DE60336287D1 - Durchführung und Optimierung eines Druckwechseladsorptionsverfahrens - Google Patents
Durchführung und Optimierung eines DruckwechseladsorptionsverfahrensInfo
- Publication number
- DE60336287D1 DE60336287D1 DE60336287T DE60336287T DE60336287D1 DE 60336287 D1 DE60336287 D1 DE 60336287D1 DE 60336287 T DE60336287 T DE 60336287T DE 60336287 T DE60336287 T DE 60336287T DE 60336287 D1 DE60336287 D1 DE 60336287D1
- Authority
- DE
- Germany
- Prior art keywords
- adsorbable component
- strongly adsorbable
- swing adsorption
- pressure swing
- adsorption process
- Prior art date
- Legal status (The legal status is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the status listed.)
- Expired - Lifetime
Links
Classifications
-
- B—PERFORMING OPERATIONS; TRANSPORTING
- B01—PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
- B01D—SEPARATION
- B01D53/00—Separation of gases or vapours; Recovering vapours of volatile solvents from gases; Chemical or biological purification of waste gases, e.g. engine exhaust gases, smoke, fumes, flue gases, aerosols
- B01D53/02—Separation of gases or vapours; Recovering vapours of volatile solvents from gases; Chemical or biological purification of waste gases, e.g. engine exhaust gases, smoke, fumes, flue gases, aerosols by adsorption, e.g. preparative gas chromatography
- B01D53/04—Separation of gases or vapours; Recovering vapours of volatile solvents from gases; Chemical or biological purification of waste gases, e.g. engine exhaust gases, smoke, fumes, flue gases, aerosols by adsorption, e.g. preparative gas chromatography with stationary adsorbents
- B01D53/047—Pressure swing adsorption
-
- B—PERFORMING OPERATIONS; TRANSPORTING
- B01—PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
- B01D—SEPARATION
- B01D2253/00—Adsorbents used in seperation treatment of gases and vapours
- B01D2253/10—Inorganic adsorbents
- B01D2253/102—Carbon
-
- B—PERFORMING OPERATIONS; TRANSPORTING
- B01—PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
- B01D—SEPARATION
- B01D2253/00—Adsorbents used in seperation treatment of gases and vapours
- B01D2253/10—Inorganic adsorbents
- B01D2253/104—Alumina
-
- B—PERFORMING OPERATIONS; TRANSPORTING
- B01—PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
- B01D—SEPARATION
- B01D2253/00—Adsorbents used in seperation treatment of gases and vapours
- B01D2253/10—Inorganic adsorbents
- B01D2253/106—Silica or silicates
- B01D2253/108—Zeolites
-
- B—PERFORMING OPERATIONS; TRANSPORTING
- B01—PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
- B01D—SEPARATION
- B01D2253/00—Adsorbents used in seperation treatment of gases and vapours
- B01D2253/25—Coated, impregnated or composite adsorbents
-
- B—PERFORMING OPERATIONS; TRANSPORTING
- B01—PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
- B01D—SEPARATION
- B01D2253/00—Adsorbents used in seperation treatment of gases and vapours
- B01D2253/30—Physical properties of adsorbents
- B01D2253/302—Dimensions
- B01D2253/304—Linear dimensions, e.g. particle shape, diameter
-
- B—PERFORMING OPERATIONS; TRANSPORTING
- B01—PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
- B01D—SEPARATION
- B01D2256/00—Main component in the product gas stream after treatment
- B01D2256/12—Oxygen
-
- B—PERFORMING OPERATIONS; TRANSPORTING
- B01—PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
- B01D—SEPARATION
- B01D2256/00—Main component in the product gas stream after treatment
- B01D2256/16—Hydrogen
-
