GB349220A - Improvements in or relating to the production of filaments, yarns, threads and other articles from natural silk - Google Patents
Improvements in or relating to the production of filaments, yarns, threads and other articles from natural silkInfo
- Publication number
- GB349220A GB349220A GB10731/30A GB1073130A GB349220A GB 349220 A GB349220 A GB 349220A GB 10731/30 A GB10731/30 A GB 10731/30A GB 1073130 A GB1073130 A GB 1073130A GB 349220 A GB349220 A GB 349220A
- Authority
- GB
- United Kingdom
- Prior art keywords
- acid
- yarns
- solution
- silk
- natural silk
- Prior art date
- Legal status (The legal status is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the status listed.)
- Expired
Links
- 239000002253 acid Substances 0.000 abstract 4
- 239000000243 solution Substances 0.000 abstract 4
- LFQSCWFLJHTTHZ-UHFFFAOYSA-N Ethanol Natural products CCO LFQSCWFLJHTTHZ-UHFFFAOYSA-N 0.000 abstract 3
- OKKJLVBELUTLKV-UHFFFAOYSA-N Methanol Chemical compound OC OKKJLVBELUTLKV-UHFFFAOYSA-N 0.000 abstract 3
- 230000001376 precipitating effect Effects 0.000 abstract 3
- VEXZGXHMUGYJMC-UHFFFAOYSA-N Hydrochloric acid Chemical compound Cl VEXZGXHMUGYJMC-UHFFFAOYSA-N 0.000 abstract 2
- NBIIXXVUZAFLBC-UHFFFAOYSA-N Phosphoric acid Chemical compound OP(O)(O)=O NBIIXXVUZAFLBC-UHFFFAOYSA-N 0.000 abstract 2
- QAOWNCQODCNURD-UHFFFAOYSA-N Sulfuric acid Chemical compound OS(O)(=O)=O QAOWNCQODCNURD-UHFFFAOYSA-N 0.000 abstract 2
- 235000019441 ethanol Nutrition 0.000 abstract 2
- 239000001117 sulphuric acid Substances 0.000 abstract 2
- 235000011149 sulphuric acid Nutrition 0.000 abstract 2
- VHUUQVKOLVNVRT-UHFFFAOYSA-N Ammonium hydroxide Chemical class [NH4+].[OH-] VHUUQVKOLVNVRT-UHFFFAOYSA-N 0.000 abstract 1
- 229920002955 Art silk Polymers 0.000 abstract 1
- 229920000742 Cotton Polymers 0.000 abstract 1
- DGAQECJNVWCQMB-PUAWFVPOSA-M Ilexoside XXIX Chemical compound C[C@@H]1CC[C@@]2(CC[C@@]3(C(=CC[C@H]4[C@]3(CC[C@@H]5[C@@]4(CC[C@@H](C5(C)C)OS(=O)(=O)[O-])C)C)[C@@H]2[C@]1(C)O)C)C(=O)O[C@H]6[C@@H]([C@H]([C@@H]([C@H](O6)CO)O)O)O.[Na+] DGAQECJNVWCQMB-PUAWFVPOSA-M 0.000 abstract 1
- ZLMJMSJWJFRBEC-UHFFFAOYSA-N Potassium Chemical compound [K] ZLMJMSJWJFRBEC-UHFFFAOYSA-N 0.000 abstract 1
- 150000001242 acetic acid derivatives Chemical class 0.000 abstract 1
- 150000001298 alcohols Chemical class 0.000 abstract 1
- 235000011114 ammonium hydroxide Nutrition 0.000 abstract 1
- 229920002678 cellulose Polymers 0.000 abstract 1
- 239000001913 cellulose Substances 0.000 abstract 1
- 229920002301 cellulose acetate Polymers 0.000 abstract 1
- 239000003795 chemical substances by application Substances 0.000 abstract 1
- 230000006866 deterioration Effects 0.000 abstract 1
- 239000003085 diluting agent Substances 0.000 abstract 1
- 125000001495 ethyl group Chemical group [H]C([H])([H])C([H])([H])* 0.000 abstract 1
- 238000007689 inspection Methods 0.000 abstract 1
- 239000000463 material Substances 0.000 abstract 1
- 238000000034 method Methods 0.000 abstract 1
- 230000003472 neutralizing effect Effects 0.000 abstract 1
- 235000011007 phosphoric acid Nutrition 0.000 abstract 1
- 229910052700 potassium Inorganic materials 0.000 abstract 1
- 239000011591 potassium Substances 0.000 abstract 1
- 235000011118 potassium hydroxide Nutrition 0.000 abstract 1
