DE2301735A1 - Verfahren zur herstellung von 1-nitroanthrachinon - Google Patents
Verfahren zur herstellung von 1-nitroanthrachinonInfo
- Publication number
- DE2301735A1 DE2301735A1 DE2301735A DE2301735A DE2301735A1 DE 2301735 A1 DE2301735 A1 DE 2301735A1 DE 2301735 A DE2301735 A DE 2301735A DE 2301735 A DE2301735 A DE 2301735A DE 2301735 A1 DE2301735 A1 DE 2301735A1
- Authority
- DE
- Germany
- Prior art keywords
- nitric acid
- anthraquinone
- mole fraction
- reaction
- nitro
- Prior art date
- Legal status (The legal status is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the status listed.)
- Withdrawn
Links
- YCANAXVBJKNANM-UHFFFAOYSA-N 1-nitroanthracene-9,10-dione Chemical compound O=C1C2=CC=CC=C2C(=O)C2=C1C=CC=C2[N+](=O)[O-] YCANAXVBJKNANM-UHFFFAOYSA-N 0.000 title claims description 33
- 238000000034 method Methods 0.000 title claims description 24
- GRYLNZFGIOXLOG-UHFFFAOYSA-N Nitric acid Chemical compound O[N+]([O-])=O GRYLNZFGIOXLOG-UHFFFAOYSA-N 0.000 claims description 102
- 229910017604 nitric acid Inorganic materials 0.000 claims description 102
- 150000004056 anthraquinones Chemical class 0.000 claims description 33
- PYKYMHQGRFAEBM-UHFFFAOYSA-N anthraquinone Natural products CCC(=O)c1c(O)c2C(=O)C3C(C=CC=C3O)C(=O)c2cc1CC(=O)OC PYKYMHQGRFAEBM-UHFFFAOYSA-N 0.000 claims description 32
- 238000006243 chemical reaction Methods 0.000 claims description 30
- XLYOFNOQVPJJNP-UHFFFAOYSA-N water Substances O XLYOFNOQVPJJNP-UHFFFAOYSA-N 0.000 claims description 30
- 238000006396 nitration reaction Methods 0.000 claims description 14
- 239000011541 reaction mixture Substances 0.000 claims description 12
- 238000001556 precipitation Methods 0.000 claims description 7
- 239000002244 precipitate Substances 0.000 claims description 5
- 238000002360 preparation method Methods 0.000 claims description 4
- 239000000203 mixture Substances 0.000 description 16
- 239000000047 product Substances 0.000 description 14
- 238000001816 cooling Methods 0.000 description 9
- 239000006227 byproduct Substances 0.000 description 7
- 239000000706 filtrate Substances 0.000 description 7
- 238000007865 diluting Methods 0.000 description 4
- 238000010583 slow cooling Methods 0.000 description 4
- 239000003085 diluting agent Substances 0.000 description 3
- 239000002253 acid Substances 0.000 description 2
- 230000015572 biosynthetic process Effects 0.000 description 2
- 238000005119 centrifugation Methods 0.000 description 2
- 238000004140 cleaning Methods 0.000 description 2
- 238000001035 drying Methods 0.000 description 2
- 238000010438 heat treatment Methods 0.000 description 2
- 239000012452 mother liquor Substances 0.000 description 2
- 238000005406 washing Methods 0.000 description 2
- 238000010626 work up procedure Methods 0.000 description 2
- QCVMOSGPTRRUQZ-UHFFFAOYSA-N 2-nitroanthracene-9,10-dione Chemical compound C1=CC=C2C(=O)C3=CC([N+](=O)[O-])=CC=C3C(=O)C2=C1 QCVMOSGPTRRUQZ-UHFFFAOYSA-N 0.000 description 1
- ZXVONLUNISGICL-UHFFFAOYSA-N 4,6-dinitro-o-cresol Chemical group CC1=CC([N+]([O-])=O)=CC([N+]([O-])=O)=C1O ZXVONLUNISGICL-UHFFFAOYSA-N 0.000 description 1
