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FR3130830B1 - Procédé de captation de mercaptans mettant en œuvre une masse de captation mésoporeuse - Google Patents

Procédé de captation de mercaptans mettant en œuvre une masse de captation mésoporeuse Download PDF

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Publication number
FR3130830B1
FR3130830B1 FR2113808A FR2113808A FR3130830B1 FR 3130830 B1 FR3130830 B1 FR 3130830B1 FR 2113808 A FR2113808 A FR 2113808A FR 2113808 A FR2113808 A FR 2113808A FR 3130830 B1 FR3130830 B1 FR 3130830B1
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France
Prior art keywords
capture mass
volume
capturing
mercaptans
mesoporous
Prior art date
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Application number
FR2113808A
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English (en)
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FR3130830A1 (fr
Inventor
Antoine Fecant
Antoine Hugon
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IFP Energies Nouvelles IFPEN
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IFP Energies Nouvelles IFPEN
Priority date (The priority date is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the date listed.)
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Publication date
Priority to FR2113808A priority Critical patent/FR3130830B1/fr
Application filed by IFP Energies Nouvelles IFPEN filed Critical IFP Energies Nouvelles IFPEN
Priority to PCT/EP2022/085350 priority patent/WO2023110728A1/fr
Priority to US18/718,860 priority patent/US20250043198A1/en
Priority to EP22835371.0A priority patent/EP4448689A1/fr
Priority to JP2024535622A priority patent/JP2025502658A/ja
Priority to MX2024006866A priority patent/MX2024006866A/es
Priority to AU2022413308A priority patent/AU2022413308A1/en
Priority to KR1020247019659A priority patent/KR20240121752A/ko
Priority to CN202280083717.XA priority patent/CN118434830A/zh
Priority to ARP220103450A priority patent/AR127980A1/es
Publication of FR3130830A1 publication Critical patent/FR3130830A1/fr
Application granted granted Critical
Publication of FR3130830B1 publication Critical patent/FR3130830B1/fr
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Classifications

