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EP0597840A1 - Corrugated board manufacture - Google Patents

Corrugated board manufacture

Info

Publication number
EP0597840A1
EP0597840A1 EP91909478A EP91909478A EP0597840A1 EP 0597840 A1 EP0597840 A1 EP 0597840A1 EP 91909478 A EP91909478 A EP 91909478A EP 91909478 A EP91909478 A EP 91909478A EP 0597840 A1 EP0597840 A1 EP 0597840A1
Authority
EP
European Patent Office
Prior art keywords
corrugated
mediums
roll
corrugations
tips
Prior art date
Legal status (The legal status is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the status listed.)
Granted
Application number
EP91909478A
Other languages
German (de)
French (fr)
Other versions
EP0597840B1 (en
Inventor
Michael John 2 Sir William Lyons Road Cahill
Colin Stutt
Current Assignee (The listed assignees may be inaccurate. Google has not performed a legal analysis and makes no representation or warranty as to the accuracy of the list.)
Langston Machine Co Ltd
Original Assignee
Langston Machine Co Ltd
Priority date (The priority date is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the date listed.)
Filing date
Publication date
Priority claimed from GB909010815A external-priority patent/GB9010815D0/en
Priority claimed from GB909010814A external-priority patent/GB9010814D0/en
Application filed by Langston Machine Co Ltd filed Critical Langston Machine Co Ltd
Publication of EP0597840A1 publication Critical patent/EP0597840A1/en
Application granted granted Critical
Publication of EP0597840B1 publication Critical patent/EP0597840B1/en
Anticipated expiration legal-status Critical
Expired - Lifetime legal-status Critical Current

Links

Classifications

    • BPERFORMING OPERATIONS; TRANSPORTING
    • B31MAKING ARTICLES OF PAPER, CARDBOARD OR MATERIAL WORKED IN A MANNER ANALOGOUS TO PAPER; WORKING PAPER, CARDBOARD OR MATERIAL WORKED IN A MANNER ANALOGOUS TO PAPER
    • B31FMECHANICAL WORKING OR DEFORMATION OF PAPER, CARDBOARD OR MATERIAL WORKED IN A MANNER ANALOGOUS TO PAPER
    • B31F1/00Mechanical deformation without removing material, e.g. in combination with laminating
    • B31F1/20Corrugating; Corrugating combined with laminating to other layers
    • B31F1/24Making webs in which the channel of each corrugation is transverse to the web feed
    • B31F1/26Making webs in which the channel of each corrugation is transverse to the web feed by interengaging toothed cylinders cylinder constructions
    • B31F1/28Making webs in which the channel of each corrugation is transverse to the web feed by interengaging toothed cylinders cylinder constructions combined with uniting the corrugated webs to flat webs ; Making double-faced corrugated cardboard
    • B31F1/2813Making corrugated cardboard of composite structure, e.g. comprising two or more corrugated layers

Definitions

  • the register rolls are driven by separate motors which are electronically timed with respect to one another to ensure that the flute alignment occurs between the two webs. This timing is achieved with the aid of flute count encoders 35 and 36. Similar encoders are mounted adjacent to the exposed portion of the middle roll of each single-facer machine; Figure 1 shows such an encoder 37 adjacent to the corrugator roll 5 of the lower single-facer 3.

Landscapes

  • Engineering & Computer Science (AREA)
  • Mechanical Engineering (AREA)
  • Machines For Manufacturing Corrugated Board In Mechanical Paper-Making Processes (AREA)
  • Laminated Bodies (AREA)

