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EP1944376A4 - PROCESS FOR PRODUCING AN AMIDE COMPOUND - Google Patents

PROCESS FOR PRODUCING AN AMIDE COMPOUND

Info

Publication number
EP1944376A4
EP1944376A4 EP06811414A EP06811414A EP1944376A4 EP 1944376 A4 EP1944376 A4 EP 1944376A4 EP 06811414 A EP06811414 A EP 06811414A EP 06811414 A EP06811414 A EP 06811414A EP 1944376 A4 EP1944376 A4 EP 1944376A4
Authority
EP
European Patent Office
Prior art keywords
producing
amide compound
amide
compound
Prior art date
Legal status (The legal status is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the status listed.)
Granted
Application number
EP06811414A
Other languages
German (de)
French (fr)
Other versions
EP1944376A1 (en
EP1944376B1 (en
Inventor
Hiroko Shibamoto
Toshikazu Aikawa
Teruo Arii
Masanori Muramoto
Takeshi Fukuda
Kiyoshi Ito
Takeya Abe
Souichi Hazama
Current Assignee (The listed assignees may be inaccurate. Google has not performed a legal analysis and makes no representation or warranty as to the accuracy of the list.)
Mitsui Chemicals Inc
Original Assignee
Mitsui Chemicals Inc
Priority date (The priority date is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the date listed.)
Filing date
Publication date
Application filed by Mitsui Chemicals Inc filed Critical Mitsui Chemicals Inc
Priority to EP16187709.7A priority Critical patent/EP3135767B1/en
Publication of EP1944376A1 publication Critical patent/EP1944376A1/en
Publication of EP1944376A4 publication Critical patent/EP1944376A4/en
Application granted granted Critical
Publication of EP1944376B1 publication Critical patent/EP1944376B1/en
Active legal-status Critical Current
Anticipated expiration legal-status Critical

Links

Classifications

    • CCHEMISTRY; METALLURGY
    • C12BIOCHEMISTRY; BEER; SPIRITS; WINE; VINEGAR; MICROBIOLOGY; ENZYMOLOGY; MUTATION OR GENETIC ENGINEERING
    • C12PFERMENTATION OR ENZYME-USING PROCESSES TO SYNTHESISE A DESIRED CHEMICAL COMPOUND OR COMPOSITION OR TO SEPARATE OPTICAL ISOMERS FROM A RACEMIC MIXTURE
    • C12P13/00Preparation of nitrogen-containing organic compounds
    • CCHEMISTRY; METALLURGY
    • C07ORGANIC CHEMISTRY
    • C07CACYCLIC OR CARBOCYCLIC COMPOUNDS
    • C07C231/00Preparation of carboxylic acid amides
    • C07C231/06Preparation of carboxylic acid amides from nitriles by transformation of cyano groups into carboxamide groups
    • CCHEMISTRY; METALLURGY
    • C07ORGANIC CHEMISTRY
    • C07CACYCLIC OR CARBOCYCLIC COMPOUNDS
    • C07C233/00Carboxylic acid amides
    • C07C233/01Carboxylic acid amides having carbon atoms of carboxamide groups bound to hydrogen atoms or to acyclic carbon atoms
    • C07C233/02Carboxylic acid amides having carbon atoms of carboxamide groups bound to hydrogen atoms or to acyclic carbon atoms having nitrogen atoms of carboxamide groups bound to hydrogen atoms or to carbon atoms of unsubstituted hydrocarbon radicals
    • C07C233/09Carboxylic acid amides having carbon atoms of carboxamide groups bound to hydrogen atoms or to acyclic carbon atoms having nitrogen atoms of carboxamide groups bound to hydrogen atoms or to carbon atoms of unsubstituted hydrocarbon radicals with carbon atoms of carboxamide groups bound to carbon atoms of an acyclic unsaturated carbon skeleton
    • CCHEMISTRY; METALLURGY
    • C08ORGANIC MACROMOLECULAR COMPOUNDS; THEIR PREPARATION OR CHEMICAL WORKING-UP; COMPOSITIONS BASED THEREON
    • C08FMACROMOLECULAR COMPOUNDS OBTAINED BY REACTIONS ONLY INVOLVING CARBON-TO-CARBON UNSATURATED BONDS
    • C08F20/00Homopolymers and copolymers of compounds having one or more unsaturated aliphatic radicals, each having only one carbon-to-carbon double bond, and only one being terminated by only one carboxyl radical or a salt, anhydride, ester, amide, imide or nitrile thereof
    • C08F20/02Monocarboxylic acids having less than ten carbon atoms, Derivatives thereof
    • C08F20/52Amides or imides
    • C08F20/54Amides, e.g. N,N-dimethylacrylamide or N-isopropylacrylamide
    • C08F20/56Acrylamide; Methacrylamide
    • CCHEMISTRY; METALLURGY
    • C08ORGANIC MACROMOLECULAR COMPOUNDS; THEIR PREPARATION OR CHEMICAL WORKING-UP; COMPOSITIONS BASED THEREON
    • C08FMACROMOLECULAR COMPOUNDS OBTAINED BY REACTIONS ONLY INVOLVING CARBON-TO-CARBON UNSATURATED BONDS
    • C08F220/00Copolymers of compounds having one or more unsaturated aliphatic radicals, each having only one carbon-to-carbon double bond, and only one being terminated by only one carboxyl radical or a salt, anhydride ester, amide, imide or nitrile thereof
    • C08F220/02Monocarboxylic acids having less than ten carbon atoms; Derivatives thereof
    • C08F220/52Amides or imides
    • C08F220/54Amides, e.g. N,N-dimethylacrylamide or N-isopropylacrylamide
    • C08F220/56Acrylamide; Methacrylamide
    • CCHEMISTRY; METALLURGY
    • C12BIOCHEMISTRY; BEER; SPIRITS; WINE; VINEGAR; MICROBIOLOGY; ENZYMOLOGY; MUTATION OR GENETIC ENGINEERING
    • C12NMICROORGANISMS OR ENZYMES; COMPOSITIONS THEREOF; PROPAGATING, PRESERVING, OR MAINTAINING MICROORGANISMS; MUTATION OR GENETIC ENGINEERING; CULTURE MEDIA
    • C12N9/00Enzymes; Proenzymes; Compositions thereof; Processes for preparing, activating, inhibiting, separating or purifying enzymes
    • C12N9/14Hydrolases (3)
    • CCHEMISTRY; METALLURGY
    • C12BIOCHEMISTRY; BEER; SPIRITS; WINE; VINEGAR; MICROBIOLOGY; ENZYMOLOGY; MUTATION OR GENETIC ENGINEERING
    • C12PFERMENTATION OR ENZYME-USING PROCESSES TO SYNTHESISE A DESIRED CHEMICAL COMPOUND OR COMPOSITION OR TO SEPARATE OPTICAL ISOMERS FROM A RACEMIC MIXTURE
    • C12P13/00Preparation of nitrogen-containing organic compounds
    • C12P13/02Amides, e.g. chloramphenicol or polyamides; Imides or polyimides; Urethanes, i.e. compounds comprising N-C=O structural element or polyurethanes

