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ES320732A1 - Procedure for the manufacture of N-dietile amino acetyl 2,4,6 trimethyl anilide. (Machine-translation by Google Translate, not legally binding) - Google Patents

Procedure for the manufacture of N-dietile amino acetyl 2,4,6 trimethyl anilide. (Machine-translation by Google Translate, not legally binding)

Info

Publication number
ES320732A1
ES320732A1 ES0320732A ES320732A ES320732A1 ES 320732 A1 ES320732 A1 ES 320732A1 ES 0320732 A ES0320732 A ES 0320732A ES 320732 A ES320732 A ES 320732A ES 320732 A1 ES320732 A1 ES 320732A1
Authority
ES
Spain
Prior art keywords
dietile
anilide
trimethyl
translation
machine
Prior art date
Legal status (The legal status is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the status listed.)
Expired
Application number
ES0320732A
Other languages
Spanish (es)
Current Assignee (The listed assignees may be inaccurate. Google has not performed a legal analysis and makes no representation or warranty as to the accuracy of the list.)
JUSTE SOC ANENIMA
Original Assignee
JUSTE SOC ANENIMA
Priority date (The priority date is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the date listed.)
Filing date
Publication date
Application filed by JUSTE SOC ANENIMA filed Critical JUSTE SOC ANENIMA
Priority to ES0320732A priority Critical patent/ES320732A1/en
Publication of ES320732A1 publication Critical patent/ES320732A1/en
Priority to BR184979/66A priority patent/BR6684979D0/en
Priority to FR86732A priority patent/FR1504210A/en
Expired legal-status Critical Current

Links

Classifications

    • C—CHEMISTRY; METALLURGY
    • C07—ORGANIC CHEMISTRY
    • C07C—ACYCLIC OR CARBOCYCLIC COMPOUNDS
    • C07C201/00—Preparation of esters of nitric or nitrous acid or of compounds containing nitro or nitroso groups bound to a carbon skeleton
    • C07C201/06—Preparation of nitro compounds
    • C07C201/08—Preparation of nitro compounds by substitution of hydrogen atoms by nitro groups
    • C—CHEMISTRY; METALLURGY
    • C07—ORGANIC CHEMISTRY
    • C07C—ACYCLIC OR CARBOCYCLIC COMPOUNDS
    • C07C209/00—Preparation of compounds containing amino groups bound to a carbon skeleton
    • C07C209/30—Preparation of compounds containing amino groups bound to a carbon skeleton by reduction of nitrogen-to-oxygen or nitrogen-to-nitrogen bonds
    • C07C209/32—Preparation of compounds containing amino groups bound to a carbon skeleton by reduction of nitrogen-to-oxygen or nitrogen-to-nitrogen bonds by reduction of nitro groups
    • C07C209/36—Preparation of compounds containing amino groups bound to a carbon skeleton by reduction of nitrogen-to-oxygen or nitrogen-to-nitrogen bonds by reduction of nitro groups by reduction of nitro groups bound to carbon atoms of six-membered aromatic rings in presence of hydrogen-containing gases and a catalyst
    • C—CHEMISTRY; METALLURGY
    • C07—ORGANIC CHEMISTRY
    • C07C—ACYCLIC OR CARBOCYCLIC COMPOUNDS
    • C07C231/00—Preparation of carboxylic acid amides
    • C07C231/02—Preparation of carboxylic acid amides from carboxylic acids or from esters, anhydrides, or halides thereof by reaction with ammonia or amines
    • C—CHEMISTRY; METALLURGY
    • C07—ORGANIC CHEMISTRY
    • C07C—ACYCLIC OR CARBOCYCLIC COMPOUNDS
    • C07C231/00—Preparation of carboxylic acid amides
    • C07C231/12—Preparation of carboxylic acid amides by reactions not involving the formation of carboxamide groups

Landscapes

  • Chemical & Material Sciences (AREA)
  • Organic Chemistry (AREA)
  • Chemical Kinetics & Catalysis (AREA)
  • Extraction Or Liquid Replacement (AREA)
  • Organic Low-Molecular-Weight Compounds And Preparation Thereof (AREA)

Abstract

"MANUFACTURING PROCEDURE OF N-DIETILE AMINO ACETYL 2,4,6-TRIMETHYL ANILIDE" characterized in that the glacial acetic acid in a flask equipped with a stirrer and thermometer is introduced into a cold bath, gradually adding fuming nitric acid mixing at 10º C to add mesitylene, keeping the temperature at less than 20º C; then adding acetic anhydride maintaining the temperature between 25-30º C and allowing the mixture to cool for two hours at room temperature and then heating at 50º C for ten minutes, then letting it cool; pouring the product on a mixture of ice and salt for the precipitate of the obtained nitrated derivative, filtering it, washing it extracting it with petroleum ether; washing the ethereal extracts with aqueous alkaline solution, drying with calcium chloride, distilling the solvent and recrystallizing the residue in methyl alcohol. (Machine-translation by Google Translate, not legally binding)
ES0320732A 1965-12-14 1965-12-14 Procedure for the manufacture of N-dietile amino acetyl 2,4,6 trimethyl anilide. (Machine-translation by Google Translate, not legally binding) Expired ES320732A1 (en)

Priority Applications (3)

Application Number Priority Date Filing Date Title
ES0320732A ES320732A1 (en) 1965-12-14 1965-12-14 Procedure for the manufacture of N-dietile amino acetyl 2,4,6 trimethyl anilide. (Machine-translation by Google Translate, not legally binding)
BR184979/66A BR6684979D0 (en) 1965-12-14 1966-11-30 PROCESS OF OBTAINING NEW ANESTHETICS
FR86732A FR1504210A (en) 1965-12-14 1966-12-08 Process for preparing n-diethylaminoacetyl 2,4,6-trimethylaniline

Applications Claiming Priority (1)

Application Number Priority Date Filing Date Title
ES0320732A ES320732A1 (en) 1965-12-14 1965-12-14 Procedure for the manufacture of N-dietile amino acetyl 2,4,6 trimethyl anilide. (Machine-translation by Google Translate, not legally binding)

Publications (1)

Publication Number Publication Date
ES320732A1 true ES320732A1 (en) 1966-06-16

Family

ID=8442716

Family Applications (1)

Application Number Title Priority Date Filing Date
ES0320732A Expired ES320732A1 (en) 1965-12-14 1965-12-14 Procedure for the manufacture of N-dietile amino acetyl 2,4,6 trimethyl anilide. (Machine-translation by Google Translate, not legally binding)

Country Status (3)

Country Link
BR (1) BR6684979D0 (en)
ES (1) ES320732A1 (en)
FR (1) FR1504210A (en)

Also Published As

Publication number Publication date
FR1504210A (en) 1967-12-01
BR6684979D0 (en) 1973-11-13

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