DE60304330D1 - Verfahren zur gewinnung von hochreinem uran aus schwacher düngemittelgradiger phosphorsäure - Google Patents
Verfahren zur gewinnung von hochreinem uran aus schwacher düngemittelgradiger phosphorsäureInfo
- Publication number
- DE60304330D1 DE60304330D1 DE60304330T DE60304330T DE60304330D1 DE 60304330 D1 DE60304330 D1 DE 60304330D1 DE 60304330 T DE60304330 T DE 60304330T DE 60304330 T DE60304330 T DE 60304330T DE 60304330 D1 DE60304330 D1 DE 60304330D1
- Authority
- DE
- Germany
- Prior art keywords
- phosphoric acid
- hydrogen peroxide
- uranium
- acid
- stripped
- Prior art date
- Legal status (The legal status is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the status listed.)
- Expired - Lifetime
Links
- NBIIXXVUZAFLBC-UHFFFAOYSA-N Phosphoric acid Chemical compound OP(O)(O)=O NBIIXXVUZAFLBC-UHFFFAOYSA-N 0.000 title abstract 10
- 229910000147 aluminium phosphate Inorganic materials 0.000 title abstract 5
- 229910052770 Uranium Inorganic materials 0.000 title abstract 3
- 238000000034 method Methods 0.000 title abstract 2
- JFALSRSLKYAFGM-UHFFFAOYSA-N uranium(0) Chemical compound [U] JFALSRSLKYAFGM-UHFFFAOYSA-N 0.000 title abstract 2
- MHAJPDPJQMAIIY-UHFFFAOYSA-N Hydrogen peroxide Chemical compound OO MHAJPDPJQMAIIY-UHFFFAOYSA-N 0.000 abstract 6
- XEEYBQQBJWHFJM-UHFFFAOYSA-N Iron Chemical compound [Fe] XEEYBQQBJWHFJM-UHFFFAOYSA-N 0.000 abstract 4
- QAOWNCQODCNURD-UHFFFAOYSA-N Sulfuric acid Chemical compound OS(O)(=O)=O QAOWNCQODCNURD-UHFFFAOYSA-N 0.000 abstract 4
- HEMHJVSKTPXQMS-UHFFFAOYSA-M Sodium hydroxide Chemical compound [OH-].[Na+] HEMHJVSKTPXQMS-UHFFFAOYSA-M 0.000 abstract 3
- SEGLCEQVOFDUPX-UHFFFAOYSA-N di-(2-ethylhexyl)phosphoric acid Chemical compound CCCCC(CC)COP(O)(=O)OCC(CC)CCCC SEGLCEQVOFDUPX-UHFFFAOYSA-N 0.000 abstract 2
- 238000000605 extraction Methods 0.000 abstract 2
- 229910052742 iron Inorganic materials 0.000 abstract 2
- STCOOQWBFONSKY-UHFFFAOYSA-N tributyl phosphate Chemical compound CCCCOP(=O)(OCCCC)OCCCC STCOOQWBFONSKY-UHFFFAOYSA-N 0.000 abstract 2
- BVKZGUZCCUSVTD-UHFFFAOYSA-L Carbonate Chemical compound [O-]C([O-])=O BVKZGUZCCUSVTD-UHFFFAOYSA-L 0.000 abstract 1
- DGAQECJNVWCQMB-PUAWFVPOSA-M Ilexoside XXIX Chemical compound C[C@@H]1CC[C@@]2(CC[C@@]3(C(=CC[C@H]4[C@]3(CC[C@@H]5[C@@]4(CC[C@@H](C5(C)C)OS(=O)(=O)[O-])C)C)[C@@H]2[C@]1(C)O)C)C(=O)O[C@H]6[C@@H]([C@H]([C@@H]([C@H](O6)CO)O)O)O.[Na+] DGAQECJNVWCQMB-PUAWFVPOSA-M 0.000 abstract 1
- 239000002253 acid Substances 0.000 abstract 1
- 239000003513 alkali Substances 0.000 abstract 1
- ZAASRHQPRFFWCS-UHFFFAOYSA-P diazanium;oxygen(2-);uranium Chemical compound [NH4+].[NH4+].[O-2].[O-2].[O-2].[O-2].[O-2].[O-2].[O-2].[U].[U] ZAASRHQPRFFWCS-UHFFFAOYSA-P 0.000 abstract 1
- 239000003337 fertilizer Substances 0.000 abstract 1
- 239000003350 kerosene Substances 0.000 abstract 1
- 239000002244 precipitate Substances 0.000 abstract 1
- 230000001376 precipitating effect Effects 0.000 abstract 1
- 238000011084 recovery Methods 0.000 abstract 1
- 229910052708 sodium Inorganic materials 0.000 abstract 1
- 239000011734 sodium Substances 0.000 abstract 1
- 230000002195 synergetic effect Effects 0.000 abstract 1
