26954/35 A GB 26954/35A GB 2695435 A GB2695435 A GB 2695435A GB 445405 A GB445405 A GB 445405A
- Authority
- GB
- United Kingdom
- Prior art keywords
- acetylamino
- glucose
- monoses
- glucamine
- methylbenzene
- Prior art date
- Legal status (The legal status is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the status listed.)
- Expired
Links
Classifications
-
- C—CHEMISTRY; METALLURGY
- C10—PETROLEUM, GAS OR COKE INDUSTRIES; TECHNICAL GASES CONTAINING CARBON MONOXIDE; FUELS; LUBRICANTS; PEAT
- C10B—DESTRUCTIVE DISTILLATION OF CARBONACEOUS MATERIALS FOR PRODUCTION OF GAS, COKE, TAR, OR SIMILAR MATERIALS
- C10B1/00—Retorts
- C10B1/02—Stationary retorts
- C10B1/04—Vertical retorts
Landscapes
- Chemical & Material Sciences (AREA)
- Engineering & Computer Science (AREA)
- Oil, Petroleum & Natural Gas (AREA)
- Materials Engineering (AREA)
- Organic Chemistry (AREA)
- Organic Low-Molecular-Weight Compounds And Preparation Thereof (AREA)
Abstract
N-Arylglucamines are prepared by the catalytic hydrogenation of monoses in the presence of primary amines of the benzene series at a temperature of 90--140 DEG C. and a pressure of 15--20 atmospheres, the monoses being used in the dissolved state and nickel employed as the catalyst. The products are stable crystalline compounds, of use as intermediates for the manufacture of pharmaceutical substances. According to the examples: (1) a solution of glucose and aniline in aqueous methyl alcohol is heated with hydrogen in an autoclave in the presence of a catalyst prepared by reducing nickel carbonate mounted on kieselguhr, and phenyl-glucamine separated from the product; (2) in the same way, glucose and p-toluidine yield p-tolyl-glucamine, glucose and 4 - acetylamino - 3 - amino - 1 - methylbenzene give 4 - acetylamino - 3 - glucamino - 1 - methylbenzene, and arabinose and mono-acetyl-o-phenylenediamine produce o-acetylamino-arabinaminobenzene. British Specifications 313,617, [Class 2 (iii)], and 426,062 and French Specification 770,294 are referred to.
Applications Claiming Priority (1)
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| DE445405X | 1934-11-08 |
Publications (1)
| Publication Number | Publication Date |
|---|---|
| GB445405A true GB445405A (en) | 1936-04-08 |
Family
ID=6537752
Family Applications (1)
| Application Number | Title | Priority Date | Filing Date |
|---|---|---|---|
| GB26954/35A Expired GB445405A (en) | 1934-11-08 | 1935-09-30 | Process for the manufacture of n-aryl-glucamines |
Country Status (2)
| Country | Link |
|---|---|
| FR (2) | FR445405A (en) |
| GB (1) | GB445405A (en) |
-
1912
- 1912-06-25 FR FR445405D patent/FR445405A/en not_active Expired
-
1935
- 1935-09-30 GB GB26954/35A patent/GB445405A/en not_active Expired
- 1935-10-03 FR FR795909D patent/FR795909A/en not_active Expired
Also Published As
| Publication number | Publication date |
|---|---|
| FR795909A (en) | 1936-03-25 |
| FR445405A (en) | 1912-11-11 |
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