    • C—CHEMISTRY; METALLURGY
    • C10—PETROLEUM, GAS OR COKE INDUSTRIES; TECHNICAL GASES CONTAINING CARBON MONOXIDE; FUELS; LUBRICANTS; PEAT
    • C10G—CRACKING HYDROCARBON OILS; PRODUCTION OF LIQUID HYDROCARBON MIXTURES, e.g. BY DESTRUCTIVE HYDROGENATION, OLIGOMERISATION, POLYMERISATION; RECOVERY OF HYDROCARBON OILS FROM OIL-SHALE, OIL-SAND, OR GASES; REFINING MIXTURES MAINLY CONSISTING OF HYDROCARBONS; REFORMING OF NAPHTHA; MINERAL WAXES
    • C10G25/00—Refining of hydrocarbon oils in the absence of hydrogen, with solid sorbents
    • C10G25/02—Refining of hydrocarbon oils in the absence of hydrogen, with solid sorbents with ion-exchange material
    • C10G25/03—Refining of hydrocarbon oils in the absence of hydrogen, with solid sorbents with ion-exchange material with crystalline alumino-silicates, e.g. molecular sieves
    • C10G25/05—Removal of non-hydrocarbon compounds, e.g. sulfur compounds
    • B—PERFORMING OPERATIONS; TRANSPORTING
    • B01—PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
    • B01J—CHEMICAL OR PHYSICAL PROCESSES, e.g. CATALYSIS OR COLLOID CHEMISTRY; THEIR RELEVANT APPARATUS
    • B01J21/00—Catalysts comprising the elements, oxides, or hydroxides of magnesium, boron, aluminium, carbon, silicon, titanium, zirconium, or hafnium
    • B01J21/02—Boron or aluminium; Oxides or hydroxides thereof
    • B01J21/04—Alumina
    • B—PERFORMING OPERATIONS; TRANSPORTING
    • B01—PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
    • B01J—CHEMICAL OR PHYSICAL PROCESSES, e.g. CATALYSIS OR COLLOID CHEMISTRY; THEIR RELEVANT APPARATUS
    • B01J23/00—Catalysts comprising metals or metal oxides or hydroxides, not provided for in group B01J21/00
    • B01J23/70—Catalysts comprising metals or metal oxides or hydroxides, not provided for in group B01J21/00 of the iron group metals or copper
    • B01J23/74—Iron group metals
    • B01J23/755—Nickel
    • B—PERFORMING OPERATIONS; TRANSPORTING
    • B01—PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
    • B01J—CHEMICAL OR PHYSICAL PROCESSES, e.g. CATALYSIS OR COLLOID CHEMISTRY; THEIR RELEVANT APPARATUS
    • B01J23/00—Catalysts comprising metals or metal oxides or hydroxides, not provided for in group B01J21/00
    • B01J23/70—Catalysts comprising metals or metal oxides or hydroxides, not provided for in group B01J21/00 of the iron group metals or copper
    • B01J23/76—Catalysts comprising metals or metal oxides or hydroxides, not provided for in group B01J21/00 of the iron group metals or copper combined with metals, oxides or hydroxides provided for in groups B01J23/02 - B01J23/36
    • B01J23/84—Catalysts comprising metals or metal oxides or hydroxides, not provided for in group B01J21/00 of the iron group metals or copper combined with metals, oxides or hydroxides provided for in groups B01J23/02 - B01J23/36 with arsenic, antimony, bismuth, vanadium, niobium, tantalum, polonium, chromium, molybdenum, tungsten, manganese, technetium or rhenium
    • B01J23/85—Chromium, molybdenum or tungsten
    • B—PERFORMING OPERATIONS; TRANSPORTING
    • B01—PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
    • B01J—CHEMICAL OR PHYSICAL PROCESSES, e.g. CATALYSIS OR COLLOID CHEMISTRY; THEIR RELEVANT APPARATUS
    • B01J35/00—Catalysts, in general, characterised by their form or physical properties
    • B01J35/60—Catalysts, in general, characterised by their form or physical properties characterised by their surface properties or porosity
    • B01J35/61—Surface area
    • B01J35/615—100-500 m2/g
    • B—PERFORMING OPERATIONS; TRANSPORTING
    • B01—PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
    • B01J—CHEMICAL OR PHYSICAL PROCESSES, e.g. CATALYSIS OR COLLOID CHEMISTRY; THEIR RELEVANT APPARATUS
    • B01J35/00—Catalysts, in general, characterised by their form or physical properties
    • B01J35/60—Catalysts, in general, characterised by their form or physical properties characterised by their surface properties or porosity
    • B01J35/63—Pore volume
    • B01J35/633—Pore volume less than 0.5 ml/g
    • B—PERFORMING OPERATIONS; TRANSPORTING
    • B01—PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
    • B01J—CHEMICAL OR PHYSICAL PROCESSES, e.g. CATALYSIS OR COLLOID CHEMISTRY; THEIR RELEVANT APPARATUS
    • B01J37/00—Processes, in general, for preparing catalysts; Processes, in general, for activation of catalysts
    • B01J37/02—Impregnation, coating or precipitation
    • B01J37/0201—Impregnation
    • B—PERFORMING OPERATIONS; TRANSPORTING
    • B01—PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
    • B01J—CHEMICAL OR PHYSICAL PROCESSES, e.g. CATALYSIS OR COLLOID CHEMISTRY; THEIR RELEVANT APPARATUS
    • B01J37/00—Processes, in general, for preparing catalysts; Processes, in general, for activation of catalysts
    • B01J37/02—Impregnation, coating or precipitation
    • B01J37/0236—Drying, e.g. preparing a suspension, adding a soluble salt and drying
    • B—PERFORMING OPERATIONS; TRANSPORTING
    • B01—PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
    • B01J—CHEMICAL OR PHYSICAL PROCESSES, e.g. CATALYSIS OR COLLOID CHEMISTRY; THEIR RELEVANT APPARATUS
