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FR3130828B1 - Procédé de captation de mercaptans mettant en œuvre une masse de captation macro et mésoporeuse - Google Patents

Procédé de captation de mercaptans mettant en œuvre une masse de captation macro et mésoporeuse Download PDF

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Publication number
FR3130828B1
FR3130828B1 FR2113811A FR2113811A FR3130828B1 FR 3130828 B1 FR3130828 B1 FR 3130828B1 FR 2113811 A FR2113811 A FR 2113811A FR 2113811 A FR2113811 A FR 2113811A FR 3130828 B1 FR3130828 B1 FR 3130828B1
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FR
France
Prior art keywords
capture mass
volume
mesoporous
capturing
mercaptans
Prior art date
Legal status (The legal status is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the status listed.)
Active
Application number
FR2113811A
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English (en)
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FR3130828A1 (fr
Inventor
Antoine Fecant
Antoine Hugon
Current Assignee (The listed assignees may be inaccurate. Google has not performed a legal analysis and makes no representation or warranty as to the accuracy of the list.)
IFP Energies Nouvelles IFPEN
Original Assignee
IFP Energies Nouvelles IFPEN
Priority date (The priority date is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the date listed.)
Filing date
Publication date
Priority to FR2113811A priority Critical patent/FR3130828B1/fr
Application filed by IFP Energies Nouvelles IFPEN filed Critical IFP Energies Nouvelles IFPEN
Priority to EP22835661.4A priority patent/EP4448690A1/fr
Priority to JP2024535625A priority patent/JP2025500212A/ja
Priority to AU2022410203A priority patent/AU2022410203A1/en
Priority to US18/720,507 priority patent/US20250041822A1/en
Priority to PCT/EP2022/085352 priority patent/WO2023110730A1/fr
Priority to KR1020247019660A priority patent/KR20240121753A/ko
Priority to CN202280083711.2A priority patent/CN118414410A/zh
Priority to MX2024006995A priority patent/MX2024006995A/es
Priority to ARP220103451A priority patent/AR127981A1/es
Publication of FR3130828A1 publication Critical patent/FR3130828A1/fr
Application granted granted Critical
Publication of FR3130828B1 publication Critical patent/FR3130828B1/fr
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    • B—PERFORMING OPERATIONS; TRANSPORTING
    • B01—PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
    • B01J—CHEMICAL OR PHYSICAL PROCESSES, e.g. CATALYSIS OR COLLOID CHEMISTRY; THEIR RELEVANT APPARATUS
    • B01J20/00—Solid sorbent compositions or filter aid compositions; Sorbents for chromatography; Processes for preparing, regenerating or reactivating thereof
    • B01J20/02—Solid sorbent compositions or filter aid compositions; Sorbents for chromatography; Processes for preparing, regenerating or reactivating thereof comprising inorganic material
    • B01J20/0203—Solid sorbent compositions or filter aid compositions; Sorbents for chromatography; Processes for preparing, regenerating or reactivating thereof comprising inorganic material comprising compounds of metals not provided for in B01J20/04
    • B01J20/0225—Compounds of Fe, Ru, Os, Co, Rh, Ir, Ni, Pd, Pt
    • B—PERFORMING OPERATIONS; TRANSPORTING
    • B01—PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
    • B01J—CHEMICAL OR PHYSICAL PROCESSES, e.g. CATALYSIS OR COLLOID CHEMISTRY; THEIR RELEVANT APPARATUS
    • B01J20/00—Solid sorbent compositions or filter aid compositions; Sorbents for chromatography; Processes for preparing, regenerating or reactivating thereof
    • B01J20/28—Solid sorbent compositions or filter aid compositions; Sorbents for chromatography; Processes for preparing, regenerating or reactivating thereof characterised by their form or physical properties
    • B01J20/28054—Solid sorbent compositions or filter aid compositions; Sorbents for chromatography; Processes for preparing, regenerating or reactivating thereof characterised by their form or physical properties characterised by their surface properties or porosity
    • B01J20/28057—Surface area, e.g. B.E.T specific surface area
    • B01J20/28061—Surface area, e.g. B.E.T specific surface area being in the range 100-500 m2/g
    • B—PERFORMING OPERATIONS; TRANSPORTING
    • B01—PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