- B—PERFORMING OPERATIONS; TRANSPORTING
- B01—PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
- B01D—SEPARATION
- B01D2257/00—Components to be removed
- B01D2257/10—Single element gases other than halogens
- B01D2257/102—Nitrogen
-
- B—PERFORMING OPERATIONS; TRANSPORTING
- B01—PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
- B01D—SEPARATION
- B01D2257/00—Components to be removed
- B01D2257/50—Carbon oxides
- B01D2257/502—Carbon monoxide
-
- B—PERFORMING OPERATIONS; TRANSPORTING
- B01—PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
- B01D—SEPARATION
- B01D2257/00—Components to be removed
- B01D2257/80—Water
-
- B—PERFORMING OPERATIONS; TRANSPORTING
- B01—PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
- B01D—SEPARATION
- B01D2259/00—Type of treatment
- B01D2259/40—Further details for adsorption processes and devices
- B01D2259/40007—Controlling pressure or temperature swing adsorption
-
- B—PERFORMING OPERATIONS; TRANSPORTING
- B01—PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
- B01D—SEPARATION
- B01D2259/00—Type of treatment
- B01D2259/40—Further details for adsorption processes and devices
- B01D2259/40011—Methods relating to the process cycle in pressure or temperature swing adsorption
- B01D2259/40058—Number of sequence steps, including sub-steps, per cycle
- B01D2259/40062—Four
-
- B—PERFORMING OPERATIONS; TRANSPORTING
- B01—PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
- B01D—SEPARATION
- B01D2259/00—Type of treatment
- B01D2259/40—Further details for adsorption processes and devices
- B01D2259/414—Further details for adsorption processes and devices using different types of adsorbents
- B01D2259/4141—Further details for adsorption processes and devices using different types of adsorbents within a single bed
- B01D2259/4145—Further details for adsorption processes and devices using different types of adsorbents within a single bed arranged in series
- B01D2259/4146—Contiguous multilayered adsorbents
-
- B—PERFORMING OPERATIONS; TRANSPORTING
- B01—PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
- B01D—SEPARATION
- B01D53/00—Separation of gases or vapours; Recovering vapours of volatile solvents from gases; Chemical or biological purification of waste gases, e.g. engine exhaust gases, smoke, fumes, flue gases, aerosols
- B01D53/26—Drying gases or vapours
- B01D53/261—Drying gases or vapours by adsorption
Landscapes
- Chemical & Material Sciences (AREA)
- Engineering & Computer Science (AREA)
- Analytical Chemistry (AREA)
- General Chemical & Material Sciences (AREA)
- Oil, Petroleum & Natural Gas (AREA)
- Chemical Kinetics & Catalysis (AREA)
- Separation Of Gases By Adsorption (AREA)
- Solid-Sorbent Or Filter-Aiding Compositions (AREA)
- Oxygen, Ozone, And Oxides In General (AREA)
- Hydrogen, Water And Hydrids (AREA)
- Auxiliary Devices For And Details Of Packaging Control (AREA)
Applications Claiming Priority (1)
Application Number | Priority Date | Filing Date | Title |
---|---|---|---|
US10/192,360 US6605136B1 (en) | 2002-07-10 | 2002-07-10 | Pressure swing adsorption process operation and optimization |
Publications (1)
Publication Number | Publication Date |
---|---|
DE60336287D1 true DE60336287D1 (de) | 2011-04-21 |
Family
ID=27662667
Family Applications (1)
Application Number | Title | Priority Date | Filing Date |
---|---|---|---|
DE60336287T Expired - Lifetime DE60336287D1 (de) | 2002-07-10 | 2003-07-03 | Durchführung und Optimierung eines Druckwechseladsorptionsverfahrens |
