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GB1082188A - Process for the separation of a mixture containing hydrocarbons - Google Patents

Process for the separation of a mixture containing hydrocarbons

Info

Publication number
GB1082188A
GB1082188A GB13784/66A GB1378466A GB1082188A GB 1082188 A GB1082188 A GB 1082188A GB 13784/66 A GB13784/66 A GB 13784/66A GB 1378466 A GB1378466 A GB 1378466A GB 1082188 A GB1082188 A GB 1082188A
Authority
GB
United Kingdom
Prior art keywords
column
solvent
sulpholane
extract
mixture
Prior art date
Legal status (The legal status is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the status listed.)
Expired
Application number
GB13784/66A
Current Assignee (The listed assignees may be inaccurate. Google has not performed a legal analysis and makes no representation or warranty as to the accuracy of the list.)
Shell Internationale Research Maatschappij BV
Original Assignee
Shell Internationale Research Maatschappij BV
Priority date (The priority date is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the date listed.)
Filing date
Publication date
Application filed by Shell Internationale Research Maatschappij BV filed Critical Shell Internationale Research Maatschappij BV
Publication of GB1082188A publication Critical patent/GB1082188A/en
Expired legal-status Critical Current

Links

Classifications

    • B—PERFORMING OPERATIONS; TRANSPORTING
    • B01—PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
    • B01D—SEPARATION
    • B01D11/00—Solvent extraction
    • B01D11/04—Solvent extraction of solutions which are liquid
    • B01D11/0488—Flow sheets
    • C—CHEMISTRY; METALLURGY
    • C10—PETROLEUM, GAS OR COKE INDUSTRIES; TECHNICAL GASES CONTAINING CARBON MONOXIDE; FUELS; LUBRICANTS; PEAT
    • C10G—CRACKING HYDROCARBON OILS; PRODUCTION OF LIQUID HYDROCARBON MIXTURES, e.g. BY DESTRUCTIVE HYDROGENATION, OLIGOMERISATION, POLYMERISATION; RECOVERY OF HYDROCARBON OILS FROM OIL-SHALE, OIL-SAND, OR GASES; REFINING MIXTURES MAINLY CONSISTING OF HYDROCARBONS; REFORMING OF NAPHTHA; MINERAL WAXES
    • C10G21/00—Refining of hydrocarbon oils, in the absence of hydrogen, by extraction with selective solvents
    • C10G21/28—Recovery of used solvent

Landscapes

  • Chemical & Material Sciences (AREA)
  • Chemical Kinetics & Catalysis (AREA)
  • Oil, Petroleum & Natural Gas (AREA)
  • Engineering & Computer Science (AREA)
  • General Chemical & Material Sciences (AREA)
  • Organic Chemistry (AREA)
  • Production Of Liquid Hydrocarbon Mixture For Refining Petroleum (AREA)
  • Organic Low-Molecular-Weight Compounds And Preparation Thereof (AREA)
  • Extraction Or Liquid Replacement (AREA)

Abstract

In a process for separating a hydrocarbon mixture by means of liquid-liquid extraction by a selective solvent boiling higher than the mixture, a raffinate and an extract phase being obtained, the extract phase being separated into solvent and an extract, and solvent being recovered from the raffinate and/or the extract by washing at least one of these by means of an aqueous washing medium, the used washing medium is then treated for recovery of solvent therefrom by contacting it with a hydrocarbon-containing mixture, e.g. the incoming feed hydrocarbon mixture. Additional solvent may be recovered from the contacted used washing medium by distillation, and the finally treated aqueous washing medium may be recycled. Suitable solvents are of the sulpholane or glycol type, examples being given, and the process is particularly suitable for recovering aromatics from kerosene or catalytic reformates. In the illustrated embodiment, feed hydrocarbon 1 is used to wash a water/sulpholane mixture 7 <PICT:1082188/C4-C5/1> in column 3, the solvent-freed water leaving at 5, and the hydrocarbon/sulpholane mixture 8 then being countercurrently contacted in column 9 with sulpholane 11. The extract 15 is then stripped in column 17 to give a non-aromatic extract which is returned to column 9, and an aromatic extract 21 which is passed to column 23 where sulpholane is separated and recycled to column 9. The raffinate 13 from column 9 and the aromatics 25 from column 23 are separately washed for removal of solvent by water 28 and 33 in columns 27 and 32, respectively, the used water now containing sulpholane being combined as stream 7 which is passed to unit 3 for contact with incoming feed. The washed raffinate and aromatics are recovered as 29 and 35 respectively.
GB13784/66A 1965-03-31 1965-03-29 Process for the separation of a mixture containing hydrocarbons Expired GB1082188A (en)

Applications Claiming Priority (1)

Application Number Priority Date Filing Date Title
US444366A US3308059A (en) 1965-03-31 1965-03-31 Sulfolane solvent recovery from water wash

Publications (1)

Publication Number Publication Date
GB1082188A true GB1082188A (en) 1967-09-06

Family

ID=23764595

Family Applications (1)

Application Number Title Priority Date Filing Date
GB13784/66A Expired GB1082188A (en) 1965-03-31 1965-03-29 Process for the separation of a mixture containing hydrocarbons

Country Status (8)

Country Link
US (1) US3308059A (en)
AT (1) AT275695B (en)
BE (1) BE678610A (en)
DE (1) DE1545376A1 (en)
DK (1) DK116017B (en)
ES (1) ES324828A1 (en)
GB (1) GB1082188A (en)
NL (1) NL6604095A (en)

Cited By (1)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
FR2128740A1 (en) * 1971-03-08 1972-10-20 Petrolchemisches Kombinat Solvent extraction of aromatics - giving higher yield or purity

Families Citing this family (5)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
US3457166A (en) * 1966-12-16 1969-07-22 Universal Oil Prod Co Separation method for purifying an edible oil solvent
US3429802A (en) * 1966-12-16 1969-02-25 Universal Oil Prod Co Method for producing a solvent for edible oils
US3492222A (en) * 1967-11-14 1970-01-27 Universal Oil Prod Co Solvent recovery process
US4353794A (en) * 1980-11-26 1982-10-12 Uop Inc. Process for the solvent extraction of aromatics and the recovery of an aromatics-free non-aromatic product from a hydrocarbon feedstock
US7959102B2 (en) * 2007-10-12 2011-06-14 Swiss Winding Performance Ag Winder for a meterial web of flexible material

Family Cites Families (2)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
US2999892A (en) * 1958-09-02 1961-09-12 Shell Oil Co Solvent extraction process
BE622633A (en) * 1961-09-21

Cited By (1)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
FR2128740A1 (en) * 1971-03-08 1972-10-20 Petrolchemisches Kombinat Solvent extraction of aromatics - giving higher yield or purity

Also Published As

Publication number Publication date
NL6604095A (en) 1966-10-03
DE1545376A1 (en) 1970-01-22
ES324828A1 (en) 1967-02-16
DK116017B (en) 1969-12-01
BE678610A (en) 1966-09-29
AT275695B (en) 1969-11-10
US3308059A (en) 1967-03-07

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