Landscapes

  • Chemical & Material Sciences (AREA)
  • Organic Chemistry (AREA)
  • Life Sciences & Earth Sciences (AREA)
  • Wood Science & Technology (AREA)
  • Engineering & Computer Science (AREA)
  • Health & Medical Sciences (AREA)
  • Zoology (AREA)
  • Chemical Kinetics & Catalysis (AREA)
  • Genetics & Genomics (AREA)
  • Bioinformatics & Cheminformatics (AREA)
  • Biotechnology (AREA)
  • Biochemistry (AREA)
  • General Engineering & Computer Science (AREA)
  • General Health & Medical Sciences (AREA)
  • Microbiology (AREA)
  • General Chemical & Material Sciences (AREA)
  • Medicinal Chemistry (AREA)
  • Polymers & Plastics (AREA)
  • Molecular Biology (AREA)
  • Biomedical Technology (AREA)
  • Preparation Of Compounds By Using Micro-Organisms (AREA)
  • Addition Polymer Or Copolymer, Post-Treatments, Or Chemical Modifications (AREA)
EP06811414.9A 2005-10-07 2006-10-06 Process for producing amide compound Active EP1944376B1 (en)

Priority Applications (1)

Application Number Priority Date Filing Date Title
EP16187709.7A EP3135767B1 (en) 2005-10-07 2006-10-06 Process for producing acrylamide

Applications Claiming Priority (3)

Application Number Priority Date Filing Date Title
JP2005295561 2005-10-07
JP2005375024 2005-12-27
PCT/JP2006/320087 WO2007043466A1 (en) 2005-10-07 2006-10-06 Process for producing amide compound

Related Child Applications (2)

Application Number Title Priority Date Filing Date
EP16187709.7A Division-Into EP3135767B1 (en) 2005-10-07 2006-10-06 Process for producing acrylamide
EP16187709.7A Division EP3135767B1 (en) 2005-10-07 2006-10-06 Process for producing acrylamide

Publications (3)

Publication Number Publication Date
EP1944376A1 EP1944376A1 (en) 2008-07-16
EP1944376A4 true EP1944376A4 (en) 2012-03-14
EP1944376B1 EP1944376B1 (en) 2016-11-30

Family

ID=37942709

Family Applications (2)

