DE438670C - Process for the production of a highly active carbon - Google Patents
Process for the production of a highly active carbonInfo
- Publication number
- DE438670C DE438670C DEA39534D DEA0039534D DE438670C DE 438670 C DE438670 C DE 438670C DE A39534 D DEA39534 D DE A39534D DE A0039534 D DEA0039534 D DE A0039534D DE 438670 C DE438670 C DE 438670C
- Authority
- DE
- Germany
- Prior art keywords
- production
- active carbon
- highly active
- wood
- bisulfate
- Prior art date
- Legal status (The legal status is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the status listed.)
- Expired
Links
Classifications
-
- C—CHEMISTRY; METALLURGY
- C01—INORGANIC CHEMISTRY
- C01B—NON-METALLIC ELEMENTS; COMPOUNDS THEREOF; METALLOIDS OR COMPOUNDS THEREOF NOT COVERED BY SUBCLASS C01C
- C01B32/00—Carbon; Compounds thereof
- C01B32/30—Active carbon
- C01B32/312—Preparation
- C01B32/342—Preparation characterised by non-gaseous activating agents
Landscapes
- Chemical & Material Sciences (AREA)
- Organic Chemistry (AREA)
- Inorganic Chemistry (AREA)
- Carbon And Carbon Compounds (AREA)
- Solid-Sorbent Or Filter-Aiding Compositions (AREA)
Description
Verfahren zur Herstellung einer hochaktiven Kohle. Es ist bekannt, eine Entfärbungskohle dadurch herzustellen, daß man mit Natriumbisulfat versetztes Holz oder ähnliche Stoffe nach längerem Stehenlassen trocknet, an der Luft auf 3oo bis 5oo° erhitzt, mit Wasser zwecks Herauslösens des Bisulfats kocht, filtriert und schließlich bei 8oo bis rooo° unter Luftabschluß glüht (amerikanisches Patent i383755)- Die Wirksamkeit einer derart hergestellten Kohle ist aber recht schlecht.Process for the production of a high-active carbon. It is known, to produce a decolorizing carbon by adding sodium bisulfate Wood or similar material dries after standing for a long time, in the open air to 300 Heated to 500 °, boiled with water to dissolve the bisulfate, filtered and finally glows at 8oo to rooo ° in the absence of air (American patent i383755) - The effectiveness of charcoal produced in this way is, however, very poor.
Es wurde nun die überraschende Beobachtung gemacht, daß man eine hervorragend aktive Kohle - und zwar in einem Arbeitsgang -- erhält, wenn man Holz oder andere cellulosehaltige Stoffe mit Bisulfat imprägniert, auf Temperaturen oberhalb 5oo° erhitzt und alsdann auslaugt. Hierbei erhält man nebenbei noch eine Lösung von Schwefelnatrium, aus der in bekannter Weise das feste Produkt erhalten werde« kann. Der Vorteil des neuen Verfahrens bestellt in der einfacheren Herstellungsweise, dem Erhalt eines wertollen Nebenproduktes und besonders in der Gewinnung einer hervorragend aktiven Kohle. -Beispiel. Zerkleinertes Kiefernholz wird getränkt mit konzentrierter Natriumbisulfatlauge, getrocknet und vorteilhaft bei Luftabschluß bei 6oo bis rooo° etwa z Stunden geglüht. Nach dem Erkalten wird die Kohle mit Wasser ausgelaugt. Beim Verdampfen :ler Lange bleibt sehr hochwertiges Schwefelnatrium als Rückstand. Die Kohle kann entweder direkt oder nach Auswaschen mit Salzsäure getrocknet werden. Sie zeigt ein hervorragendes Absorptions- und Entfärbungsvermögen.The surprising observation has now been made that one is excellent active charcoal - in one operation - is obtained when wood or something else is used cellulose-containing substances impregnated with bisulphate, to temperatures above 500 ° heated and then leached. Here you also get a solution of sodium sulphide, from which the solid product can be obtained in a known manner. The advantage of the new process ordered in the simpler production method, the receipt of a valuable by-product and especially in the extraction of an excellently active one Money. -Example. Crushed pine wood is soaked with concentrated sodium bisulphate lye, dried and advantageously calcined with the exclusion of air at 600 to rooo ° for about z hours. After cooling, the coal is leached with water. When evaporating: longer very high quality sodium sulphide remains as a residue. The coal can either dried directly or after washing with hydrochloric acid. She shows an excellent Absorbance and discoloration capacity.
Claims (1)
Priority Applications (1)
Application Number | Priority Date | Filing Date | Title |
---|---|---|---|
DEA39534D DE438670C (en) | 1923-03-04 | 1923-03-04 | Process for the production of a highly active carbon |
Applications Claiming Priority (1)
Application Number | Priority Date | Filing Date | Title |
---|---|---|---|
DEA39534D DE438670C (en) | 1923-03-04 | 1923-03-04 | Process for the production of a highly active carbon |
Publications (1)
Publication Number | Publication Date |
---|---|
DE438670C true DE438670C (en) | 1926-12-24 |
Family
ID=6931414
Family Applications (1)
Application Number | Title | Priority Date | Filing Date |
---|---|---|---|
DEA39534D Expired DE438670C (en) | 1923-03-04 | 1923-03-04 | Process for the production of a highly active carbon |
Country Status (1)
Country | Link |
---|---|
DE (1) | DE438670C (en) |
-
1923
- 1923-03-04 DE DEA39534D patent/DE438670C/en not_active Expired
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