    • B01J—CHEMICAL OR PHYSICAL PROCESSES, e.g. CATALYSIS OR COLLOID CHEMISTRY; THEIR RELEVANT APPARATUS
    • B01J20/00—Solid sorbent compositions or filter aid compositions; Sorbents for chromatography; Processes for preparing, regenerating or reactivating thereof
    • B01J20/28—Solid sorbent compositions or filter aid compositions; Sorbents for chromatography; Processes for preparing, regenerating or reactivating thereof characterised by their form or physical properties
    • B01J20/28054—Solid sorbent compositions or filter aid compositions; Sorbents for chromatography; Processes for preparing, regenerating or reactivating thereof characterised by their form or physical properties characterised by their surface properties or porosity
    • B01J20/28069—Pore volume, e.g. total pore volume, mesopore volume, micropore volume
    • B01J20/28071—Pore volume, e.g. total pore volume, mesopore volume, micropore volume being less than 0.5 ml/g
    • B—PERFORMING OPERATIONS; TRANSPORTING
    • B01—PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
    • B01J—CHEMICAL OR PHYSICAL PROCESSES, e.g. CATALYSIS OR COLLOID CHEMISTRY; THEIR RELEVANT APPARATUS
    • B01J20/00—Solid sorbent compositions or filter aid compositions; Sorbents for chromatography; Processes for preparing, regenerating or reactivating thereof
    • B01J20/28—Solid sorbent compositions or filter aid compositions; Sorbents for chromatography; Processes for preparing, regenerating or reactivating thereof characterised by their form or physical properties
    • B01J20/28054—Solid sorbent compositions or filter aid compositions; Sorbents for chromatography; Processes for preparing, regenerating or reactivating thereof characterised by their form or physical properties characterised by their surface properties or porosity
    • B01J20/28069—Pore volume, e.g. total pore volume, mesopore volume, micropore volume
    • B01J20/28073—Pore volume, e.g. total pore volume, mesopore volume, micropore volume being in the range 0.5-1.0 ml/g
    • B—PERFORMING OPERATIONS; TRANSPORTING
    • B01—PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
    • B01J—CHEMICAL OR PHYSICAL PROCESSES, e.g. CATALYSIS OR COLLOID CHEMISTRY; THEIR RELEVANT APPARATUS
    • B01J20/00—Solid sorbent compositions or filter aid compositions; Sorbents for chromatography; Processes for preparing, regenerating or reactivating thereof
    • B01J20/30—Processes for preparing, regenerating, or reactivating
    • B01J20/3078—Thermal treatment, e.g. calcining or pyrolizing
    • B—PERFORMING OPERATIONS; TRANSPORTING
    • B01—PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
    • B01J—CHEMICAL OR PHYSICAL PROCESSES, e.g. CATALYSIS OR COLLOID CHEMISTRY; THEIR RELEVANT APPARATUS
    • B01J20/00—Solid sorbent compositions or filter aid compositions; Sorbents for chromatography; Processes for preparing, regenerating or reactivating thereof
    • B01J20/30—Processes for preparing, regenerating, or reactivating
    • B01J20/32—Impregnating or coating ; Solid sorbent compositions obtained from processes involving impregnating or coating
    • B01J20/3202—Impregnating or coating ; Solid sorbent compositions obtained from processes involving impregnating or coating characterised by the carrier, support or substrate used for impregnation or coating
    • B01J20/3204—Inorganic carriers, supports or substrates
    • B—PERFORMING OPERATIONS; TRANSPORTING
    • B01—PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
    • B01J—CHEMICAL OR PHYSICAL PROCESSES, e.g. CATALYSIS OR COLLOID CHEMISTRY; THEIR RELEVANT APPARATUS
    • B01J20/00—Solid sorbent compositions or filter aid compositions; Sorbents for chromatography; Processes for preparing, regenerating or reactivating thereof
    • B01J20/30—Processes for preparing, regenerating, or reactivating
    • B01J20/32—Impregnating or coating ; Solid sorbent compositions obtained from processes involving impregnating or coating
    • B01J20/3231—Impregnating or coating ; Solid sorbent compositions obtained from processes involving impregnating or coating characterised by the coating or impregnating layer
    • B01J20/3234—Inorganic material layers
    • B01J20/3236—Inorganic material layers containing metal, other than zeolites, e.g. oxides, hydroxides, sulphides or salts
