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CN87100319A - Plant leaf fertilizer and preparation method thereof - Google Patents

Plant leaf fertilizer and preparation method thereof Download PDF

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Publication number
CN87100319A
CN87100319A CN87100319A CN87100319A CN87100319A CN 87100319 A CN87100319 A CN 87100319A CN 87100319 A CN87100319 A CN 87100319A CN 87100319 A CN87100319 A CN 87100319A CN 87100319 A CN87100319 A CN 87100319A
Authority
CN
China
Prior art keywords
whey
starch
fertilizer
dispersion medium
suspension
Prior art date
Legal status (The legal status is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the status listed.)
Pending
Application number
CN87100319A
Other languages
Chinese (zh)
Inventor
科斯塔丁·科斯塔迪诺·科斯塔迪诺夫
阿纳·帕夫洛瓦·帕夫洛瓦
帕维尔·萨哈里夫·巴克瓦罗夫
埃夫吉尼·斯塔奇夫·依瓦尼奇科夫
普拉门·依瓦诺夫·特里福诺夫
Current Assignee (The listed assignees may be inaccurate. Google has not performed a legal analysis and makes no representation or warranty as to the accuracy of the list.)
Ivsd "avangard" (bg) Sofia Bulgaria
Original Assignee
Ivsd "avangard" (bg) Sofia Bulgaria
Priority date (The priority date is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the date listed.)
Filing date
Publication date
Application filed by Ivsd "avangard" (bg) Sofia Bulgaria filed Critical Ivsd "avangard" (bg) Sofia Bulgaria
Publication of CN87100319A publication Critical patent/CN87100319A/en
Pending legal-status Critical Current

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Classifications

    • CCHEMISTRY; METALLURGY
    • C05FERTILISERS; MANUFACTURE THEREOF
    • C05FORGANIC FERTILISERS NOT COVERED BY SUBCLASSES C05B, C05C, e.g. FERTILISERS FROM WASTE OR REFUSE
    • C05F1/00Fertilisers made from animal corpses, or parts thereof
    • C05F1/005Fertilisers made from animal corpses, or parts thereof from meat-wastes or from other wastes of animal origin, e.g. skins, hair, hoofs, feathers, blood
    • YGENERAL TAGGING OF NEW TECHNOLOGICAL DEVELOPMENTS; GENERAL TAGGING OF CROSS-SECTIONAL TECHNOLOGIES SPANNING OVER SEVERAL SECTIONS OF THE IPC; TECHNICAL SUBJECTS COVERED BY FORMER USPC CROSS-REFERENCE ART COLLECTIONS [XRACs] AND DIGESTS
    • Y02TECHNOLOGIES OR APPLICATIONS FOR MITIGATION OR ADAPTATION AGAINST CLIMATE CHANGE
    • Y02ATECHNOLOGIES FOR ADAPTATION TO CLIMATE CHANGE
    • Y02A40/00Adaptation technologies in agriculture, forestry, livestock or agroalimentary production
    • Y02A40/10Adaptation technologies in agriculture, forestry, livestock or agroalimentary production in agriculture
    • Y02A40/20Fertilizers of biological origin, e.g. guano or fertilizers made from animal corpses
    • YGENERAL TAGGING OF NEW TECHNOLOGICAL DEVELOPMENTS; GENERAL TAGGING OF CROSS-SECTIONAL TECHNOLOGIES SPANNING OVER SEVERAL SECTIONS OF THE IPC; TECHNICAL SUBJECTS COVERED BY FORMER USPC CROSS-REFERENCE ART COLLECTIONS [XRACs] AND DIGESTS
    • Y02TECHNOLOGIES OR APPLICATIONS FOR MITIGATION OR ADAPTATION AGAINST CLIMATE CHANGE
    • Y02PCLIMATE CHANGE MITIGATION TECHNOLOGIES IN THE PRODUCTION OR PROCESSING OF GOODS
    • Y02P20/00Technologies relating to chemical industry
    • Y02P20/141Feedstock
    • Y02P20/145Feedstock the feedstock being materials of biological origin