- 238000001556 precipitation Methods 0.000 abstract 1
- 239000012266 salt solution Substances 0.000 abstract 1
- 229910052708 sodium Inorganic materials 0.000 abstract 1
- 239000011734 sodium Substances 0.000 abstract 1
- 235000011121 sodium hydroxide Nutrition 0.000 abstract 1
- 238000009987 spinning Methods 0.000 abstract 1
- 239000000126 substance Substances 0.000 abstract 1
- 239000004753 textile Substances 0.000 abstract 1
- XLYOFNOQVPJJNP-UHFFFAOYSA-N water Substances O XLYOFNOQVPJJNP-UHFFFAOYSA-N 0.000 abstract 1
- 238000004804 winding Methods 0.000 abstract 1
- 210000002268 wool Anatomy 0.000 abstract 1
Classifications
-
- D—TEXTILES; PAPER
- D01—NATURAL OR MAN-MADE THREADS OR FIBRES; SPINNING
- D01F—CHEMICAL FEATURES IN THE MANUFACTURE OF ARTIFICIAL FILAMENTS, THREADS, FIBRES, BRISTLES OR RIBBONS; APPARATUS SPECIALLY ADAPTED FOR THE MANUFACTURE OF CARBON FILAMENTS
- D01F4/00—Monocomponent artificial filaments or the like of proteins; Manufacture thereof
- D01F4/02—Monocomponent artificial filaments or the like of proteins; Manufacture thereof from fibroin
Landscapes
- Chemical & Material Sciences (AREA)
- Chemical Kinetics & Catalysis (AREA)
- General Chemical & Material Sciences (AREA)
- Engineering & Computer Science (AREA)
- Textile Engineering (AREA)
- Artificial Filaments (AREA)
- Chemical Or Physical Treatment Of Fibers (AREA)
- Treatments For Attaching Organic Compounds To Fibrous Goods (AREA)
Abstract
Albumens and albuminoids, processes for making artificial silk and like textile materials from; albumens and albuminoids, films or sheets containing.-Filaments, threads, yarns, bristles and other articles are formed by dissolving natural silk in an acid, imparting to the solution the desired shape and then subjecting the solution to the action of a precipitating agent comprising one or more alcohols, e.g. ethyl or methyl alcohol. A strong acid is preferably employed, but not sufficiently strong to impair the silk at the temperature employed. Sulphuric acid of 25-75 per cent, syrupy orthophosphoric acid and hydrochloric acid are specified. To prevent deterioration, low temperatures are employed, e.g. from -10 DEG C. to 10 DEG C., and are preferably maintained during storage, if any, and precipitation. The solution is extruded to form light or heavy filaments. The precipitating bath is preferably of large volume and may include a diluent for the acid and/or neutralizing substances, e.g. sodium, potassium or ammonium hydroxides or acetates. Yarns produced by the invention may be associated with other yarns, e.g. natural silk, cotton, wool or yarns of cellulose acetate or other organic derivatives of cellulose. In an example, 8 kg. of degummed natural silk is added to 25 litres of 50 per cent sulphuric acid cooled to about 0 DEG C., and the cold solution is extruded into a large bath of ethyl alcohol kept at about 0 DEG . The spun threads may be wound by a cup-spinning device, centrifugal pot, &c. and are thoroughly washed to remove traces of acid either prior or subsequent to winding. The Specification as open to inspection under Sect. 91 (3) (a) states that the precipitating bath may consist of water or dilute aqueous salt solutions. This subject-matter does not appear in the Specification as accepted.