Country Status (7)
Country | Link |
---|---|
US (1) | US6605136B1 (de) |
EP (1) | EP1380336B2 (de) |
JP (1) | JP4028447B2 (de) |
CN (1) | CN1306988C (de) |
AT (1) | ATE500876T1 (de) |
DE (1) | DE60336287D1 (de) |
ES (1) | ES2359687T5 (de) |
Families Citing this family (63)
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US7954490B2 (en) | 2005-02-09 | 2011-06-07 | Vbox, Incorporated | Method of providing ambulatory oxygen |
US7404846B2 (en) * | 2005-04-26 | 2008-07-29 | Air Products And Chemicals, Inc. | Adsorbents for rapid cycle pressure swing adsorption processes |
US7390350B2 (en) * | 2005-04-26 | 2008-06-24 | Air Products And Chemicals, Inc. | Design and operation methods for pressure swing adsorption systems |
US7651549B2 (en) | 2006-06-13 | 2010-01-26 | Air Products And Chemicals, Inc. | Pressure swing adsorption process with improved recovery of high-purity product |
US20080028933A1 (en) * | 2006-08-07 | 2008-02-07 | Ross David A | Radial sieve module |
CA2667051A1 (en) * | 2006-10-20 | 2008-04-24 | Sumitomo Seika Chemicals Co., Ltd. | Method and apparatus for separating hydrogen gas |
US7828878B2 (en) * | 2006-12-15 | 2010-11-09 | Praxair Technology, Inc. | High frequency PSA process for gas separation |
FR2913969B1 (fr) * | 2007-03-22 | 2010-02-19 | Air Liquide | Ecretement des pics d'impurete |
US20090065007A1 (en) * | 2007-09-06 | 2009-03-12 | Wilkinson William R | Oxygen concentrator apparatus and method |
US8906138B2 (en) | 2007-11-12 | 2014-12-09 | Exxonmobil Upstream Research Company | Methods of generating and utilizing utility gas |
EP2276550A4 (de) | 2008-04-30 | 2012-02-29 | Exxonmobil Upstream Res Co | Verfahren und vorrichtung zur entfernung von öl aus einem nutzgasstrom |
US20120000462A1 (en) | 2010-04-07 | 2012-01-05 | Chart Sequal Technologies Inc. | Portable Oxygen Delivery Device |
WO2011149640A1 (en) | 2010-05-28 | 2011-12-01 | Exxonmobil Upstream Research Company | Integrated adsorber head and valve design and swing adsorption methods related thereto |
US20120055475A1 (en) | 2010-09-07 | 2012-03-08 | Wilkinson William R | Oxygen concentrator system and methods for oral delivery of oxygen enriched gas |
US8616207B2 (en) | 2010-09-07 | 2013-12-31 | Inova Labs, Inc. | Oxygen concentrator heat management system and method |
US8535414B2 (en) * | 2010-09-30 | 2013-09-17 | Air Products And Chemicals, Inc. | Recovering of xenon by adsorption process |
US8734570B2 (en) | 2010-10-13 | 2014-05-27 | Wintek Corporation | Pressure and vacuum swing adsorption separation processes |
TWI495501B (zh) | 2010-11-15 | 2015-08-11 | Exxonmobil Upstream Res Co | 動力分餾器及用於氣體混合物之分餾的循環法 |
WO2012161828A1 (en) | 2011-03-01 | 2012-11-29 | Exxonmobil Upstream Research Company | Apparatus and systems having a rotary valve assembly and swing adsorption processes related thereto |
CA2825148C (en) | 2011-03-01 | 2017-06-20 | Exxonmobil Upstream Research Company | Methods of removing contaminants from a hydrocarbon stream by swing adsorption and related apparatus and systems |
WO2012118757A1 (en) | 2011-03-01 | 2012-09-07 | Exxonmobil Upstream Research Company | Apparatus and systems having a reciprocating valve head assembly and swing adsorption processes related thereto |
WO2012118760A2 (en) | 2011-03-01 | 2012-09-07 | Exxonmobil Upstream Research Company | Apparatus and systems having compact configuration multiple swing adsorption beds and methods related thereto |