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  • Engineering & Computer Science (AREA)
  • Environmental & Geological Engineering (AREA)
  • Chemical & Material Sciences (AREA)
  • Organic Chemistry (AREA)
  • Fertilizers (AREA)
  • Coloring Foods And Improving Nutritive Qualities (AREA)
  • Fodder In General (AREA)
  • Medicines That Contain Protein Lipid Enzymes And Other Medicines (AREA)

Abstract

The plant leaf fertilizer is a suspended fertilizer containing a large amount of trace elements, the liquid phase of the fertilizer is concentrated whey containing 2-4% of protein hydrolysate (amino acid), and the preparation method comprises the following steps: dissolving inorganic salt in a dispersion medium containing fermented whey and a concentrated protein hydrolysate solution at 60-80 deg.C, adding the concentrate of trace elements and the starch suspension to the dispersion medium, and cooling the resulting solution to 20-25 deg.C in 2-15 min. The sequence of adding the inorganic salt is as follows: potassium nitrate, ammonium phosphate, urea and ammonium saltpeter. The starch is dissolved in concentrated whey to obtain a starch suspension. The starch content in the final product is 2.5-4%. The plant leaf fertilizer can be applied to agriculture.

Description

Means for leaf feeding of plants and preparation method thereof
The present invention relates to a kind of means for leaf feeding of plants that is used for agricultural and preparation method thereof.
The leaf fertilizer of known plants contains a large amount of and micronutrient element, and its content is: nitrogen 25%, phosphorus 6%, potassium 10%, iron 0.1%, boron 200mg/kg, manganese 500mg/kg, copper 500mg/kg, zinc 500mg/kg, molybdenum 5mg/kg and cobalt 5mg/kg(1).
The shortcoming of this fertilizer is that its protein accumulation of using plant and cereal does not produce direct effect.
Known have a kind of method and apparatus for preparing this suspension fertilizer, and wherein macroelement and trace element (salt) are mixed together with water and other additive, grind (2) under the state of cooling in the mixing tank of using mutually.
It is to rest at it to form crystallization-mainly from making the rotten complete crystalline saltpetre of suspension in suspension process that preparation has the shortcoming of method of the suspension leaf fertilizer of this salt composition.In order to suppress crystalline growth, add the material-filler and the stablizer of no physiologically active usually, make this higher concentration fertilizer of leaf confrontation dosed administration produce negative influence.In order to limit the highly crystalline of saltpetre, can add other sylvite, particularly measure up to 30% Repone K, obtain the potassium of aequum, the result makes the very deleterious chlorion of development of plants is present in the mixture.
The object of the present invention is to provide a kind of leaf fertilizer and a kind of preparation that improves plant organ output and protein content to have the method for the suspension leaf fertilizer of uniform microgranular texture.
Can reach this purpose with the suspension leaf fertilizer that contains macroelement and trace element, its liquid phase is for containing the dense whey of 2-4% proteolysate (amino acid); The method for preparing plant suspension leaf fertilizer is all the components of leaf fertilizer during heating is dissolved in the dispersion medium of dense whey and proteolysate solution.Make a kind of uniform microparticle suspending liquid after the mixture cooling that obtains like this, and do not change with the passing of time.
The advantage of leaf fertilizer of the present invention is it to be applied to leaf protein yield of plant and content are increased; The advantage for preparing the method for this leaf fertilizer is can obtain by heat treated the solvate of dispersion medium composition, after the cooling of the mixture that obtains like this, is formed on the micro-crystallization that retention period of preparation process can not grow.Another advantage of this method is can avoid the operant activity of high rotation or use high-pressure pump in heat-processed.
Example explanation the present invention with following composition:
1. proteolysate (amino acid)-2%.
2. the lactic acid solution of whey concentrates 3 times-25%.
Comprise in the lactic acid solution:
-lactic acid-10%;
-calcium-0.5% and manganese-0.1%;
-riboflavin-0.5mg/l; Xitix-3mg/l;
-VitB1-0.1mg/l;
3. macroelement: nitrogen-31.25%; Phosphorus-7.5%; Potassium-15%.
4. micro-: iron-400mg/l; Boron-312.5mg/l; Manganese-250mg/l; Copper-187.5mg/l; Zinc-125mg/l; Molybdenum-18.75mg/l; Cobalt-6.25mg/l.
The method for preparing this leaf fertilizer is implemented in a kind of device, and technical process comprises following each step:
1. the fermentation of waste liquid (whey).
2. by vacuum-evaporation the lactic acid solution of fermented whey is concentrated.
3. the enzymolysis of protein ingredient and by vacuum-evaporation protein concentrate hydrolyzate.
4. prepare suspension and precision work the finished product.
The first step in technological process, whey is kept by the quantitative adding of sylvite at 45 ℃ and pH5.0-5.2() condition bottom fermentation container in ferment, bacillus bulgaricus in the lactic acid can make the lactose in the whey transform whereby, and the trace element in this compound that is easily assimilated by plant for coupling is necessary.