- -1 uranium peroxide Chemical class 0.000 abstract 1
- XLYOFNOQVPJJNP-UHFFFAOYSA-N water Substances O XLYOFNOQVPJJNP-UHFFFAOYSA-N 0.000 abstract 1
Classifications
-
- C—CHEMISTRY; METALLURGY
- C22—METALLURGY; FERROUS OR NON-FERROUS ALLOYS; TREATMENT OF ALLOYS OR NON-FERROUS METALS
- C22B—PRODUCTION AND REFINING OF METALS; PRETREATMENT OF RAW MATERIALS
- C22B60/00—Obtaining metals of atomic number 87 or higher, i.e. radioactive metals
- C22B60/02—Obtaining thorium, uranium, or other actinides
- C22B60/0204—Obtaining thorium, uranium, or other actinides obtaining uranium
- C22B60/0217—Obtaining thorium, uranium, or other actinides obtaining uranium by wet processes
- C22B60/0252—Obtaining thorium, uranium, or other actinides obtaining uranium by wet processes treatment or purification of solutions or of liquors or of slurries
- C22B60/026—Obtaining thorium, uranium, or other actinides obtaining uranium by wet processes treatment or purification of solutions or of liquors or of slurries liquid-liquid extraction with or without dissolution in organic solvents
-
- C—CHEMISTRY; METALLURGY
- C22—METALLURGY; FERROUS OR NON-FERROUS ALLOYS; TREATMENT OF ALLOYS OR NON-FERROUS METALS
- C22B—PRODUCTION AND REFINING OF METALS; PRETREATMENT OF RAW MATERIALS
- C22B3/00—Extraction of metal compounds from ores or concentrates by wet processes
- C22B3/20—Treatment or purification of solutions, e.g. obtained by leaching
- C22B3/26—Treatment or purification of solutions, e.g. obtained by leaching by liquid-liquid extraction using organic compounds
- C22B3/38—Treatment or purification of solutions, e.g. obtained by leaching by liquid-liquid extraction using organic compounds containing phosphorus
- C22B3/384—Pentavalent phosphorus oxyacids, esters thereof
- C22B3/3846—Phosphoric acid, e.g. (O)P(OH)3
-
- C—CHEMISTRY; METALLURGY
- C22—METALLURGY; FERROUS OR NON-FERROUS ALLOYS; TREATMENT OF ALLOYS OR NON-FERROUS METALS
- C22B—PRODUCTION AND REFINING OF METALS; PRETREATMENT OF RAW MATERIALS
- C22B60/00—Obtaining metals of atomic number 87 or higher, i.e. radioactive metals
- C22B60/02—Obtaining thorium, uranium, or other actinides
- C22B60/0204—Obtaining thorium, uranium, or other actinides obtaining uranium
- C22B60/0217—Obtaining thorium, uranium, or other actinides obtaining uranium by wet processes
- C22B60/0221—Obtaining thorium, uranium, or other actinides obtaining uranium by wet processes by leaching
- C22B60/0226—Obtaining thorium, uranium, or other actinides obtaining uranium by wet processes by leaching using acidic solutions or liquors
- C22B60/0243—Obtaining thorium, uranium, or other actinides obtaining uranium by wet processes by leaching using acidic solutions or liquors phosphorated ion as active agent
-
- C—CHEMISTRY; METALLURGY
- C22—METALLURGY; FERROUS OR NON-FERROUS ALLOYS; TREATMENT OF ALLOYS OR NON-FERROUS METALS
- C22B—PRODUCTION AND REFINING OF METALS; PRETREATMENT OF RAW MATERIALS
- C22B60/00—Obtaining metals of atomic number 87 or higher, i.e. radioactive metals
- C22B60/02—Obtaining thorium, uranium, or other actinides
- C22B60/0204—Obtaining thorium, uranium, or other actinides obtaining uranium
