GB1501673A - Process for the manufacture of alkyl-tin trihalides - Google Patents
Process for the manufacture of alkyl-tin trihalidesInfo
- Publication number
- GB1501673A GB1501673A GB38391/75A GB3839175A GB1501673A GB 1501673 A GB1501673 A GB 1501673A GB 38391/75 A GB38391/75 A GB 38391/75A GB 3839175 A GB3839175 A GB 3839175A GB 1501673 A GB1501673 A GB 1501673A
- Authority
- GB
- United Kingdom
- Prior art keywords
- alkyl
- aluminium
- tin
- sept
- ether
- Prior art date
- Legal status (The legal status is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the status listed.)
- Expired
Links
- 238000004519 manufacturing process Methods 0.000 title 1
- 238000000034 method Methods 0.000 title 1
- RTZKZFJDLAIYFH-UHFFFAOYSA-N Diethyl ether Chemical compound CCOCC RTZKZFJDLAIYFH-UHFFFAOYSA-N 0.000 abstract 5
- ZMANZCXQSJIPKH-UHFFFAOYSA-N Triethylamine Chemical compound CCN(CC)CC ZMANZCXQSJIPKH-UHFFFAOYSA-N 0.000 abstract 3
- -1 alkyl tin Chemical compound 0.000 abstract 3
- 229910052782 aluminium Inorganic materials 0.000 abstract 3
- JUJWROOIHBZHMG-UHFFFAOYSA-N Pyridine Chemical compound C1=CC=NC=C1 JUJWROOIHBZHMG-UHFFFAOYSA-N 0.000 abstract 2
- ATJFFYVFTNAWJD-UHFFFAOYSA-N Tin Chemical compound [Sn] ATJFFYVFTNAWJD-UHFFFAOYSA-N 0.000 abstract 2
- XAGFODPZIPBFFR-UHFFFAOYSA-N aluminium Chemical compound [Al] XAGFODPZIPBFFR-UHFFFAOYSA-N 0.000 abstract 2
- 239000004411 aluminium Substances 0.000 abstract 2
- RDOXTESZEPMUJZ-UHFFFAOYSA-N anisole Chemical compound COC1=CC=CC=C1 RDOXTESZEPMUJZ-UHFFFAOYSA-N 0.000 abstract 2
- RYHBNJHYFVUHQT-UHFFFAOYSA-N 1,4-Dioxane Chemical compound C1COCCO1 RYHBNJHYFVUHQT-UHFFFAOYSA-N 0.000 abstract 1
- DURPTKYDGMDSBL-UHFFFAOYSA-N 1-butoxybutane Chemical compound CCCCOCCCC DURPTKYDGMDSBL-UHFFFAOYSA-N 0.000 abstract 1
- JLTDJTHDQAWBAV-UHFFFAOYSA-N N,N-dimethylaniline Chemical compound CN(C)C1=CC=CC=C1 JLTDJTHDQAWBAV-UHFFFAOYSA-N 0.000 abstract 1
- WYURNTSHIVDZCO-UHFFFAOYSA-N Tetrahydrofuran Chemical compound C1CCOC1 WYURNTSHIVDZCO-UHFFFAOYSA-N 0.000 abstract 1
- 150000001399 aluminium compounds Chemical class 0.000 abstract 1
- 239000008139 complexing agent Substances 0.000 abstract 1
- UZKWTJUDCOPSNM-UHFFFAOYSA-N methoxybenzene Substances CCCCOC=C UZKWTJUDCOPSNM-UHFFFAOYSA-N 0.000 abstract 1
- UMJSCPRVCHMLSP-UHFFFAOYSA-N pyridine Natural products COC1=CC=CN=C1 UMJSCPRVCHMLSP-UHFFFAOYSA-N 0.000 abstract 1
- 239000000376 reactant Substances 0.000 abstract 1
- 150000003512 tertiary amines Chemical class 0.000 abstract 1
Classifications
-
- C—CHEMISTRY; METALLURGY
- C07—ORGANIC CHEMISTRY
- C07F—ACYCLIC, CARBOCYCLIC OR HETEROCYCLIC COMPOUNDS CONTAINING ELEMENTS OTHER THAN CARBON, HYDROGEN, HALOGEN, OXYGEN, NITROGEN, SULFUR, SELENIUM OR TELLURIUM
- C07F7/00—Compounds containing elements of Groups 4 or 14 of the Periodic Table
- C07F7/22—Tin compounds
- C07F7/2208—Compounds having tin linked only to carbon, hydrogen and/or halogen
Landscapes
- Chemical & Material Sciences (AREA)
- Organic Chemistry (AREA)
- Low-Molecular Organic Synthesis Reactions Using Catalysts (AREA)
- Organic Low-Molecular-Weight Compounds And Preparation Thereof (AREA)
Abstract
1501673 Preparing alkyl tin trihalides SCHERING AG 18 Sept 1975 [19 Sept 1974] 38391/75 Heading C2J An alkyl tin trihalide is prepared by reacting an aluminium trialkyl or an alkyl aluminium halide with a tin tetrahalide, the aluminium compound being in the form of a donor complex with an ether or a tertiary amine and at no stage of the reaction being present in more than the stoichiometric amount required for monoalkylation of the tin tetrahalide. The complexing agent may particularly be diethyl ether, di-n-butyl ether, THF, dioxan, anisole, triethylamine, pyridine or dimethylaniline. In Examples, the aluminium reactants used are (C 4 H 9 ) 3 Al, (C 8 H 17 ) 3 Al, (C 18 H 37 ) 3 Al and C 8 H 17 - AlCl 2 .