    • B—PERFORMING OPERATIONS; TRANSPORTING
    • B01—PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
    • B01J—CHEMICAL OR PHYSICAL PROCESSES, e.g. CATALYSIS OR COLLOID CHEMISTRY; THEIR RELEVANT APPARATUS
    • B01J23/00—Catalysts comprising metals or metal oxides or hydroxides, not provided for in group B01J21/00
    • B01J23/70—Catalysts comprising metals or metal oxides or hydroxides, not provided for in group B01J21/00 of the iron group metals or copper
    • B01J23/74—Iron group metals
    • B01J23/755—Nickel
    • B—PERFORMING OPERATIONS; TRANSPORTING
    • B01—PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
    • B01J—CHEMICAL OR PHYSICAL PROCESSES, e.g. CATALYSIS OR COLLOID CHEMISTRY; THEIR RELEVANT APPARATUS
    • B01J35/00—Catalysts, in general, characterised by their form or physical properties
    • B01J35/60—Catalysts, in general, characterised by their form or physical properties characterised by their surface properties or porosity
    • B01J35/61—Surface area
    • B01J35/615—100-500 m2/g
    • B—PERFORMING OPERATIONS; TRANSPORTING
    • B01—PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
    • B01J—CHEMICAL OR PHYSICAL PROCESSES, e.g. CATALYSIS OR COLLOID CHEMISTRY; THEIR RELEVANT APPARATUS
    • B01J35/00—Catalysts, in general, characterised by their form or physical properties
    • B01J35/60—Catalysts, in general, characterised by their form or physical properties characterised by their surface properties or porosity
    • B01J35/63—Pore volume
    • B01J35/633—Pore volume less than 0.5 ml/g
    • C—CHEMISTRY; METALLURGY
    • C10—PETROLEUM, GAS OR COKE INDUSTRIES; TECHNICAL GASES CONTAINING CARBON MONOXIDE; FUELS; LUBRICANTS; PEAT
    • C10G—CRACKING HYDROCARBON OILS; PRODUCTION OF LIQUID HYDROCARBON MIXTURES, e.g. BY DESTRUCTIVE HYDROGENATION, OLIGOMERISATION, POLYMERISATION; RECOVERY OF HYDROCARBON OILS FROM OIL-SHALE, OIL-SAND, OR GASES; REFINING MIXTURES MAINLY CONSISTING OF HYDROCARBONS; REFORMING OF NAPHTHA; MINERAL WAXES
    • C10G25/00—Refining of hydrocarbon oils in the absence of hydrogen, with solid sorbents
    • C10G25/003—Specific sorbent material, not covered by C10G25/02 or C10G25/03
    • C—CHEMISTRY; METALLURGY
    • C10—PETROLEUM, GAS OR COKE INDUSTRIES; TECHNICAL GASES CONTAINING CARBON MONOXIDE; FUELS; LUBRICANTS; PEAT
    • C10G—CRACKING HYDROCARBON OILS; PRODUCTION OF LIQUID HYDROCARBON MIXTURES, e.g. BY DESTRUCTIVE HYDROGENATION, OLIGOMERISATION, POLYMERISATION; RECOVERY OF HYDROCARBON OILS FROM OIL-SHALE, OIL-SAND, OR GASES; REFINING MIXTURES MAINLY CONSISTING OF HYDROCARBONS; REFORMING OF NAPHTHA; MINERAL WAXES
    • C10G25/00—Refining of hydrocarbon oils in the absence of hydrogen, with solid sorbents
    • C10G25/02—Refining of hydrocarbon oils in the absence of hydrogen, with solid sorbents with ion-exchange material
    • C10G25/03—Refining of hydrocarbon oils in the absence of hydrogen, with solid sorbents with ion-exchange material with crystalline alumino-silicates, e.g. molecular sieves
    • C10G25/05—Removal of non-hydrocarbon compounds, e.g. sulfur compounds
    • C—CHEMISTRY; METALLURGY
    • C10—PETROLEUM, GAS OR COKE INDUSTRIES; TECHNICAL GASES CONTAINING CARBON MONOXIDE; FUELS; LUBRICANTS; PEAT
    • C10G—CRACKING HYDROCARBON OILS; PRODUCTION OF LIQUID HYDROCARBON MIXTURES, e.g. BY DESTRUCTIVE HYDROGENATION, OLIGOMERISATION, POLYMERISATION; RECOVERY OF HYDROCARBON OILS FROM OIL-SHALE, OIL-SAND, OR GASES; REFINING MIXTURES MAINLY CONSISTING OF HYDROCARBONS; REFORMING OF NAPHTHA; MINERAL WAXES
    • C10G2300/00—Aspects relating to hydrocarbon processing covered by groups C10G1/00 - C10G99/00
    • C10G2300/20—Characteristics of the feedstock or the products
    • C10G2300/201—Impurities
    • C10G2300/202—Heteroatoms content, i.e. S, N, O, P
    • C—CHEMISTRY; METALLURGY
    • C10—PETROLEUM, GAS OR COKE INDUSTRIES; TECHNICAL GASES CONTAINING CARBON MONOXIDE; FUELS; LUBRICANTS; PEAT
    • C10G—CRACKING HYDROCARBON OILS; PRODUCTION OF LIQUID HYDROCARBON MIXTURES, e.g. BY DESTRUCTIVE HYDROGENATION, OLIGOMERISATION, POLYMERISATION; RECOVERY OF HYDROCARBON OILS FROM OIL-SHALE, OIL-SAND, OR GASES; REFINING MIXTURES MAINLY CONSISTING OF HYDROCARBONS; REFORMING OF NAPHTHA; MINERAL WAXES
    • C10G2400/00—Products obtained by processes covered by groups C10G9/00 - C10G69/14
    • C10G2400/02—Gasoline