MY173802A (en) | 2011-03-01 | 2020-02-24 | Exxonmobil Upstream Res Co | Apparatus and systems having an encased adsorbent contractor and swing adsorption processes related thereto |
EA201391249A1 (ru) | 2011-03-01 | 2014-02-28 | Эксонмобил Апстрим Рисерч Компани | Устройства и системы, имеющие узел поворотного клапана, и связанные с этим циклические адсорбционные процессы |
BR112013018276A2 (pt) | 2011-03-01 | 2019-09-24 | Exxonmobil Upstream Res Co | métodos de remover contaminantes de uma corrente de hidrocarbonetos por adsorção oscilante e aparelhos e sistemas relacionados |
US9034078B2 (en) | 2012-09-05 | 2015-05-19 | Exxonmobil Upstream Research Company | Apparatus and systems having an adsorbent contactor and swing adsorption processes related thereto |
EP3578220B1 (de) | 2012-10-12 | 2023-05-24 | Inova Labs, Inc. | Sauerstoffkonzentratorsysteme und -verfahren |
US9440036B2 (en) | 2012-10-12 | 2016-09-13 | InovaLabs, LLC | Method and systems for the delivery of oxygen enriched gas |
BR112015008210A2 (pt) | 2012-10-12 | 2017-07-04 | Inova Labs Inc | métodos e sistemas de concentrador de oxigênio dual. |
US9440179B2 (en) | 2014-02-14 | 2016-09-13 | InovaLabs, LLC | Oxygen concentrator pump systems and methods |
WO2016014232A1 (en) | 2014-07-25 | 2016-01-28 | Exxonmobil Upstream Research Company | Apparatus and system having a valve assembly and swing adsorption processes related thereto |
US10307749B2 (en) | 2014-11-11 | 2019-06-04 | Exxonmobil Upstream Research Company | High capacity structures and monoliths via paste imprinting |
US9713787B2 (en) | 2014-12-10 | 2017-07-25 | Exxonmobil Upstream Research Company | Adsorbent-incorporated polymer fibers in packed bed and fabric contactors, and methods and devices using same |
US9744521B2 (en) | 2014-12-23 | 2017-08-29 | Exxonmobil Upstream Research Company | Structured adsorbent beds, methods of producing the same and uses thereof |
EA201792488A1 (ru) | 2015-05-15 | 2018-03-30 | Эксонмобил Апстрим Рисерч Компани | Аппарат и система для процессов короткоцикловой адсорбции, связанные с ней, содержащие системы продувки среднего слоя |
US9751041B2 (en) | 2015-05-15 | 2017-09-05 | Exxonmobil Upstream Research Company | Apparatus and system for swing adsorption processes related thereto |
CA2996139C (en) | 2015-09-02 | 2021-06-15 | Exxonmobil Upstream Research Company | Process and system for swing adsorption using an overhead stream of a demethanizer as purge gas |
US10080991B2 (en) | 2015-09-02 | 2018-09-25 | Exxonmobil Upstream Research Company | Apparatus and system for swing adsorption processes related thereto |
SG11201802604TA (en) | 2015-10-27 | 2018-05-30 | Exxonmobil Upstream Res Co | Apparatus and system for swing adsorption processes related thereto having actively-controlled feed poppet valves and passively controlled product valves |
SG11201802606VA (en) | 2015-10-27 | 2018-05-30 | Exxonmobil Upstream Res Co | Apparatus and system for swing adsorption processes related thereto having a plurality of valves |
US10322365B2 (en) | 2015-10-27 | 2019-06-18 | Exxonmobil Upstream Reseach Company | Apparatus and system for swing adsorption processes related thereto |
SG11201803968XA (en) | 2015-11-16 | 2018-06-28 | Exxonmobil Upstream Res Co | Adsorbent materials and methods of adsorbing carbon dioxide |
US10427088B2 (en) | 2016-03-18 | 2019-10-01 | Exxonmobil Upstream Research Company | Apparatus and system for swing adsorption processes related thereto |
WO2017192660A1 (en) | 2016-05-03 | 2017-11-09 | Inova Labs, Inc. | Method and systems for the delivery of oxygen enriched gas |