Applications Claiming Priority (1)
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| DE19742444786 DE2444786C3 (en) | 1974-09-19 | Process for the preparation of alkyl tin tri chlorides |
Publications (1)
| Publication Number | Publication Date |
|---|---|
| GB1501673A true GB1501673A (en) | 1978-02-22 |
Family
ID=5926207
Family Applications (1)
| Application Number | Title | Priority Date | Filing Date |
|---|---|---|---|
| GB38391/75A Expired GB1501673A (en) | 1974-09-19 | 1975-09-18 | Process for the manufacture of alkyl-tin trihalides |
Country Status (9)
| Country | Link |
|---|---|
| JP (1) | JPS5918398B2 (en) |
| BE (1) | BE833621A (en) |
| DK (1) | DK284875A (en) |
| ES (1) | ES439161A1 (en) |
| FR (1) | FR2285393A1 (en) |
| GB (1) | GB1501673A (en) |
| NL (1) | NL181108C (en) |
| SU (1) | SU598566A3 (en) |
| ZA (1) | ZA755980B (en) |
Cited By (2)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| EP1389620A1 (en) * | 2002-08-08 | 2004-02-18 | Crompton GmbH | Process for the preparation of mono- and dialkyltin halogen compounds and use thereof |
| EP3037425A1 (en) | 2014-12-23 | 2016-06-29 | Chemtura Corporation | A process for purifying monooctyltin trichloride |
Families Citing this family (1)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| JP7301759B2 (en) * | 2017-06-30 | 2023-07-03 | タタ、スティール、ネダーランド、テクノロジー、ベスローテン、フェンノートシャップ | Hot-dip plating apparatus and method |
-
1975
- 1975-06-24 DK DK284875A patent/DK284875A/en unknown
- 1975-07-04 ES ES439161A patent/ES439161A1/en not_active Expired
- 1975-09-15 NL NLAANVRAGE7510816,A patent/NL181108C/en not_active IP Right Cessation
- 1975-09-18 GB GB38391/75A patent/GB1501673A/en not_active Expired
- 1975-09-18 SU SU752174306A patent/SU598566A3/en active
- 1975-09-19 ZA ZA00755980A patent/ZA755980B/en unknown
- 1975-09-19 BE BE160206A patent/BE833621A/en not_active IP Right Cessation
- 1975-09-19 JP JP50113521A patent/JPS5918398B2/en not_active Expired
- 1975-09-19 FR FR7528740A patent/FR2285393A1/en active Granted
Cited By (5)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| EP1389620A1 (en) * | 2002-08-08 | 2004-02-18 | Crompton GmbH | Process for the preparation of mono- and dialkyltin halogen compounds and use thereof |
| US6846944B2 (en) | 2002-08-08 | 2005-01-25 | Crompton Gmbh | Process for preparing monoalkyltin halides and dialkyltin halides and their use |
| EP3037425A1 (en) | 2014-12-23 | 2016-06-29 | Chemtura Corporation | A process for purifying monooctyltin trichloride |
| WO2016103011A1 (en) | 2014-12-23 | 2016-06-30 | Chemtura Corporation | A process for purifying monooctylin trichloride |
| US10174060B2 (en) | 2014-12-23 | 2019-01-08 | Lanxess Organometallics Gmbh | Process for purifying monooctylin trichloride |
Also Published As
| Publication number | Publication date |
|---|---|
| NL181108C (en) | 1987-06-16 |
| ES439161A1 (en) | 1977-03-01 |
| SU598566A3 (en) | 1978-03-15 |
| BE833621A (en) | 1976-03-19 |
| DE2444786A1 (en) | 1976-04-08 |
| FR2285393A1 (en) | 1976-04-16 |
| FR2285393B1 (en) | 1978-08-18 |
| AU8482075A (en) | 1977-03-24 |
| DK284875A (en) | 1976-03-20 |
| JPS5156417A (en) | 1976-05-18 |
| DE2444786B2 (en) | 1976-11-11 |
| ZA755980B (en) | 1976-08-25 |
| NL7510816A (en) | 1976-03-23 |
| NL181108B (en) | 1987-01-16 |
| JPS5918398B2 (en) | 1984-04-26 |
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Legal Events
| Date | Code | Title | Description |
|---|---|---|---|
| PS | Patent sealed | ||
| PCNP | Patent ceased through non-payment of renewal fee |
Effective date: 19940918 |