Second step in technological process concentrates 3 times with the lactic acid solution of whey in vacuum-evaporator, be that the lactic acid content of 1-2% is increased to 10% thereby make lactic protein, and improves other composition of also containing in the whey-mainly be VITAMIN and salt.The strong solution that obtains like this is the essential part of the dispersion medium of the suspension produced.
In the 3rd step of technology, obtain the protein part (polypeptide of the necessary component of made fertilizer, peptide and amino acid) proteolysate, in a reactor vessel-hydrolyzer, the protein carrier of microorganism or proteolysate is subjected to enzymolysis, and the proteolysate that obtains like this concentrates 3-5 doubly in vacuum-evaporator, it is joined in the liquid medium of a certain amount of suspension then, and guaranteeing has 3% albumen existence.
In the 4th step process, be added to the liquid medium-dense whey and the proteolysate of fertilizer in the reactor with agitator with the amount that accounts for its volume 20%, it is heated to 75-80 ℃, add the trace element of the salt of different amounts from a storage blender loader (bin-dosator) then: saltpetre with the assurance necessary amount, ammonium phosphate, urea, ammonium saltpetre.After pressing the said sequence adding, till they dissolve fully.With said sequence add these salt be by its solubleness separately determine-solubleness of saltpetre is minimum, the solubleness of ammonium saltpetre is the highest.After this, add the salt that necessary amount iron and trace element are provided: ferric sulfate, boric acid, copper sulfate, zinc nitrate, ammonium molybdate, manganous nitrate, cobalt chloride.These salt are dissolved in the dense whey in advance through being heated to 75 ℃, then it are joined in above-mentioned total material, after this add the starch solution that is dissolved in advance in the dense whey again, and its amount accounts for the 2.5-3% of total material.
With the mixture homogenate that so obtains 30-40 minute, in cooling segment-a coil type crystallizer, be cooled to 20-25 ℃ then.Thereby obtain the suspension leaf fertilizer of purified fine particle.
Can understand the present invention better by the following examples
Embodiment 1:
" Sadovol " tests with wheat, and according to the suggestion of this area agrotechnique, wheat " Sadovol " is cultivated on the soil of elimination alluviation grass.Test area is 10 square metres, revision test 3 times.In two stages of development of plants, promptly handle plant at stem (handle) fringe formation phase and heading stage.The amount of spray solution is between 400ml/1000m 2To 800ml/1000m 2Between.
Embodiment 2:
With 25 liters in vacuum-evaporator, concentrate and the concentrated solution of the proteolysate that the wheys of fermentation and 5 liters obtain by enzymolysis to pour capacity into be in 300 liters the reactor that has agitator.Under constantly stirring,, add 48kg saltpetre (according to process explanation) then with mixture heating up to 70 ℃.In 1 hour, add nitrate.Begin to add ammonium phosphate-21kg then, also in 25-30 minute, add by part.Temperature with medium increases to 75-80 ℃ by heating with suitable device simultaneously.In 25-30 minute, add 50kg urea then.This is an endothermic process concerning ammonium saltpetre, temperature is reduced, but temperature should not be lower than 70 ℃.In the end a urea suspends 10-15 minute so that temperature rises to 75-80 ℃ after adding, and adds the 32.5kg ammonium saltpetre then in 20-25 minute.So the mixture that contains all macroelement that obtains is stirred 15-20 minute, and with 4 liters in advance the dense whey solution of salt such as the iron of (under 70-75 ℃) dissolving aequum and trace element join in this mixture.These trace elements are: boric acid-0.214kg, ammonium molybdate-0.108kg, cobalt chloride-0.003kg, copper sulfate 0.088kg and ferric sulfate-3750kg.(pass swap switch) stirs total material 15-20 minute under case without heating, enters cooling system then, drops to 20-25 ℃ through 10-15 minute its temperature.The suspension that will so obtain is processed into final product at last.
Further specify the present invention with tabulating down:
-table 1 is shown in the yield data that obtains in the field test;
-table 2 shows the protein content of wheat and the protein yield data in field test;
-table 3 is shown in the absolute magnitude and the hectolitre weight data of the wheat seed sample of producing in the field test.
Table 1: wheat yield
Different treatment 10m 2Mean value (kg)
1. contrast-water sprays 2.820
2.Vuksal-400ml/1000m 2Stem forms the phase 3.400
3 Vuksal-400+800ml/1000m 23.450
Stem formation+heading stage
4. leaf fertilizer-400ml/1000m of the present invention 2, stem forms the phase 3.500
5. leaf fertilizer-400+800ml/1000m of the present invention 23.680
Stem formation+heading stage
Annotate: these data are the mean value of three revision tests
Table 2, the protein content of the wheat under field condition and protein yield
Different treatment protein content (%) kg albumen/1000m in the table 1 2
1. contrast 13.05 36.8
2.Vuksal 12.86 43.7
3.Vuksal 12.82 44.2
4. leaf of the present invention fertile 13.50 47.2
5. leaf of the present invention fertile 13.31 48.9
Annotate: these data are the mean value of three revision tests.
Table 3, the absolute magnitude of wheat and hectolitre weight in field test
Different treatment absolute magnitude (g)/1000 in the table 1 a seed hectolitre weight (g/dm 3)
1. contrast 45.55 655
2.Vuksal 46.33 788
3.Vuksal 45.81 781
4. leaf of the present invention fertile 46.73 780
5. leaf of the present invention fertile 46.98 793
Annotate: these data are the mean value of three revision tests.