- C22B60/0217—Obtaining thorium, uranium, or other actinides obtaining uranium by wet processes
- C22B60/0252—Obtaining thorium, uranium, or other actinides obtaining uranium by wet processes treatment or purification of solutions or of liquors or of slurries
- C22B60/0278—Obtaining thorium, uranium, or other actinides obtaining uranium by wet processes treatment or purification of solutions or of liquors or of slurries by chemical methods
- C22B60/0282—Solutions containing P ions, e.g. treatment of solutions resulting from the leaching of phosphate ores or recovery of uranium from wet-process phosphoric acid
-
- Y—GENERAL TAGGING OF NEW TECHNOLOGICAL DEVELOPMENTS; GENERAL TAGGING OF CROSS-SECTIONAL TECHNOLOGIES SPANNING OVER SEVERAL SECTIONS OF THE IPC; TECHNICAL SUBJECTS COVERED BY FORMER USPC CROSS-REFERENCE ART COLLECTIONS [XRACs] AND DIGESTS
- Y02—TECHNOLOGIES OR APPLICATIONS FOR MITIGATION OR ADAPTATION AGAINST CLIMATE CHANGE
- Y02P—CLIMATE CHANGE MITIGATION TECHNOLOGIES IN THE PRODUCTION OR PROCESSING OF GOODS
- Y02P10/00—Technologies related to metal processing
- Y02P10/20—Recycling
Landscapes
- Engineering & Computer Science (AREA)
- Chemical & Material Sciences (AREA)
- Life Sciences & Earth Sciences (AREA)
- General Life Sciences & Earth Sciences (AREA)
- Materials Engineering (AREA)
- Geology (AREA)
- Manufacturing & Machinery (AREA)
- Environmental & Geological Engineering (AREA)
- Mechanical Engineering (AREA)
- Metallurgy (AREA)
- Organic Chemistry (AREA)
- Geochemistry & Mineralogy (AREA)
- Manufacture And Refinement Of Metals (AREA)
- Extraction Or Liquid Replacement (AREA)
- Solid-Sorbent Or Filter-Aiding Compositions (AREA)
- Fertilizers (AREA)
- Inorganic Compounds Of Heavy Metals (AREA)
Applications Claiming Priority (1)
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| PCT/IN2003/000132 WO2004087971A1 (en) | 2003-03-31 | 2003-03-31 | A process for recovery of high purity uranium from fertilizer grade weak phosphoric acid |
Publications (2)
| Publication Number | Publication Date |
|---|---|
| DE60304330D1 true DE60304330D1 (de) | 2006-05-18 |
| DE60304330T2 DE60304330T2 (de) | 2006-11-30 |
Family
ID=33104981
Family Applications (1)
| Application Number | Title | Priority Date | Filing Date |
|---|---|---|---|
| DE60304330T Expired - Lifetime DE60304330T2 (de) | 2003-03-31 | 2003-03-31 | Verfahren zur gewinnung von hochreinem uran aus schwacher düngemittelgradiger phosphorsäure |
Country Status (7)
| Country | Link |
|---|---|
| US (1) | US7192563B2 (de) |
| EP (1) | EP1511869B9 (de) |
| AT (1) | ATE321896T1 (de) |
| AU (1) | AU2003238666A1 (de) |
| DE (1) | DE60304330T2 (de) |
| ES (1) | ES2261944T3 (de) |
| WO (1) | WO2004087971A1 (de) |
Families Citing this family (14)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN100400687C (zh) * | 2006-10-30 | 2008-07-09 | 北京斯帕顿矿产资源投资咨询有限公司 | 从磷酸盐中提取放射性铀的方法 |
| CN100387734C (zh) * | 2006-10-30 | 2008-05-14 | 北京斯帕顿矿产资源投资咨询有限公司 | 从粉煤灰中提取放射性铀的方法 |
| AU2007363064B2 (en) | 2007-12-26 | 2014-02-13 | Thorium Power Inc. | Nuclear reactor (variants), fuel assembly consisting of driver-breeding modules for a nuclear reactor (variants) and a fuel cell for a fuel assembly |