- KADDEZWVEAQOCJ-UHFFFAOYSA-N anthracene-9,10-dione;nitric acid Chemical compound O[N+]([O-])=O.C1=CC=C2C(=O)C3=CC=CC=C3C(=O)C2=C1 KADDEZWVEAQOCJ-UHFFFAOYSA-N 0.000 description 1
- 239000000470 constituent Substances 0.000 description 1
- 238000002425 crystallisation Methods 0.000 description 1
- 230000008025 crystallization Effects 0.000 description 1
- 230000003247 decreasing effect Effects 0.000 description 1
- 238000010790 dilution Methods 0.000 description 1
- 239000012895 dilution Substances 0.000 description 1
- 238000004821 distillation Methods 0.000 description 1
- 230000002349 favourable effect Effects 0.000 description 1
- 238000001914 filtration Methods 0.000 description 1
- 238000002156 mixing Methods 0.000 description 1
- 230000007935 neutral effect Effects 0.000 description 1
- 150000002823 nitrates Chemical class 0.000 description 1
- 238000005121 nitriding Methods 0.000 description 1
- 238000000746 purification Methods 0.000 description 1
- 238000011084 recovery Methods 0.000 description 1
- 238000005057 refrigeration Methods 0.000 description 1
- 239000000243 solution Substances 0.000 description 1
- 238000001228 spectrum Methods 0.000 description 1
- 238000003756 stirring Methods 0.000 description 1
- 239000010409 thin film Substances 0.000 description 1
Classifications
-
- C—CHEMISTRY; METALLURGY
- C05—FERTILISERS; MANUFACTURE THEREOF
- C05G—MIXTURES OF FERTILISERS COVERED INDIVIDUALLY BY DIFFERENT SUBCLASSES OF CLASS C05; MIXTURES OF ONE OR MORE FERTILISERS WITH MATERIALS NOT HAVING A SPECIFIC FERTILISING ACTIVITY, e.g. PESTICIDES, SOIL-CONDITIONERS, WETTING AGENTS; FERTILISERS CHARACTERISED BY THEIR FORM
- C05G3/00—Mixtures of one or more fertilisers with additives not having a specially fertilising activity
- C05G3/60—Biocides or preservatives, e.g. disinfectants, pesticides or herbicides; Pest repellants or attractants
Landscapes
- Life Sciences & Earth Sciences (AREA)
- Pest Control & Pesticides (AREA)
- Plant Pathology (AREA)
- Chemical & Material Sciences (AREA)
- Organic Chemistry (AREA)
- Organic Low-Molecular-Weight Compounds And Preparation Thereof (AREA)
Priority Applications (13)
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| DE2301735A DE2301735A1 (de) | 1973-01-13 | 1973-01-13 | Verfahren zur herstellung von 1-nitroanthrachinon |
| NL7400354A NL7400354A (xx) | 1973-01-13 | 1974-01-10 | |
| LU69139A LU69139A1 (xx) | 1973-01-13 | 1974-01-10 | |
| BR173/74A BR7400173D0 (pt) | 1973-01-13 | 1974-01-11 | Processo para a preparacao de 1-nitro-antraquinona |
| DD175964A DD111070A5 (xx) | 1973-01-13 | 1974-01-11 | |
| AT23374*#A AT329043B (de) | 1973-01-13 | 1974-01-11 | Verfahren zur herstellung von 1-nitro-antrachinon |
| GB137474A GB1427884A (en) | 1973-01-13 | 1974-01-11 | Process for the preparation of 1-nitroanthraquinone |
| BE139719A BE809639A (fr) | 1973-01-13 | 1974-01-11 | Procede de production de la 1-nitro-anthraquinone |
| FR7400967A FR2213931B1 (xx) | 1973-01-13 | 1974-01-11 | |
| CH39274A CH595317A5 (xx) | 1973-01-13 | 1974-01-11 | |