Claims (5)

1, contain the means for leaf feeding of plants of macroelement and trace element, liquid phase wherein is spissated whey, it is characterized in that it also contains the proteolysate of 2-4% (amino acid).
2, the method for the means for leaf feeding of plants of preparation suspension, it is characterized in that inorganic salt are dissolved in the dispersion medium of being made up of the concentrated solution of fermented whey and proteolysate, temperature is 60-85 ℃, enriched material and starch suspension with trace element joins in this dispersion medium then, at last this solution is delivered in the refrigerating unit, guaranteed that temperature dropped to 20-25 ℃ in 2-15 minute.
3, according to the method for claim 2, it is characterized in that inorganic components in the following order with saltpetre, ammonium phosphate, urea, ammonium saltpetre joins in the dispersion medium.
4, according to the method for claim 2, it is characterized in that the trace element concentrated solution be by under 70-80 ℃ temperature with following salt: boric acid, ammonium molybdate, zinc nitrate, manganous nitrate, cobalt chloride, copper sulfate, ferric sulfate are dissolved in successively in the condensed whey and obtain.
5,, it is characterized in that starch suspension is by obtaining starch dissolution in spissated whey solution under the state of cooling according to the method for claim 2.The content of starch in leaf fertilizer is 2.5-4%.
CN87100319A 1986-01-20 1987-01-20 Plant leaf fertilizer and preparation method thereof Pending CN87100319A (en)

Applications Claiming Priority (2)

Application Number Priority Date Filing Date Title
BG8673169A BG44893A1 (en) 1986-01-20 1986-01-20
BG73169 1986-01-20