EP3463620A1 (de) | 2016-05-31 | 2019-04-10 | ExxonMobil Upstream Research Company | Vorrichtung und system für wechseladsorptionsprozesse |
US10427089B2 (en) | 2016-05-31 | 2019-10-01 | Exxonmobil Upstream Research Company | Apparatus and system for swing adsorption processes |
US10434458B2 (en) | 2016-08-31 | 2019-10-08 | Exxonmobil Upstream Research Company | Apparatus and system for swing adsorption processes related thereto |
WO2018044501A1 (en) | 2016-09-01 | 2018-03-08 | Exxonmobil Upstream Research Company | Swing adsorption processes for removing water using 3a zeolite structures |
US10328382B2 (en) | 2016-09-29 | 2019-06-25 | Exxonmobil Upstream Research Company | Apparatus and system for testing swing adsorption processes |
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CN109248541B (zh) * | 2017-07-12 | 2021-03-05 | 中国石油化工股份有限公司 | 氢气回收系统协同优化方法及系统 |
US11571651B2 (en) | 2017-12-22 | 2023-02-07 | Praxair Technology, Inc. | Core-shell composite adsorbent for use in hydrogen and helium PSA processes |
US11331620B2 (en) | 2018-01-24 | 2022-05-17 | Exxonmobil Upstream Research Company | Apparatus and system for swing adsorption processes |
WO2019168628A1 (en) | 2018-02-28 | 2019-09-06 | Exxonmobil Upstream Research Company | Apparatus and system for swing adsorption processes |
US10835856B2 (en) * | 2018-08-14 | 2020-11-17 | Air Products And Chemicals, Inc. | Carbon molecular sieve adsorbent |
WO2020131496A1 (en) | 2018-12-21 | 2020-06-25 | Exxonmobil Upstream Research Company | Flow modulation systems, apparatus, and methods for cyclical swing adsorption |
CN111375288B (zh) * | 2018-12-27 | 2022-04-05 | 中国石油化工股份有限公司 | 存储器、变压吸附装置的优化方法、装置及设备 |
US11376545B2 (en) | 2019-04-30 | 2022-07-05 | Exxonmobil Upstream Research Company | Rapid cycle adsorbent bed |
US11642486B2 (en) | 2019-05-17 | 2023-05-09 | Breathe Technologies, Inc. | Portable oxygen concentrator retrofit system and method |
US11607519B2 (en) | 2019-05-22 | 2023-03-21 | Breathe Technologies, Inc. | O2 concentrator with sieve bed bypass and control method thereof |
US11655910B2 (en) | 2019-10-07 | 2023-05-23 | ExxonMobil Technology and Engineering Company | Adsorption processes and systems utilizing step lift control of hydraulically actuated poppet valves |
WO2021076594A1 (en) | 2019-10-16 | 2021-04-22 | Exxonmobil Upstream Research Company | Dehydration processes utilizing cationic zeolite rho |
Family Cites Families (22)
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US3430418A (en) * | 1967-08-09 | 1969-03-04 | Union Carbide Corp | Selective adsorption process |
US4194891A (en) * | 1978-12-27 | 1980-03-25 | Union Carbide Corporation | Multiple bed rapid pressure swing adsorption for oxygen |
US5240474A (en) * | 1991-01-23 | 1993-08-31 | Air Products And Chemicals, Inc. | Air separation by pressure swing adsorption with a high capacity carbon molecular sieve |
US5226933A (en) * | 1992-03-31 | 1993-07-13 | Ohio State University | Pressure swing adsorption system to purify oxygen |
FR2731918B1 (fr) * | 1995-03-24 | 1997-05-23 | Air Liquide | Procede de separation d'azote de composes moins polaires |
FR2743507B1 (fr) | 1996-01-16 | 1998-03-06 | Air Liquide | Procede pour la separation de melanges d'oxygene et d'azote utilisant un adsorbant a porosite amelioree |
FR2758739B1 (fr) * | 1997-01-24 | 1999-02-26 | Ceca Sa | Perfectionnement dans les procedes psa de purification de l'hydrogene |