Applications Claiming Priority (1)
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| US356597A US1936753A (en) | 1929-04-19 | 1929-04-19 | Method of making silk products |
Publications (1)
| Publication Number | Publication Date |
|---|---|
| GB349220A true GB349220A (en) | 1931-05-28 |
Family
ID=23402115
Family Applications (1)
| Application Number | Title | Priority Date | Filing Date |
|---|---|---|---|
| GB10731/30A Expired GB349220A (en) | 1929-04-19 | 1930-04-04 | Improvements in or relating to the production of filaments, yarns, threads and other articles from natural silk |
Country Status (2)
| Country | Link |
|---|---|
| US (1) | US1936753A (en) |
| GB (1) | GB349220A (en) |
Families Citing this family (5)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| US2733975A (en) * | 1956-02-07 | Process of coating and dyeing textile | ||
| US2472267A (en) * | 1945-08-17 | 1949-06-07 | Henry C Reitz | Process for preparing gluten sulfate and salts thereof |
| US2592120A (en) * | 1949-02-16 | 1952-04-08 | Eastman Kodak Co | Preparation of globular protein solutions |
| NL71084C (en) * | 1949-05-20 | |||
| CN100346012C (en) * | 2005-08-19 | 2007-10-31 | 刘小鹏 | Extraction method of silk from silkworm silk gland |
-
1929
- 1929-04-19 US US356597A patent/US1936753A/en not_active Expired - Lifetime
-
1930
- 1930-04-04 GB GB10731/30A patent/GB349220A/en not_active Expired
Also Published As
| Publication number | Publication date |
|---|---|
| US1936753A (en) | 1933-11-28 |
Similar Documents
| Publication | Publication Date | Title |
|---|---|---|
| GB339089A (en) | Process for making artificial threads, hairs, bands or the like from solutions of silk fibroin | |
| GB349220A (en) | Improvements in or relating to the production of filaments, yarns, threads and other articles from natural silk | |
| GB456061A (en) | Improvements in the manufacture of artificial threads or the like | |
| US2250375A (en) | Manufacture and production of artificial threads, filaments, films, and the like | |
| GB652844A (en) | Improvements in and relating to the production of artificial threads, fibres, filaments, staple fibres and the like | |
| GB343062A (en) | Improvements in the production of artificial filaments, films and like materials | |
| GB385005A (en) | Improvements relating to the manufacture of artificial silk | |
| GB475368A (en) | Improvements in or relating to the manufacture of threads and films made from cellulose acetate | |
| US1920188A (en) | Production of artificial materials | |
| GB352445A (en) | Improved treatment of artificial threads and films made from cellulose esters and ethers | |
| GB328911A (en) | Improvements in or relating to the manufacture of filaments, threads, films or other products from cellulose derivatives | |
| GB831065A (en) | Improvements in and relating to the manufacture of threads, fibres, filaments and the like from viscose | |
| GB493288A (en) | Manufacture of substitutes for wool from viscose | |
| DE610226C (en) | Manufacture of artificial structures from solutions of cellulose acetate in organic acids by the stretch spinning process | |
| GB437595A (en) | Improvements in the manufacture or treatment of artificial filaments, yarns, films and similar materials | |
| US1633221A (en) | William me | |
| GB344751A (en) | Improved process for producing artificial silk from viscose | |
| GB370943A (en) | Improvements relating to the manufacture of artificial silk | |
| GB356343A (en) | ||
| GB334838A (en) | Improvements in the production of artificial threads, filaments, ribbons, films or the like from cellulose derivatives | |
| GB385516A (en) | Method of manufacturing artificial silk | |
| GB563960A (en) | Improvements in or relating to the production of textile and other products from polyvinyl esters | |
| GB444517A (en) | Improvements in and relating to the spinning of artificial silk | |
| GB348959A (en) | Manufacture of artificial fibres and films from cellulose esters | |
| GB362785A (en) | Manufacture of artificial threads, bands, films and the like |