    • B01J37/00—Processes, in general, for preparing catalysts; Processes, in general, for activation of catalysts
    • B01J37/08—Heat treatment
    • B01J37/082—Decomposition and pyrolysis
    • B01J37/088—Decomposition of a metal salt
    • C—CHEMISTRY; METALLURGY
    • C10—PETROLEUM, GAS OR COKE INDUSTRIES; TECHNICAL GASES CONTAINING CARBON MONOXIDE; FUELS; LUBRICANTS; PEAT
    • C10G—CRACKING HYDROCARBON OILS; PRODUCTION OF LIQUID HYDROCARBON MIXTURES, e.g. BY DESTRUCTIVE HYDROGENATION, OLIGOMERISATION, POLYMERISATION; RECOVERY OF HYDROCARBON OILS FROM OIL-SHALE, OIL-SAND, OR GASES; REFINING MIXTURES MAINLY CONSISTING OF HYDROCARBONS; REFORMING OF NAPHTHA; MINERAL WAXES
    • C10G25/00—Refining of hydrocarbon oils in the absence of hydrogen, with solid sorbents
    • C10G25/003—Specific sorbent material, not covered by C10G25/02 or C10G25/03
    • C—CHEMISTRY; METALLURGY
    • C10—PETROLEUM, GAS OR COKE INDUSTRIES; TECHNICAL GASES CONTAINING CARBON MONOXIDE; FUELS; LUBRICANTS; PEAT
    • C10G—CRACKING HYDROCARBON OILS; PRODUCTION OF LIQUID HYDROCARBON MIXTURES, e.g. BY DESTRUCTIVE HYDROGENATION, OLIGOMERISATION, POLYMERISATION; RECOVERY OF HYDROCARBON OILS FROM OIL-SHALE, OIL-SAND, OR GASES; REFINING MIXTURES MAINLY CONSISTING OF HYDROCARBONS; REFORMING OF NAPHTHA; MINERAL WAXES
    • C10G67/00—Treatment of hydrocarbon oils by at least one hydrotreatment process and at least one process for refining in the absence of hydrogen only
    • C10G67/02—Treatment of hydrocarbon oils by at least one hydrotreatment process and at least one process for refining in the absence of hydrogen only plural serial stages only
    • C10G67/06—Treatment of hydrocarbon oils by at least one hydrotreatment process and at least one process for refining in the absence of hydrogen only plural serial stages only including a sorption process as the refining step in the absence of hydrogen
    • C—CHEMISTRY; METALLURGY
    • C10—PETROLEUM, GAS OR COKE INDUSTRIES; TECHNICAL GASES CONTAINING CARBON MONOXIDE; FUELS; LUBRICANTS; PEAT
    • C10G—CRACKING HYDROCARBON OILS; PRODUCTION OF LIQUID HYDROCARBON MIXTURES, e.g. BY DESTRUCTIVE HYDROGENATION, OLIGOMERISATION, POLYMERISATION; RECOVERY OF HYDROCARBON OILS FROM OIL-SHALE, OIL-SAND, OR GASES; REFINING MIXTURES MAINLY CONSISTING OF HYDROCARBONS; REFORMING OF NAPHTHA; MINERAL WAXES
    • C10G2300/00—Aspects relating to hydrocarbon processing covered by groups C10G1/00 - C10G99/00
    • C10G2300/10—Feedstock materials
    • C10G2300/1037—Hydrocarbon fractions
    • C10G2300/104—Light gasoline having a boiling range of about 20 - 100 °C
    • C—CHEMISTRY; METALLURGY
    • C10—PETROLEUM, GAS OR COKE INDUSTRIES; TECHNICAL GASES CONTAINING CARBON MONOXIDE; FUELS; LUBRICANTS; PEAT
    • C10G—CRACKING HYDROCARBON OILS; PRODUCTION OF LIQUID HYDROCARBON MIXTURES, e.g. BY DESTRUCTIVE HYDROGENATION, OLIGOMERISATION, POLYMERISATION; RECOVERY OF HYDROCARBON OILS FROM OIL-SHALE, OIL-SAND, OR GASES; REFINING MIXTURES MAINLY CONSISTING OF HYDROCARBONS; REFORMING OF NAPHTHA; MINERAL WAXES
    • C10G2300/00—Aspects relating to hydrocarbon processing covered by groups C10G1/00 - C10G99/00
    • C10G2300/10—Feedstock materials
    • C10G2300/1037—Hydrocarbon fractions
    • C10G2300/1044—Heavy gasoline or naphtha having a boiling range of about 100 - 180 °C
    • C—CHEMISTRY; METALLURGY
    • C10—PETROLEUM, GAS OR COKE INDUSTRIES; TECHNICAL GASES CONTAINING CARBON MONOXIDE; FUELS; LUBRICANTS; PEAT
    • C10G—CRACKING HYDROCARBON OILS; PRODUCTION OF LIQUID HYDROCARBON MIXTURES, e.g. BY DESTRUCTIVE HYDROGENATION, OLIGOMERISATION, POLYMERISATION; RECOVERY OF HYDROCARBON OILS FROM OIL-SHALE, OIL-SAND, OR GASES; REFINING MIXTURES MAINLY CONSISTING OF HYDROCARBONS; REFORMING OF NAPHTHA; MINERAL WAXES
    • C10G2300/00—Aspects relating to hydrocarbon processing covered by groups C10G1/00 - C10G99/00
    • C10G2300/20—Characteristics of the feedstock or the products
    • C10G2300/201—Impurities
    • C10G2300/202—Heteroatoms content, i.e. S, N, O, P
    • C—CHEMISTRY; METALLURGY
    • C10—PETROLEUM, GAS OR COKE INDUSTRIES; TECHNICAL GASES CONTAINING CARBON MONOXIDE; FUELS; LUBRICANTS; PEAT
    • C10G—CRACKING HYDROCARBON OILS; PRODUCTION OF LIQUID HYDROCARBON MIXTURES, e.g. BY DESTRUCTIVE HYDROGENATION, OLIGOMERISATION, POLYMERISATION; RECOVERY OF HYDROCARBON OILS FROM OIL-SHALE, OIL-SAND, OR GASES; REFINING MIXTURES MAINLY CONSISTING OF HYDROCARBONS; REFORMING OF NAPHTHA; MINERAL WAXES
    • C10G2400/00—Products obtained by processes covered by groups C10G9/00 - C10G69/14
    • C10G2400/02—Gasoline
    • C—CHEMISTRY; METALLURGY
    • C10—PETROLEUM, GAS OR COKE INDUSTRIES; TECHNICAL GASES CONTAINING CARBON MONOXIDE; FUELS; LUBRICANTS; PEAT
    • C10G—CRACKING HYDROCARBON OILS; PRODUCTION OF LIQUID HYDROCARBON MIXTURES, e.g. BY DESTRUCTIVE HYDROGENATION, OLIGOMERISATION, POLYMERISATION; RECOVERY OF HYDROCARBON OILS FROM OIL-SHALE, OIL-SAND, OR GASES; REFINING MIXTURES MAINLY CONSISTING OF HYDROCARBONS; REFORMING OF NAPHTHA; MINERAL WAXES
    • C10G2400/00—Products obtained by processes covered by groups C10G9/00 - C10G69/14
    • C10G2400/20—C2-C4 olefins