FR2765491B1 (fr) * | 1997-07-07 | 1999-08-06 | Air Liquide | Procede de separation d'un flux gazeux par un procede psa |
FR2767717B1 (fr) | 1997-08-28 | 1999-10-01 | Air Liquide | Granulometrie et epaisseur de lit d'une unite psa |
FR2771656B1 (fr) * | 1997-12-01 | 2000-01-07 | Air Liquide | Procede psa mettant en oeuvre un adsorbant a proprietes de capacite et/ou de selectivite heterogenes |
US6500234B1 (en) * | 1998-02-27 | 2002-12-31 | Praxair Technology, Inc. | Rate-enhanced gas separation |
BR9908291A (pt) | 1998-02-27 | 2000-10-31 | Praxair Technology Inc | Processos para a separação de nitrogênio de um gás de alimentação incluindo nitrogênio, para a seleção de adsorventes para uso na separação de nitrogênio de um gás contendo nitrogênio, para a produção de oxigênio a partir de ar e para melhorar o desempenho de um dado material adsorvente, e, aparelhagem para medir a taxa na qual um material adsorvìvel é adsorvido por um adsorvente |
WO1999043418A1 (en) | 1998-02-27 | 1999-09-02 | Praxair Technology, Inc. | Pressure swing adsorption gas separation method, using adsorbents with high intrinsic diffusivity and low pressure ratios |
AU2792899A (en) | 1998-02-27 | 1999-09-15 | Praxair Technology, Inc. | Advanced adsorbent for psa |
US6156101A (en) | 1999-02-09 | 2000-12-05 | Air Products And Chemicals, Inc. | Single bed pressure swing adsorption process and system |
FR2792220B1 (fr) * | 1999-04-19 | 2001-06-15 | Air Liquide | Procede psa mettant en oeuvre un adsorbant a resistance intrinseque favorable a la cinetique d'adsorption |
FR2799991B1 (fr) * | 1999-10-26 | 2002-10-11 | Air Liquide | Procede de production d'hydrogene utilisant un adsorbant carbone a parametres de dubinin selectionnes |
US6302943B1 (en) * | 1999-11-02 | 2001-10-16 | Air Products And Chemicals, Inc. | Optimum adsorbents for H2 recovery by pressure and vacuum swing absorption |
BR0104080A (pt) * | 2000-09-15 | 2002-04-23 | Praxair Technology Inc | Leito adsorvente para uso na separação de um ou mais componentes de uma mistura dos gases da mistura gasosa, e, aparelhagem para carregamento de múltiplos adsorventes para dentro de um leito |
US6468328B2 (en) * | 2000-12-18 | 2002-10-22 | Air Products And Chemicals, Inc. | Oxygen production by adsorption |
US6790260B2 (en) * | 2000-12-20 | 2004-09-14 | Praxair Technology, Inc. | Enhanced rate PSA process |
US6551384B1 (en) * | 2001-07-05 | 2003-04-22 | Praxair Technology, Inc. | Medical oxygen concentrator |
-
2002
- 2002-07-10 US US10/192,360 patent/US6605136B1/en not_active Expired - Lifetime
-
2003
- 2003-07-03 ES ES03014498.4T patent/ES2359687T5/es not_active Expired - Lifetime
- 2003-07-03 AT AT03014498T patent/ATE500876T1/de not_active IP Right Cessation
- 2003-07-03 DE DE60336287T patent/DE60336287D1/de not_active Expired - Lifetime
- 2003-07-03 EP EP03014498.4A patent/EP1380336B2/de not_active Expired - Lifetime
- 2003-07-09 JP JP2003194365A patent/JP4028447B2/ja not_active Expired - Lifetime
- 2003-07-10 CN CNB031476201A patent/CN1306988C/zh not_active Expired - Fee Related
Also Published As
Publication number | Publication date |
---|---|
CN1478584A (zh) | 2004-03-03 |
ES2359687T3 (es) | 2011-05-25 |
US6605136B1 (en) | 2003-08-12 |
ES2359687T5 (es) | 2014-11-11 |
ATE500876T1 (de) | 2011-03-15 |
EP1380336B2 (de) | 2014-10-01 |
EP1380336A1 (de) | 2004-01-14 |
JP4028447B2 (ja) | 2007-12-26 |
JP2004058056A (ja) | 2004-02-26 |
CN1306988C (zh) | 2007-03-28 |
EP1380336B1 (de) | 2011-03-09 |
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