Application Number Title Priority Date Filing Date
EP06811414.9A Active EP1944376B1 (en) 2005-10-07 2006-10-06 Process for producing amide compound
EP16187709.7A Active EP3135767B1 (en) 2005-10-07 2006-10-06 Process for producing acrylamide

Family Applications After (1)

Application Number Title Priority Date Filing Date
EP16187709.7A Active EP3135767B1 (en) 2005-10-07 2006-10-06 Process for producing acrylamide

Country Status (7)

Country Link
US (2) US20090171051A1 (en)
EP (2) EP1944376B1 (en)
JP (2) JP4970276B2 (en)
KR (2) KR20110038183A (en)
CN (1) CN102911973A (en)
AU (1) AU2006300431B2 (en)
WO (1) WO2007043466A1 (en)

Families Citing this family (12)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
AU2013358494B2 (en) * 2012-12-10 2015-11-26 Mitsubishi Chemical Corporation Method for producing acrylamide
US9382560B2 (en) 2013-02-19 2016-07-05 Mitsubishi Rayon Co., Ltd. Method for producing amide compound
CN106795227B (en) * 2014-12-17 2018-10-02 三菱化学株式会社 Aqueous acrylamide solution and process for producing acrylamide polymer
CN106148312A (en) * 2015-04-15 2016-11-23 四川光亚聚合物化工有限公司 The stably method of storage Production of Acrylamide by Microbial Method fermentation broth enzyme activity
US10975177B2 (en) * 2016-03-29 2021-04-13 Solenis Technologies, L.P. Process for producing a polyacrylamide solution with increased viscosity
WO2017186697A1 (en) * 2016-04-26 2017-11-02 Basf Se Method for preparing an aqueous polyacrylamide solution
WO2017186685A1 (en) * 2016-04-26 2017-11-02 Basf Se Method for preparing an aqueous polyacrylamide solution
CN109153748A (en) * 2016-04-26 2019-01-04 巴斯夫欧洲公司 Method for preparing polyacrylamide aqueous solution
AU2019243341B2 (en) * 2018-03-28 2021-09-23 Mitsui Chemicals, Inc. Method for producing amide compound
JP2019176835A (en) * 2018-03-30 2019-10-17 三井化学株式会社 Method for producing amide compound
JP2023523337A (en) * 2019-12-30 2023-06-02 ケミラ・ユルキネン・オサケユフティオ FTNIR spectroscopy for reaction monitoring of acrylamide synthesis
KR20250011936A (en) 2022-06-30 2025-01-22 미쓰이 가가쿠 가부시키가이샤 Mutant nitrile hydratase, nucleic acid encoding the mutant nitrile hydratase, vector and transformant comprising the nucleic acid, method for producing the mutant nitrile hydratase, and method for producing an amide compound

Citations (4)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
US2622097A (en) * 1950-11-13 1952-12-16 American Cyanamid Co Purification of acrylonitrile
WO1993023366A1 (en) * 1992-05-21 1993-11-25 Cryodyne Technologies Inc. Method for purification of acetonitrile
US20020043455A1 (en) * 2000-07-18 2002-04-18 Godbole Sanjay P. Process for the purification and recovery of acetonitrile
WO2005054456A1 (en) * 2003-12-02 2005-06-16 Ciba Specialty Chemicals Water Treatments Limited Strain of rhodococcus rhodochrous ncimb 41164 and its use as producer of nitrile hydratase