Abstract

Procédé de fabrication de carton ondulé comprenant deux couches de papier ondulé jointes par alignement des sommets des ondulations des deux couches de papier, sans couche intermédiaire, et avec au moins une couche externe. Ledit procédé consiste à introduire des bandes de carton à onduler entre des paires respectives de rouleaux à onduler de manière à transformer lesdites bandes en carton ondulé, à appliquer de la colle sur les sommets des ondulations de l'une des bandes de carton ondulé, afin de permettre l'adhésion avec les sommets de l'autre bande de carton ondulé, et à faire passer les deux bandes de carton ondulé le long de voies linéaires adjacentes avec alignement sommet à sommet des ondulations des deux bandes de carton, tout en exerçant une pression qui place les bandes en contact l'une avec l'autre tandis que l'on permet ou active le séchage au moins partiel de la colle. Au moins une couche extérieure est appliquée soit avant, soit après le passage des bandes de carton ondulé le long des voies linéaires où les sommets de leurs ondulations sont fixés les uns aux autres.A process for manufacturing corrugated cardboard comprising two layers of corrugated paper joined by aligning the crests of the corrugations of the two layers of paper, without an intermediate layer, and with at least one outer layer. Said method comprises inserting strips of corrugating cardboard between respective pairs of corrugating rollers so as to convert said strips into corrugated cardboard, applying glue to the crests of the corrugations of one of the corrugating cardboard strips, in order to to allow adhesion with the vertices of the other strip of corrugated cardboard, and to pass the two strips of corrugated cardboard along adjacent linear paths with top-to-vertex alignment of the corrugations of the two strips of cardboard, while exerting a pressure that places the strips in contact with each other while allowing or activating at least partial drying of the glue. At least one outer layer is applied either before or after the corrugated strips are passed along the linear paths where the tops of their corrugations are attached to each other.