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  • Chemical & Material Sciences (AREA)
  • Organic Chemistry (AREA)
  • Chemical Kinetics & Catalysis (AREA)
  • Engineering & Computer Science (AREA)
  • Oil, Petroleum & Natural Gas (AREA)
  • Analytical Chemistry (AREA)
  • Materials Engineering (AREA)
  • General Chemical & Material Sciences (AREA)
  • Inorganic Chemistry (AREA)
  • Crystallography & Structural Chemistry (AREA)
  • Physics & Mathematics (AREA)
  • Thermal Sciences (AREA)
  • Production Of Liquid Hydrocarbon Mixture For Refining Petroleum (AREA)
  • Solid-Sorbent Or Filter-Aiding Compositions (AREA)
  • Treatment Of Liquids With Adsorbents In General (AREA)

Abstract

Procédé de captation de mercaptans contenus dans une charge hydrocarbonée contenant du soufre, en présence d’une masse de captation comprenant une phase active à base d’au moins un métal du groupe VIII, IB ou IIB, et un support mésoporeux et macroporeux, ladite masse de captation comprenant une surface spécifique comprise entre 120 m2/g et 350 m2/g, et :- le volume des mésopores de diamètre supérieur ou égal à 2 nm et inférieur à 50 nm correspond entre 40% et 70% en volume du volume poreux total de ladite masse de captation ;- le volume des macropores de diamètre supérieur ou égal à 50 nm correspond entre 30% et 60% en volume du volume poreux total de ladite masse de captation.
FR2113811A 2021-12-17 2021-12-17 Procédé de captation de mercaptans mettant en œuvre une masse de captation macro et mésoporeuse Active FR3130828B1 (fr)

Priority Applications (10)

Application Number Priority Date Filing Date Title
FR2113811A FR3130828B1 (fr) 2021-12-17 2021-12-17 Procédé de captation de mercaptans mettant en œuvre une masse de captation macro et mésoporeuse
MX2024006995A MX2024006995A (es) 2021-12-17 2022-12-12 Proceso de captura de mercaptanos usando una masa de captura macro y mesoporosa.
AU2022410203A AU2022410203A1 (en) 2021-12-17 2022-12-12 Method for capturing mercaptans using a macro and mesoporous capture mass
US18/720,507 US20250041822A1 (en) 2021-12-17 2022-12-12 Method for capturing mercaptans using a macro and mesoporous capture mass
PCT/EP2022/085352 WO2023110730A1 (fr) 2021-12-17 2022-12-12 Procede de captation de mercaptans mettant en œuvre une masse de captation macro et mesoporeuse
KR1020247019660A KR20240121753A (ko) 2021-12-17 2022-12-12 매크로포어형 및 메조포어형 포획 매스를 사용하여 메르캅탄들을 포획하기 위한 프로세스
EP22835661.4A EP4448690A1 (fr) 2021-12-17 2022-12-12 Procede de captation de mercaptans mettant en ouvre une masse de captation macro et mesoporeuse
JP2024535625A JP2025500212A (ja) 2021-12-17 2022-12-12 マクロ細孔捕捉塊体およびメソ細孔捕捉塊体を用いたメルカプタンの捕捉方法
CN202280083711.2A CN118414410A (zh) 2021-12-17 2022-12-12 使用大孔和中孔捕获物质捕获硫醇的方法
ARP220103451A AR127981A1 (es) 2021-12-17 2022-12-15 Procedimiento de captación de mercaptanos que se aplica una masa de captación macro y mesoporosa