Landscapes

  • Chemical & Material Sciences (AREA)
  • Chemical Kinetics & Catalysis (AREA)
  • Engineering & Computer Science (AREA)
  • Organic Chemistry (AREA)
  • Oil, Petroleum & Natural Gas (AREA)
  • Materials Engineering (AREA)
  • General Chemical & Material Sciences (AREA)
  • Crystallography & Structural Chemistry (AREA)
  • Thermal Sciences (AREA)
  • Physics & Mathematics (AREA)
  • Production Of Liquid Hydrocarbon Mixture For Refining Petroleum (AREA)
  • Solid-Sorbent Or Filter-Aiding Compositions (AREA)
  • Catalysts (AREA)
  • Treatment Of Liquids With Adsorbents In General (AREA)

Abstract

Procédé de captation de mercaptans contenus dans une charge hydrocarbonée contenant du soufre en présence d’une masse de captation comprenant une phase active à base d’au moins un métal du groupe VIII, IB ou IIB, et un support mésoporeux comprenant une distribution bimodale de mésopores, ladite masse de captation comprenant une surface spécifique comprise entre 120 m²/g et 350 m²/g, et :- le volume des mésopores de diamètre supérieur ou égal à 2 nm et inférieur à 20 nm correspond entre 35% et 70% en volume du volume poreux total de ladite masse de captation ;- le volume des mésopores de diamètre supérieur ou égal à 20 nm et inférieur à 50 nm correspond entre 25% et 60% en volume du volume poreux total de ladite masse de captation.
FR2113808A 2021-12-17 2021-12-17 Procédé de captation de mercaptans mettant en œuvre une masse de captation mésoporeuse Active FR3130830B1 (fr)

Priority Applications (10)