Family Cites Families (26)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
JPS5268118A (en) * 1975-11-21 1977-06-06 Mitsui Toatsu Chem Inc Preparation of acrylamide
JPS581108B2 (en) * 1978-05-22 1983-01-10 三井東圧化学株式会社 Acrylonitrile purification method
US4177210A (en) 1978-07-05 1979-12-04 The Dow Chemical Company Hydration of acrylonitrile to acrylamide
GB2114118A (en) * 1982-01-29 1983-08-17 American Cyanamid Co Method for removing aldehyde impurities in acrylonitrile and acrylamide
JPS61115495A (en) * 1984-11-09 1986-06-03 Nitto Chem Ind Co Ltd Production of acrylamide polymer
JPH05308980A (en) 1992-05-07 1993-11-22 Mitsubishi Kasei Corp Production of amide
US5426208A (en) 1992-05-21 1995-06-20 Cryodyne Technologies, Inc. Method of purification of acetonitrile
JPH0655148A (en) 1992-08-06 1994-03-01 Hitachi Ltd Apparatus for washing glass substrate
JP3683916B2 (en) * 1993-07-23 2005-08-17 三井化学株式会社 Method for producing acrylamide
US5476883A (en) * 1993-07-23 1995-12-19 Mitsui Toatsu Chemicals, Inc. Preparation process of acrylamide from purified acrylonitrile
JPH07265091A (en) 1994-03-30 1995-10-17 Mitsubishi Chem Corp Method for producing amide compound
JP3521474B2 (en) 1994-03-30 2004-04-19 ダイヤニトリックス株式会社 Method for producing amide compound
JP3642590B2 (en) * 1994-12-06 2005-04-27 三井化学株式会社 Method for purifying acrylonitrile
US5552305A (en) * 1995-03-30 1996-09-03 E. I. Du Pont De Nemours And Company Biocatalytic conversion of azobisnitriles to cyanoamides or diamides using Pseudomonas, Rhodococcus or Brevibacterium
JP3908803B2 (en) * 1996-02-20 2007-04-25 三井化学株式会社 Method for producing acrylamide
JPH10316714A (en) * 1997-05-15 1998-12-02 Mitsubishi Rayon Co Ltd Production of acrylamide polymer
JP3428404B2 (en) * 1997-10-23 2003-07-22 三菱レイヨン株式会社 Method for producing amide compound
US6153415A (en) * 1998-04-29 2000-11-28 Board Of Trustees Operating Michigan State University Method for producing amide compounds using a nitrile hydratase from a thermophilic bacillus
US6074532A (en) * 1998-11-05 2000-06-13 Nalco/Exxon Energy Chemicals, L.P. Adjunct for removal of aldehydes from chemical manufacturing production streams during distillative purification
KR100482686B1 (en) * 2000-01-17 2005-04-14 미쯔이카가쿠 가부시기가이샤 Method of purifying amide compound
JP4959059B2 (en) * 2000-01-17 2012-06-20 三井化学株式会社 Method for purifying amide compounds
JP4672161B2 (en) 2000-03-29 2011-04-20 三井化学株式会社 Method for producing amide compound
JP2002080443A (en) * 2000-06-20 2002-03-19 Mitsubishi Chemicals Corp Acrylonitrile and method for producing the same
IN209344B (en) * 2000-12-20 2007-09-21 Dia Nitrix Co Ltd
US20070027294A1 (en) * 2003-04-10 2007-02-01 Dia-Nitrix Co., Ltd. Process for producing high-quality acrylamide polymer with enzyme
JP4389064B2 (en) 2003-05-28 2009-12-24 三井化学株式会社 Method for maintaining or improving nitrile hydratase activity

Patent Citations (4)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
US2622097A (en) * 1950-11-13 1952-12-16 American Cyanamid Co Purification of acrylonitrile
WO1993023366A1 (en) * 1992-05-21 1993-11-25 Cryodyne Technologies Inc. Method for purification of acetonitrile
US20020043455A1 (en) * 2000-07-18 2002-04-18 Godbole Sanjay P. Process for the purification and recovery of acetonitrile
WO2005054456A1 (en) * 2003-12-02 2005-06-16 Ciba Specialty Chemicals Water Treatments Limited Strain of rhodococcus rhodochrous ncimb 41164 and its use as producer of nitrile hydratase

Non-Patent Citations (3)

* Cited by examiner, † Cited by third party
Title
KOBAYASHI M ET AL: "Enzymatic synthesis of acrylamide: a success story not yet over", TRENDS IN BIOTECHNOLOGY, ELSEVIER PUBLICATIONS, CAMBRIDGE, GB, vol. 10, 1 January 1992 (1992-01-01), pages 402 - 408, XP023572109, ISSN: 0167-7799, [retrieved on 19920101], DOI: 10.1016/0167-7799(92)90283-2 *
NAGASAWA T ET AL: "MICROBIAL TRANSFORMATIONS OF NITRILES", TRENDS IN BIOTECHNOLOGY, ELSEVIER PUBLICATIONS, CAMBRIDGE, GB, vol. 7, no. 6, 1 June 1989 (1989-06-01), pages 153 - 158, XP001152788, ISSN: 0167-7799, DOI: 10.1016/0167-7799(89)90026-7 *
See also references of WO2007043466A1 *

Also Published As

Publication number Publication date
CN102911973A (en) 2013-02-06
WO2007043466A9 (en) 2007-06-14
KR20080056261A (en) 2008-06-20
EP1944376A1 (en) 2008-07-16
US20090171051A1 (en) 2009-07-02
JP4970276B2 (en) 2012-07-04
AU2006300431B2 (en) 2011-07-21
JPWO2007043466A1 (en) 2009-04-16
WO2007043466A1 (en) 2007-04-19
EP1944376B1 (en) 2016-11-30
JP2012029695A (en) 2012-02-16
EP3135767A1 (en) 2017-03-01
KR20110038183A (en) 2011-04-13
US20110288255A1 (en) 2011-11-24
US8329843B2 (en) 2012-12-11
EP3135767B1 (en) 2020-12-02
AU2006300431A1 (en) 2007-04-19

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