Description

Corrugated Board Manufacture
This invention is concerned with the manufacture of corrugated board comprising two layers of corrugated medium adhering to one another, with no intermediate liner, and at least one liner adhering to the outer tips of one of the two corrugated mediums. Board of this type is described and illustrated in Australian Patent Applications Nos. 62323/86 and 2271/85, and a machine for manufacturing such board is described in European Patent Application No. 279609, all in the name of Amcor Limited. A further development of the machine is described in our British Patent Application No. PCT/GB 89/01290, to which reference is directed.
According to one aspect of this invention there is provided a process for manufacturing corrugated board comprising two layers of corrugated medium joined together in tip-to-tip registration between the corrugations of the two mediums, without an intermediate liner, and with at least one outer liner, the process comprising feeding webs of corrugating material between respective pairs of corrugating rolls to form the webs into corrugated mediums, applying adhesive to the tips of one of the mediums to permit adhesion with the tips of the other medium, and conveying the two mediums along adjacent linear paths with tip-to-tip registration between the corrugations of the two mediums, while applying pressure urging the mediums into contact with one another while the adhesive is caused or allowed to set at least partially, at least one outer liner being applied either before or after the corrugated mediums are conveyed along the linear paths in which the tips of their corrugations are brought together.
According to another aspect of the present invention, apparatus for manufacturing board of the above mentioned type comprises means for forming two webs of single-faced corrugated board, means for conveying each single faced web on to a corresponding corrugated register conveyor via a path of variable length, means for controlling and equalising the speeds of the two register conveyors, and means for conveying the single-faced webs from the register conveyors and along adjacent linear paths through a pressure device whereby the single-faced webs are pressed together to cause the tips of the corrugated mediums to adhere to one another while they are conveyed through the pressure device, and including means for applying adhesive to one of" the corrugated mediums before the two single-faced webs enter the pressure device.
The means for controlling the speed (and the phase of rotation) of the register rolls with respect with one another, to ensure that the tips of the corrugated materials are accurately aligned, preferably comprises flute count encoders adjacent to the respective register rolls and arranged to control one or both of two independent drive motors for the respective register rolls. Similar flute count encoders are preferably provided adjacent to corrugated rolls of the two single-facer machines whereby the speed of each machine with respect to the corresponding register roll is controlled, any differences being compensated by the means defining a path of variable length between the single-facer machine and the corresponding register roll. The latter means may, for example, comprise a tension roll able to float up and down and adapted to maintain a substantially constant tension in the single faced web.
The pressure device conveys the two single-faced webs along adjacent linear paths. In a preferred arrangement, the pressure device comprises a number of pairs of opposed upper and lower belts, opposed belts being guided so as to be spaced apart by a distance appropriate to press the two corrugated boards together. Between the belts, the boards may be pressed together by air pressure in a chamber above the upper set of belts, the lower belts being arranged to move along a support platen having grooves containing the belts with intermediate lands for supporting the lower corrugated board. Alternatively, or in addition, downward pressure on the upper board may be applied by flexible bristles.
According to another aspect of this invention, apparatus for manufacturing board of the above-described type comprises means for separately corrugating two webs of corrugating medium, means for applying adhesive to the tips of one corrugated medium, means for bringing the tips of the corrugated medium into alignment and for pressing them together, conveyors for conveying the two corrugated mediums along a linear path while pressing the corrugations together to join them at their tips, and means for subsequently applying and adhering at least one outer liner to the joined corrugated mediums.
In a preferred form of apparatus according to this aspect of the invention, the two corrugated mediums are brought and pressed together by two corrugated rolls (i.e. rolls having corrugated peripheries) of which one has a number of circumferential recesses axially spaced along the roll to leave relatively narrow corrugated portions whereby a high pressure can be applied between those corrugated portions and the corresponding corrugations of the other roll to promote adhesion between the corrugated mediums without requiring a correspondingly large total force; that is to say, the total force is significantly less than would be required to produce the same contact pressure along the entire length of the corrugations between two non-recessed corrugated rolls. The recesses preferably accommodate conveyors formed with outer corrugations aligned with the corrugations of the roll, the conveyors being used to convey the two joined corrugated mediums along the linear path in co-operation with one or more similarly corrugated opposed conveyors.
Examples of apparatus according to this invention will now be described with reference to the accompanying drawings. In these drawings:
Figure 1 is a diagrammatic elevation of part of one apparatus according to this invention;
Figure 2 illustrates diagra matically a modification in the region of the pressure device;
Figure 3 is a diagrammatic elevation of another apparatus according to this invention;
Figure 4 is a perspective view of one of the rolls in the apparatus shown in Figure 3; and
Figure 5 shows a modification of the right hand end portion of the apparatus shown in Figure 3.
As shown in Figure 1 , one single-faced corrugated web 2 is formed by a single-facer machine 3 comprising heated upper and lower corrugating rolls 4 and 5 and a heated press roll 6. A web 7 of corrugating medium passes around a pre-conditioner guide 8 by which it is moistened prior to entry into the nip between the corrugating rolls 4 and 5. A gluing device comprising a metering roll 9 and an applicator roll 10 applies glue to the tips of the corrugated medium to cause adhesion with a liner web 11 conveyed around the press roll 6, thus forming a single-faced corrugated web 2 in which the corrugated medium lies above the liner. An infra-red heater 12 applies more heat to the web as it passes towards a pressure device indicated generally by the reference numeral 13.
A similar single-facer machine (not shown), effectively a mirror image of the single facer machine 3 mounted above the machine 3 and slightly further to the left, forms a second single-faced corrugated web 19 of which the corrugated medium lies below the liner.
The single-faced web 2 passes towards the pressure device 13 via a tensioning roll 14 which is movable up and down so as to form a loop of variable lengths between guide rolls 15 and 16. The roll 14 may be of lightweight construction, being in contact with the corrugated material, or may be mounted at its opposite ends on two pivoted levers with counter balance weights so that it applies a limited force to the web 2.