Application Number Priority Date Filing Date Title
FR2113808A FR3130830B1 (fr) 2021-12-17 2021-12-17 Procédé de captation de mercaptans mettant en œuvre une masse de captation mésoporeuse
CN202280083717.XA CN118434830A (zh) 2021-12-17 2022-12-12 使用中孔捕获物质捕获硫醇的方法
EP22835371.0A EP4448689A1 (fr) 2021-12-17 2022-12-12 Procédé de captation de mercaptans mettant en ouvre une masse de captation mésoporeuse
JP2024535622A JP2025502658A (ja) 2021-12-17 2022-12-12 メソ細孔捕捉塊体を用いたメルカプタンの捕捉方法
MX2024006866A MX2024006866A (es) 2021-12-17 2022-12-12 Proceso de captura de mercaptanos usando una masa de captura mesoporosa.
AU2022413308A AU2022413308A1 (en) 2021-12-17 2022-12-12 Method for capturing mercaptans using a mesoporous capture mass
PCT/EP2022/085350 WO2023110728A1 (fr) 2021-12-17 2022-12-12 Procédé de captation de mercaptans mettant en œuvre une masse de captation mésoporeuse
US18/718,860 US20250043198A1 (en) 2021-12-17 2022-12-12 Method for capturing mercaptans using a mesoporous capture mass
KR1020247019659A KR20240121752A (ko) 2021-12-17 2022-12-12 메조포어형 포획 매스를 사용하여 메르캅탄을 포획하기 위한 방법
ARP220103450A AR127980A1 (es) 2021-12-17 2022-12-15 Procedimiento de captación de mercaptanos que se aplica una masa de captación mesoporosa

Applications Claiming Priority (2)

Application Number Priority Date Filing Date Title
FR2113808 2021-12-17
FR2113808A FR3130830B1 (fr) 2021-12-17 2021-12-17 Procédé de captation de mercaptans mettant en œuvre une masse de captation mésoporeuse

Publications (2)

Publication Number Publication Date
FR3130830A1 FR3130830A1 (fr) 2023-06-23
FR3130830B1 true FR3130830B1 (fr) 2024-08-16

Family

ID=80786339

Family Applications (1)

Application Number Title Priority Date Filing Date
FR2113808A Active FR3130830B1 (fr) 2021-12-17 2021-12-17 Procédé de captation de mercaptans mettant en œuvre une masse de captation mésoporeuse

Country Status (10)

Country Link
US (1) US20250043198A1 (fr)
EP (1) EP4448689A1 (fr)
JP (1) JP2025502658A (fr)
KR (1) KR20240121752A (fr)
CN (1) CN118434830A (fr)
AR (1) AR127980A1 (fr)
AU (1) AU2022413308A1 (fr)
FR (1) FR3130830B1 (fr)
MX (1) MX2024006866A (fr)
WO (1) WO2023110728A1 (fr)

Family Cites Families (9)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
US5866749A (en) 1993-05-28 1999-02-02 Exxon Chemical Patents Inc. Sulfur and thiol removal from reactive hydrocarbons
FR2797639B1 (fr) 1999-08-19 2001-09-21 Inst Francais Du Petrole Procede de production d'essences a faible teneur en soufre
AU2001253223A1 (en) 2000-04-18 2001-10-30 Exxonmobil Research And Engineering Company Selective hydroprocessing and mercaptan removal
FR2811328B1 (fr) 2000-07-06 2002-08-23 Inst Francais Du Petrole Procede comprenant deux etapes d'hydrodesulfuration d'essence et une elimination intermediaire de l'h2s forme au cours de la premiere etape
US6579444B2 (en) 2000-12-28 2003-06-17 Exxonmobil Research And Engineering Company Removal of sulfur compounds from hydrocarbon feedstreams using cobalt containing adsorbents in the substantial absence of hydrogen
US7074324B2 (en) 2002-06-05 2006-07-11 Exxonmobil Research And Engineering Company Process to remove sulfur contaminants from hydrocarbon streams
FR2908781B1 (fr) 2006-11-16 2012-10-19 Inst Francais Du Petrole Procede de desulfuration profonde des essences de craquage avec une faible perte en indice d'octane
CN109266387B (zh) * 2018-10-14 2020-12-11 林雅娟 Fcc汽油选择性加氢处理方法
FR3104459B1 (fr) * 2019-12-17 2022-07-01 Ifp Energies Now Masse de captation de mercaptans préparée par voie sels fondus

Also Published As

Publication number Publication date
EP4448689A1 (fr) 2024-10-23
JP2025502658A (ja) 2025-01-28
FR3130830A1 (fr) 2023-06-23
US20250043198A1 (en) 2025-02-06
AU2022413308A1 (en) 2024-05-23
AR127980A1 (es) 2024-03-13
WO2023110728A1 (fr) 2023-06-22
KR20240121752A (ko) 2024-08-09
MX2024006866A (es) 2024-06-19
CN118434830A (zh) 2024-08-02

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