ES253183A1 - Magnesium glutamate hydrobromide and processes for the production thereof - Google Patents
Magnesium glutamate hydrobromide and processes for the production thereofInfo
- Publication number
- ES253183A1 ES253183A1 ES0253183A ES253183A ES253183A1 ES 253183 A1 ES253183 A1 ES 253183A1 ES 0253183 A ES0253183 A ES 0253183A ES 253183 A ES253183 A ES 253183A ES 253183 A1 ES253183 A1 ES 253183A1
- Authority
- ES
- Spain
- Prior art keywords
- magnesium
- hydrobromide
- glutamic acid
- crystallized
- processes
- Prior art date
- Legal status (The legal status is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the status listed.)
- Expired
Links
Landscapes
- Pharmaceuticals Containing Other Organic And Inorganic Compounds (AREA)
Abstract
The invention comprises magnesium glutamate hydrobromide and its monohydrate, and the preparation thereof by (a) neutralizing glutamic acid hydrobromide with magnesium oxide or hydroxide or a basic salt of magnesium (e.g. the carbonate) or (b) neutralizing magnesium glutamate with hydrobromic acid. Starting from glutamic acid itself, these processes may be effected as follows: (a) glutamic acid is reacted with a stiochiometric proportion of hydrobromic acid, the hydrobromide is crystallized at -10 DEG C. and dissolved in water, the pH of the solution is adjusted to as close as possible to 6 by addition of the basic magnesium compound, and magnesium glutamate hydrobromide monohydrate is crystallized slowly therefrom at a temperature below 0 DEG C. (b) a solution of glutamic acid is adjusted to pH 6.0-6.5 by addition of magnesium oxide or hydroxide or a basic salt of magnesium, filtered and a stoichiometric quantity of hydrobromic acid added slowly to the agitated filtrates and the desired product is thereafter crystallized as in (a).
Priority Applications (4)
Application Number | Priority Date | Filing Date | Title |
---|---|---|---|
ES0253183A ES253183A1 (en) | 1959-11-05 | 1959-11-05 | Magnesium glutamate hydrobromide and processes for the production thereof |
BR123941/60A BR6023941D0 (en) | 1959-11-05 | 1960-11-03 | PROCESS OF PREPARATION OF MAGNESIUM GLUTAMATE CHRONIDRATE AND THE RESULTING PRODUCT |
GB38057/60A GB955087A (en) | 1959-11-05 | 1960-11-04 | Magnesium glutamate hydrobromide and processes for the production thereof |
BE596742A BE596742A (en) | 1959-11-05 | 1960-11-04 | Magnesium glutamate bromohydrate and process for obtaining it. |
Applications Claiming Priority (1)
Application Number | Priority Date | Filing Date | Title |
---|---|---|---|
ES0253183A ES253183A1 (en) | 1959-11-05 | 1959-11-05 | Magnesium glutamate hydrobromide and processes for the production thereof |
Publications (1)
Publication Number | Publication Date |
---|---|
ES253183A1 true ES253183A1 (en) | 1960-06-01 |
Family
ID=8410837
Family Applications (1)
Application Number | Title | Priority Date | Filing Date |
---|---|---|---|
ES0253183A Expired ES253183A1 (en) | 1959-11-05 | 1959-11-05 | Magnesium glutamate hydrobromide and processes for the production thereof |
Country Status (4)
Country | Link |
---|---|
BE (1) | BE596742A (en) |
BR (1) | BR6023941D0 (en) |
ES (1) | ES253183A1 (en) |
GB (1) | GB955087A (en) |
Families Citing this family (1)
Publication number | Priority date | Publication date | Assignee | Title |
---|---|---|---|---|
FR2660653B1 (en) * | 1990-04-05 | 1994-05-20 | Mayoly Spindler Lab | EQUIMOLAR SALTS OF ALPHA-AMINO DICARBOXYLIC ACID AND DIVALENT METAL, PROCESS FOR THEIR PREPARATION AND THEIR APPLICATION FOR OBTAINING PHARMACEUTICAL COMPOSITIONS. |
-
1959
- 1959-11-05 ES ES0253183A patent/ES253183A1/en not_active Expired
-
1960
- 1960-11-03 BR BR123941/60A patent/BR6023941D0/en unknown
- 1960-11-04 GB GB38057/60A patent/GB955087A/en not_active Expired
- 1960-11-04 BE BE596742A patent/BE596742A/en unknown
Also Published As
Publication number | Publication date |
---|---|
BR6023941D0 (en) | 1973-05-24 |
GB955087A (en) | 1964-04-15 |
BE596742A (en) | 1961-03-01 |
Similar Documents
Publication | Publication Date | Title |
---|---|---|
SU648103A3 (en) | Method of obtaining tetrazol (1,5-a)-quinolines or salts thereof | |
Stephen et al. | 849. Syntheses in the quinazolone series. Part IV. The conversion of N-aroylorthanilamides into 2-arylquinazol-4-ones | |
ES253183A1 (en) | Magnesium glutamate hydrobromide and processes for the production thereof | |
GB1490289A (en) | Intermediates and production thereof for use in the preparation of 6-(2-phenyl-2-(guanylureidoacetamido)acetamido)penicillanic acid | |
SU115895A1 (en) | The method of obtaining adipic diamide and sigma-cyanovalsramid | |
ES434229A1 (en) | Process for the production of N,N-diallyldichloroacetamide | |
GB868005A (en) | Preparation of neutral potassium and magnesium double carbonate | |
SU650504A3 (en) | Method of obtaining methyl-(2-quinoxalinylmethylene)-carbazate-n',n4-dioxide | |
ES258756A1 (en) | Substituted phosphoramidopenicillanic acids | |
GB885575A (en) | Improvements in or relating to amino-guanidine preparation | |
JPS6438072A (en) | Production of 4-aminopyridines | |
GB1177259A (en) | Process for the Preparation of N-hydroxyimidothiocarboxylic Acid Esters | |
GB809410A (en) | Improved method for the preparation of n-methyleneglycino-nitrile | |
GB1354998A (en) | N,n-dimethyl-o-pyrazolylcarbamic acid esters process for their preparation and their use as insecticides | |
GB1505610A (en) | Process for preparing 3,4-dicyano-1,2,5-thiadiazole | |
GB1104323A (en) | 3-phenylpyrrole derivatives and process for preparing the same | |
GB900396A (en) | A process for the preparation of threo-ª--(p-nitrophenyl)-serine | |
JPS5231020A (en) | Process for preparation of lysine hydrate crystal | |
KR800001704B1 (en) | Process for preparing arginine salt of amoxycillin | |
GB874580A (en) | A process for the production of l-malic acid | |
GB936365A (en) | Chemotherapeutic methyl-sulphonyl-phenyl compounds | |
GB680653A (en) | Improvements in or relating to production of glutamic acid | |
ES266734A1 (en) | Process for the preparation of 2-chloroazacyclo 2.3-alkene-1-carbochlorides from Ï-lactams | |
GB750366A (en) | Improvements in or relating to the production of guanidine salts | |
GB940488A (en) | Penicillins |