Similarly, an upwardly urged tensioning roll 17 tensions and produces a path of variable length for the second single-faced corrugated web 18.
Corrugated register rolls 19 and 20 associated with the pressure device 13 engage in corrugations of the respective webs 2 and 18 and control the movement of the webs beyond the tensioning devices. The webs pass around the register rolls and around lead rolls 21 and 22 and then converge towards parallel paths extending between sets of upper and lower belts 23 and 24 arranged in upper and lower pairs. These belts are driven by drive rolls 25 and 26 and are tensioned by rolls 27 and 28. The lower belts 24 are supported by a platen 29 having grooves of just sufficient depth to accommodate the belts, the lands between the grooves being at a level such as to support.the lower web 2 during its passage through the pressure device.
An air pressure chamber 30 urges the upper single faced corrugated web 18 downwards on to the lower web to cause adhesion between the tips of the corrugated medium, adhesive having been applied to the upper corrugated medium by a device comprising a metering roll 32 and an applicator roll 33. In addition, or as an alternative, pads formed by flexible bristles may be arranged to press down on the upper web in areas lying between the upper belts, one such bristle being shown for example at 34.
The register rolls are driven by separate motors which are electronically timed with respect to one another to ensure that the flute alignment occurs between the two webs. This timing is achieved with the aid of flute count encoders 35 and 36. Similar encoders are mounted adjacent to the exposed portion of the middle roll of each single-facer machine; Figure 1 shows such an encoder 37 adjacent to the corrugator roll 5 of the lower single-facer 3.
By means of the flute count encoders 35 and 37, for example, a drive motor for the lower single-facer machine is controlled as to its speed so as to maintain an appropriate web speed. This control need not be as accurate as the control between the two register rolls. Means (not shown) are provided for detecting when the tension roll 14 moves upwards beyond a desired upper limit, whereupon the speed of the drive to the single-facer 3 is increased, movement of the tension roll 14 below a desired lower limit being similarly arranged to reduce the speed of the drive to the single- facer 3. A similar control exists between the register roll 20 and the upper single-facer machine.
After leaving the pressure device 13, the double-faced web 50 may pass through a conventional double-facer arrangement (not shown) for applying pressure, pneumatically or by means of weighted conveyors,, to opposite faces of the web 50 over a more extended distance while the adhesive fully sets.
The gap between the conveyor bands 23 and 24 of the pressure device may be adjustable so that, for example, conventional double-faced board (with just one corrugated medium) can be manufactured by feeding a simple liner in place of the single-faced web 18. Another permutation made possible by this apparatus is that a third liner may be fed between the two single-faced corrugated webs to form a "double double" board. To facilitate this possibility, the apparatus may be modified in the region of the pressure device in the manner shown in Figure 2.
As shown in Figure 2, a larger angle of convergence between the two single-faced webs 2 and 18 is provided to facilitate the conveyance between them of a third liner 37. In addition there is a further adhesive applicator comprising rolls 38 and 39 for applying adhesive to the tips of the corrugator medium of the lower web 2.
Figures 3 to 5 show a different machine.
Figure 3 shows webs 101 and 102 of corrugating medium which are corrugated respectively by corrugating rolls 103, 104 and 105, 106. After being corrugated the webs may be held on the respective rolls 104 and 105 by suction supplied through radial passages in the rolls from suction chambers 107 and 107'.
The corrugated medium 102 is further conveyed by a roll 108 which co¬ operates with the roll 104 in bringing together the tips of the respective corrugated mediums. As shown in Figure 4, the roll 108 has a number of circumferential recesses 109 leaving relatively narrow corrugated surfaces .110 for pressing the corrugated mediums 102 against the medium 101. Adhesive is applied to the tips of the corrugations of the medium 101 by an adhesive applicator unit 111.
The corrugated mediums are conveyed beyond the rolls 108 and 104 initially by conveyor belts 112 which are accommodated in the circumferential recesses in the roll 108 and are formed with external corrugated surfaces which are maintained in alignment with the roll corrugations by engagement with the corrugations of the roll 105. The belts, which may be in the form of moulded belts or may comprise chains, pass over a heater 113 and return around a roller 114.
Pressure contact between the tips of the corrugations of the two mediums is maintained, during movement along the linear path between the rolls 108 and 114" "with the aid of a further set of corrugated conveyor belts 115 passing around rolls 116 and 117. The belts 115 are maintained in appropriate timed relation to the belts 112; for example, the belts 115 may have internal timing teeth meshing with teeth on the roll 116, which may in turn be driven from, for example, the roll 108 via gears or a timing belt. A further heater 118 helps to dry the adhesive.
The conveyor belts 112 continue to support the corrugated mediums while adhesive is applied to the tips of the upper medium, by a device 119', prior to the application of a first liner 119. The tips of the lower medium then receive adhesive from a device 120' in preparation for the application of a second liner 120. Further heaters 121 and 122 apply heat to the complete product, and any suitable known means (not shown) may be used for applying pressure until the adhesive is substantially fully set.
Figure 5 shows an example of another way in which the two outer liners may be applied to the corrugated mediums. The joined corrugated mediums remain on the roller 114, being held by suction from a suction chamber 121, until they are received by a further corrugated roll 122 on which they are held by suction transmitted from a chamber 123. Adhesive is applied to the exposed outer tips of the lower corrugated medium by a device 124, and a liner 125 is then applied to the corrugated mediums, being pressed against them by a heated roll 126. The single-faced corrugated board is then received by a further roll 127 having a smooth circumference, and is held on the roll 127 by suction transmitted from a chamber 128 while adhesive is being applied to the exposed outer tips of the upper corrugated medium by a device 129. A second liner 130 is then applied with the aid of a heated roller 131 so as to form the desired board 132. The board 132 may then pass through any conventional pneumatic or other pressure device for pressing the components of the board together along an extended distance while the adhesive is allowed to fully set.
With reference to Figure 3, quick adhesion between the corrugated mediums may be achieved by applying a quick-setting adhesive to the corrugated medium 101 along bands corresponding to the corrugated positions 110 of the roll 108. Between those bands a slower drying adhesive may be used.