| US8116423B2 (en) | 2007-12-26 | 2012-02-14 | Thorium Power, Inc. | Nuclear reactor (alternatives), fuel assembly of seed-blanket subassemblies for nuclear reactor (alternatives), and fuel element for fuel assembly |
| CA2946210C (en) | 2008-12-25 | 2019-02-12 | Thorium Power, Inc. | A light-water reactor fuel assembly and fuel element thereof |
| CA2784292C (en) * | 2009-12-15 | 2018-05-29 | Cytec Technology Corp. | Methods and compositions for the removal of impurities from an impurity-loaded ionic liquid |
| FI122274B (fi) * | 2010-02-02 | 2011-11-15 | Outotec Oyj | Uuttoprosessi |
| WO2011143172A1 (en) | 2010-05-11 | 2011-11-17 | Thorium Power, Inc. | Fuel assembly with metal fuel alloy kernel and method of manufacturing thereof |
| US10192644B2 (en) | 2010-05-11 | 2019-01-29 | Lightbridge Corporation | Fuel assembly |
| US10170207B2 (en) | 2013-05-10 | 2019-01-01 | Thorium Power, Inc. | Fuel assembly |
| CN106636690B (zh) * | 2016-12-07 | 2018-05-18 | 中核四0四有限公司 | 一种酸性含硝酸铵含铀废水中铀的回收方法 |
| CN115948665B (zh) * | 2021-10-08 | 2024-10-18 | 中核矿业科技集团有限公司 | 一种高稳定性的铀纯化萃取方法 |
| CN114686688A (zh) * | 2021-10-25 | 2022-07-01 | 核工业北京化工冶金研究院 | 一种萃取法深度除铀方法 |
| CN115849451A (zh) * | 2022-11-11 | 2023-03-28 | 中核四0四有限公司 | 一种含铀废液的回收处理方法 |
Family Cites Families (4)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| FR2352062A1 (fr) | 1976-05-19 | 1977-12-16 | Minemet Rech Sa | Procede pour l'extraction de l'uranium contenu dans les minerais phosphates. |
| US4258013A (en) * | 1977-09-14 | 1981-03-24 | Earth Sciences Inc. | Uranium recovery from wet process phosphoric acid |
| US4302427A (en) * | 1979-03-19 | 1981-11-24 | International Minerals & Chemical Corporation | Recovery of uranium from wet-process phosphoric acid |
| US4649029A (en) * | 1984-04-13 | 1987-03-10 | Inderjit Nirdosh | Processes for extraction of uranium and radium from uranium-containing ores using ferric nitrate |
-
2002
- 2002-03-31 US US10/486,507 patent/US7192563B2/en not_active Expired - Fee Related
-
2003
- 2003-03-31 ES ES03733002T patent/ES2261944T3/es not_active Expired - Lifetime
- 2003-03-31 DE DE60304330T patent/DE60304330T2/de not_active Expired - Lifetime
- 2003-03-31 AU AU2003238666A patent/AU2003238666A1/en not_active Abandoned
- 2003-03-31 EP EP03733002A patent/EP1511869B9/de not_active Expired - Lifetime
- 2003-03-31 AT AT03733002T patent/ATE321896T1/de not_active IP Right Cessation
- 2003-03-31 WO PCT/IN2003/000132 patent/WO2004087971A1/en not_active Application Discontinuation
Also Published As
| Publication number | Publication date |
|---|---|
| US7192563B2 (en) | 2007-03-20 |
| DE60304330T2 (de) | 2006-11-30 |
| EP1511869B1 (de) | 2006-03-29 |
| WO2004087971A1 (en) | 2004-10-14 |
| US20040247504A1 (en) | 2004-12-09 |
| EP1511869B9 (de) | 2006-10-11 |
| AU2003238666A1 (en) | 2004-10-25 |
| ES2261944T3 (es) | 2006-11-16 |
| ATE321896T1 (de) | 2006-04-15 |
| EP1511869A1 (de) | 2005-03-09 |
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Legal Events
| Date | Code | Title | Description |
|---|---|---|---|
| 8364 | No opposition during term of opposition |