| IT19343/74A IT1006889B (it) | 1973-01-13 | 1974-01-11 | Processo per la produzione di i nitro antrachinone |
| JP608674A JPS55372B2 (xx) | 1973-01-13 | 1974-01-11 | |
| US05/594,254 US3959317A (en) | 1973-01-13 | 1975-07-09 | Process for the preparation of 1-nitroanthraquinone |
Applications Claiming Priority (1)
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| DE2301735A DE2301735A1 (de) | 1973-01-13 | 1973-01-13 | Verfahren zur herstellung von 1-nitroanthrachinon |
Publications (1)
| Publication Number | Publication Date |
|---|---|
| DE2301735A1 true DE2301735A1 (de) | 1974-08-08 |
Family
ID=5868989
Family Applications (1)
| Application Number | Title | Priority Date | Filing Date |
|---|---|---|---|
| DE2301735A Withdrawn DE2301735A1 (de) | 1973-01-13 | 1973-01-13 | Verfahren zur herstellung von 1-nitroanthrachinon |
Country Status (12)
| Country | Link |
|---|---|
| JP (1) | JPS55372B2 (xx) |
| AT (1) | AT329043B (xx) |
| BE (1) | BE809639A (xx) |
| BR (1) | BR7400173D0 (xx) |
| CH (1) | CH595317A5 (xx) |
| DD (1) | DD111070A5 (xx) |
| DE (1) | DE2301735A1 (xx) |
| FR (1) | FR2213931B1 (xx) |
| GB (1) | GB1427884A (xx) |
| IT (1) | IT1006889B (xx) |
| LU (1) | LU69139A1 (xx) |
| NL (1) | NL7400354A (xx) |
Families Citing this family (1)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| JPH0519163U (ja) * | 1991-08-29 | 1993-03-09 | 昭和アルミニウム株式会社 | 加熱殺菌用食品容器 |
Family Cites Families (1)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| US2874168A (en) * | 1957-04-02 | 1959-02-17 | Gen Aniline & Film Corp | Process for the preparation of 1-nitroanthraquinone |
-
1973
- 1973-01-13 DE DE2301735A patent/DE2301735A1/de not_active Withdrawn
-
1974
- 1974-01-10 NL NL7400354A patent/NL7400354A/xx unknown
- 1974-01-10 LU LU69139A patent/LU69139A1/xx unknown
- 1974-01-11 CH CH39274A patent/CH595317A5/xx not_active IP Right Cessation
- 1974-01-11 FR FR7400967A patent/FR2213931B1/fr not_active Expired
- 1974-01-11 BR BR173/74A patent/BR7400173D0/pt unknown
- 1974-01-11 GB GB137474A patent/GB1427884A/en not_active Expired
- 1974-01-11 JP JP608674A patent/JPS55372B2/ja not_active Expired
- 1974-01-11 DD DD175964A patent/DD111070A5/xx unknown
- 1974-01-11 AT AT23374*#A patent/AT329043B/de not_active IP Right Cessation
- 1974-01-11 BE BE139719A patent/BE809639A/xx unknown
- 1974-01-11 IT IT19343/74A patent/IT1006889B/it active
Also Published As
| Publication number | Publication date |
|---|---|
| BR7400173D0 (pt) | 1974-08-15 |
| IT1006889B (it) | 1976-10-20 |
| NL7400354A (xx) | 1974-07-16 |
| LU69139A1 (xx) | 1974-08-19 |
| ATA23374A (de) | 1975-07-15 |
| AT329043B (de) | 1976-04-26 |
| JPS4995953A (xx) | 1974-09-11 |
| FR2213931A1 (xx) | 1974-08-09 |
| BE809639A (fr) | 1974-07-11 |
| DD111070A5 (xx) | 1975-01-20 |
| JPS55372B2 (xx) | 1980-01-08 |
| FR2213931B1 (xx) | 1977-08-26 |
| GB1427884A (en) | 1976-03-10 |
| CH595317A5 (xx) | 1978-02-15 |
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Legal Events
| Date | Code | Title | Description |
|---|---|---|---|
| 8130 | Withdrawal |