Claims

Claims:
1. A process for manufacturing corrugated board comprising two layers of corrugated medium joined together in tip-to-tip registration between the corrugations of the two mediums, without an intermediate liner, and with at least one outer liner, the process comprising feeding webs of corrugating material between respective pairs of corrugating rolls to form the webs into corrugated mediums, applying adhesive to the tips of one of the mediums to permit adhesion with the tips of the other medium, and conveying the two mediums along adjacent linear paths with tip-to-tip registration between the corrugations of the two mediums, while applying pressure urging the mediums into contact with one another while the adhesive is caused or allowed to set at least partially, at least one outer liner being applied either before or after the corrugated mediums are conveyed along the linear paths in which the tips of their corrugations are brought together.
2. A process according to claim 1 in which two outer liners are joined to the respective corrugated mediums before the mediums are brought together to be joined to one another.
3. A process according to claim 1 in which two outer liners are joined to the respective corrugated mediums after the corrugated mediums have been joined to one another.
4. Apparatus for carrying out the process according to claim 2, comprising means (3) for forming two webs (2,18) of single-faced corrugated board, means for conveying each single faced web on to a corresponding corrugated register conveyor via a path of variable length, means for controlling and equalising the speeds of the two register conveyors, and means for conveying the single-faced webs from the register conveyors and along adjacent linear paths through a pressure device whereby the single- faced webs are pressed together to cause the tips of the corrugated mediums to adhere to one another while they are conveyed through the pressure device, and including means for applying adhesive to one of the corrugated mediums before the two single-faced webs enter the pressure device.
5. Apparatus according to claim 4 in which the means for conveying the webs (2,18) through the pressure device (13) comprises a pair or a number of pairs of opposed belts (23,24).
6. Apparatus according to claim 5 in which pressure device includes a pressure chamber (23) adjacent to the belt or belts (23) bearing on one of the liners.
7. Apparatus according to claim 6 in which a number of parallel belts (24) bearing on the other liner are, while doing so, arranged to move through grooves in a support plate which supports the adjacent liner in areas lying between the belts.
8. Apparatus according to any one of claims 4 to 7 in which each of the single-faced webs is arranged to move from its single facer machine (3) to its corresponding register conveyor (189) along a path of variable length including a tensioning roll (14), and in which the speed of each single- facer machine is controlled in response to the position of the corresponding tensioning roll.
9. Apparatus according to any one of claims 4 to 8 in which the means for equalising the speeds of the two register conveyors (19,20) comprises flute count encoders (35,36) adjacent to the respective register conveyors.
10. Apparatus for carrying out the process according to claim 1, comprising means (105, 106; 103, 104) for separately corrugating two webs (101,102) of corrugating medium, means (111) for applying adhesive to the tips of one corrugated medium, means (108) for bringing the tips of the corrugated mediums into alignment and for pressing them together, conveyors (112, 115) for conveying the two corrugated mediums along a linear path while pressing the corrugations together to join them at their tips, and means (119) for subsequently applying and adhering at least one outer liner (119) to the joined corrugated mediums.
11. Apparatus according to claim 10 in which the means for pressing together the two corrugated mediums comprises two corrugated rolls (108, 104) of which one (108) has a number of circumferential recesses (109) axial ly spaced along the roll to leave relatively narrow corrugated portions (110) whereby a high pressure can be applied between those corrugated portions and the corresponding corrugations of the other roll (109) to promote adhesion between the corrugated mediums without requiring a correspondingly large total force.
12. Apparatus according to claim 11 in which the recesses (109) accommodate conveyors (112) formed with outer corrugations aligned with the corrugations of the roll, the conveyors being used to convey the two joined corrugated mediums along the linear path in co-operation with one or more similarly corrugated opposed conveyors (115).
13. Apparatus according to claim 12 in which the joined corrugated mediums (101, 102) after leaving the primary means (112, 113, 115, 118), are received by a corrugated roll (1122) adjacent to which there is an adhesive device (124) for applying adhesive to the tips of the corrugations of the outer medium, followed by a roll for applying and pressing one liner (125) to the adhesive-bearing medium.
14. Apparatus according to claim 13 including a further corrugated roll (127) which receives the single-lined mediums and adjacent to which there is an adhesive device (129) for applying adhesive to the tips of the corrugators of the then-outer medium, followed by a roll (131) for applying and pressing a second liner (130) to the outer medium, the double-lined board (132) so formed being conveyed tangential ly from the further conveyor roll (127).
EP91909478A 1990-05-15 1991-05-14 Corrugated board manufacture Expired - Lifetime EP0597840B1 (en)