Publications (1)

Publication Number Publication Date
CN87100319A true CN87100319A (en) 1987-09-09

Family

ID=3916617

Family Applications (1)

Application Number Title Priority Date Filing Date
CN87100319A Pending CN87100319A (en) 1986-01-20 1987-01-20 Plant leaf fertilizer and preparation method thereof

Country Status (10)

Country Link
CN (1) CN87100319A (en)
BG (1) BG44893A1 (en)
CS (1) CS272254B2 (en)
DD (1) DD288054A7 (en)
DE (1) DE3701042A1 (en)
FR (1) FR2593172B1 (en)
GB (1) GB2185472B (en)
HU (1) HUT42252A (en)
NL (1) NL8700105A (en)
YU (1) YU5487A (en)

Cited By (3)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
CN1914137B (en) * 2003-11-20 2011-04-13 康迪特国际有限公司 Biological fertilizer containing whey
CN102835668A (en) * 2012-09-05 2012-12-26 王向华 Method for preparing animal and plant nutrition liquid by using potato cell liquid
CN104557291A (en) * 2014-12-26 2015-04-29 中国热带农业科学院分析测试中心 Production technology of slurry type compound fertilizer

Families Citing this family (6)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
DE3826390C1 (en) * 1988-08-03 1989-11-16 Andreas 2330 Altenhof De Moll Use of whey as a fertiliser
ES2141767T3 (en) * 1992-06-19 2000-04-01 Arthur M Nonomura PROCEDURES AND COMPOSITIONS THAT STIMULATE THE FIXATION OF CARBON IN PLANTS.
US5846908A (en) * 1992-06-19 1998-12-08 Nonomura; Arthur M. Methods and compositions for enhancing plant growth with p-amino- or p-nitro-benzoic acids
IES74258B2 (en) * 1995-12-18 1997-07-16 Dairygold Tech Ltd Growing medium and a process for its manufacture
US6406511B2 (en) 2000-06-14 2002-06-18 Ecoorganics, Inc. Sprayable organic fertilizer
ES2186553B1 (en) * 2001-07-10 2004-09-16 Bioiberica, S.A. COMPOSITION FOR ORNAMENTAL PLANTS.

Family Cites Families (5)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
CH217774A (en) * 1938-12-23 1941-11-15 Ernesto Dr Alberizzi Process for preparing a product for agricultural use.
FR1198105A (en) * 1957-05-04 1959-12-04 Biologically based additive product for fertilizers
US3914438A (en) * 1973-10-03 1975-10-21 Lemmie C Holt Nutrient composition and method for making same
GB1500326A (en) * 1975-08-15 1978-02-08 Ferma Gro Corp Nutrient composition for plants and animals
BG41837A1 (en) * 1985-03-26 1987-09-15 Kostadinov Means for regulating plant growth and development

Cited By (4)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
CN1914137B (en) * 2003-11-20 2011-04-13 康迪特国际有限公司 Biological fertilizer containing whey
CN102835668A (en) * 2012-09-05 2012-12-26 王向华 Method for preparing animal and plant nutrition liquid by using potato cell liquid
CN104557291A (en) * 2014-12-26 2015-04-29 中国热带农业科学院分析测试中心 Production technology of slurry type compound fertilizer
CN104557291B (en) * 2014-12-26 2018-01-05 中国热带农业科学院分析测试中心 A kind of production technology of sludge-type composite fertilizer

Also Published As

Publication number Publication date
NL8700105A (en) 1987-08-17
CS21887A2 (en) 1990-03-14
DE3701042A1 (en) 1987-07-23
CS272254B2 (en) 1991-01-15
DD288054A7 (en) 1991-03-21
HUT42252A (en) 1987-07-28
GB2185472A (en) 1987-07-22
GB8701018D0 (en) 1987-02-18
GB2185472B (en) 1989-11-01
BG44893A1 (en) 1989-03-15
YU5487A (en) 1988-08-31
FR2593172B1 (en) 1990-07-20
FR2593172A1 (en) 1987-07-24

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