Applications Claiming Priority (2)

Application Number Priority Date Filing Date Title
FR2113811A FR3130828B1 (fr) 2021-12-17 2021-12-17 Procédé de captation de mercaptans mettant en œuvre une masse de captation macro et mésoporeuse
FR2113811 2021-12-17

Publications (2)

Publication Number Publication Date
FR3130828A1 FR3130828A1 (fr) 2023-06-23
FR3130828B1 true FR3130828B1 (fr) 2024-08-16

Family

ID=80786235

Family Applications (1)

Application Number Title Priority Date Filing Date
FR2113811A Active FR3130828B1 (fr) 2021-12-17 2021-12-17 Procédé de captation de mercaptans mettant en œuvre une masse de captation macro et mésoporeuse

Country Status (10)

Country Link
US (1) US20250041822A1 (fr)
EP (1) EP4448690A1 (fr)
JP (1) JP2025500212A (fr)
KR (1) KR20240121753A (fr)
CN (1) CN118414410A (fr)
AR (1) AR127981A1 (fr)
AU (1) AU2022410203A1 (fr)
FR (1) FR3130828B1 (fr)
MX (1) MX2024006995A (fr)
WO (1) WO2023110730A1 (fr)

Family Cites Families (10)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
US5866749A (en) 1993-05-28 1999-02-02 Exxon Chemical Patents Inc. Sulfur and thiol removal from reactive hydrocarbons
FR2797639B1 (fr) 1999-08-19 2001-09-21 Inst Francais Du Petrole Procede de production d'essences a faible teneur en soufre
AU2001253223A1 (en) 2000-04-18 2001-10-30 Exxonmobil Research And Engineering Company Selective hydroprocessing and mercaptan removal
FR2811328B1 (fr) 2000-07-06 2002-08-23 Inst Francais Du Petrole Procede comprenant deux etapes d'hydrodesulfuration d'essence et une elimination intermediaire de l'h2s forme au cours de la premiere etape
US6579444B2 (en) 2000-12-28 2003-06-17 Exxonmobil Research And Engineering Company Removal of sulfur compounds from hydrocarbon feedstreams using cobalt containing adsorbents in the substantial absence of hydrogen
US7074324B2 (en) 2002-06-05 2006-07-11 Exxonmobil Research And Engineering Company Process to remove sulfur contaminants from hydrocarbon streams
FR2908781B1 (fr) 2006-11-16 2012-10-19 Inst Francais Du Petrole Procede de desulfuration profonde des essences de craquage avec une faible perte en indice d'octane
CN109420506B (zh) * 2017-08-31 2021-07-30 中国石油天然气股份有限公司 一种汽油脱硫醇的催化剂及制备方法
CN109266387B (zh) * 2018-10-14 2020-12-11 林雅娟 Fcc汽油选择性加氢处理方法
FR3104459B1 (fr) * 2019-12-17 2022-07-01 Ifp Energies Now Masse de captation de mercaptans préparée par voie sels fondus

Also Published As

Publication number Publication date
KR20240121753A (ko) 2024-08-09
FR3130828A1 (fr) 2023-06-23
EP4448690A1 (fr) 2024-10-23
CN118414410A (zh) 2024-07-30
AU2022410203A1 (en) 2024-05-23
WO2023110730A1 (fr) 2023-06-22
MX2024006995A (es) 2024-06-19
AR127981A1 (es) 2024-03-13
JP2025500212A (ja) 2025-01-09
US20250041822A1 (en) 2025-02-06

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