Applications Claiming Priority (5)

Application Number Priority Date Filing Date Title
GB909010815A GB9010815D0 (en) 1990-05-15 1990-05-15 Corrugrated board manufacture
GB9010815 1990-05-15
GB909010814A GB9010814D0 (en) 1990-05-15 1990-05-15 Corrugated board manufacture
GB9010814 1990-05-15
PCT/GB1991/000758 WO1991017881A1 (en) 1990-05-15 1991-05-14 Corrugated board manufacture

Publications (2)

Publication Number Publication Date
EP0597840A1 true EP0597840A1 (en) 1994-05-25
EP0597840B1 EP0597840B1 (en) 1998-07-22

Family

ID=26297075

Family Applications (1)

Application Number Title Priority Date Filing Date
EP91909478A Expired - Lifetime EP0597840B1 (en) 1990-05-15 1991-05-14 Corrugated board manufacture

Country Status (6)

Country Link
EP (1) EP0597840B1 (en)
JP (1) JPH05506825A (en)
AU (1) AU664018B2 (en)
DE (1) DE69129863T2 (en)
NZ (1) NZ238143A (en)
WO (1) WO1991017881A1 (en)

Families Citing this family (6)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
DE4420958A1 (en) * 1994-06-16 1995-12-21 Bhs Corr Masch & Anlagenbau Machine for the production of a single-sided laminated corrugated cardboard web
AUPN367095A0 (en) * 1995-06-20 1995-07-13 Amcor Limited Corrugated board manufacture
JP2786620B2 (en) * 1996-08-23 1998-08-13 三菱重工業株式会社 Corrugated sheet manufacturing equipment
EP0869865A1 (en) * 1996-10-30 1998-10-14 Best Carton, Ltd. Production of corrugated board structures
DE19828124A1 (en) * 1998-06-25 1999-12-30 Bhs Corr Masch & Anlagenbau Method for producing a metal foam workpiece
DE19954301A1 (en) * 1999-11-11 2001-05-17 Bhs Corr Masch & Anlagenbau Process and plant for the production of at least 4-ply corrugated cardboard

Family Cites Families (6)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
FR12081E (en) * 1910-07-05 Societe L. Sutre Et J. Tardieu Packaging and material to make it
FR1494318A (en) * 1966-07-29 1967-09-08 Creusot Forges Ateliers Method and machine for the continuous manufacture of rigid, cross-corrugated corrugated board
US3700518A (en) * 1971-03-17 1972-10-24 Honshu Paper Co Ltd Method for manufacturing a composite corrugated paper board
CA1312540C (en) * 1987-12-18 1993-01-12 Peter Gordon Bennett Forming corrugated board structures
AU615053B2 (en) * 1988-03-31 1991-09-19 Amcor Limited Manufacturing corrugated board
WO1989009127A1 (en) * 1988-03-31 1989-10-05 Amcor Limited Manufacturing corrugated board

Non-Patent Citations (1)

* Cited by examiner, † Cited by third party
Title
See references of WO9117881A1 *

Also Published As

Publication number Publication date
DE69129863D1 (en) 1998-08-27
AU7874191A (en) 1991-12-10
DE69129863T2 (en) 1998-12-03
WO1991017881A1 (en) 1991-11-28
JPH05506825A (en) 1993-10-07
NZ238143A (en) 1993-04-28
EP0597840B1 (en) 1998-07-22
AU664018B2 (en) 1995-11-02

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