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CN2808362Y - Equipment for manufacturing oriental-congealing casting pieces - Google Patents

Equipment for manufacturing oriental-congealing casting pieces Download PDF

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CN2808362Y
CN2808362Y CN 200520090634 CN200520090634U CN2808362Y CN 2808362 Y CN2808362 Y CN 2808362Y CN 200520090634 CN200520090634 CN 200520090634 CN 200520090634 U CN200520090634 U CN 200520090634U CN 2808362 Y CN2808362 Y CN 2808362Y
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equipment
crystallizer
holding furnace
molten pool
crucible
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张健
燕冰川
楼琅洪
陈忠政
朱玉红
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Institute of Metal Research of CAS
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Abstract

The utility model provides equipment for manufacturing oriental-congealing casting pieces. The utility model mainly comprises a smelting chamber, a holding furnace, a crystallizer, wherein a crucible is arranged in the smelting chamber, and the circumference of the crucible is provided with induction heating coils; holes are arranged in the bottom of the crucible and covered through diaphragm plates. The holding furnace is arranged under the smelting chamber, and a casting mold is arranged inside the holding furnace; the circumference of the casting mold is provided with heating elements, and a funnel is arranged above the casting mold; a chassis of the crystallizer underlays the casting mold, and the crystallizer is arranged under the holding furnace and installed on a lifting mechanism; the crystallizer and the holding furnace are connected with a vacuum system. The utility model is characterized in that the crystallizer belongs to an alloy melting bath with low melting points, and a heat insulation layer is arranged on the surface of alloy solution with low melting points. The device has the advantages that the temperature gradient which is generated in the oriental-congealing operation is raised by big percentages, and the temperature gradient can be enhanced to 120-180k/cm from 40-60k/cm of the traditional HRS technology, so the device can make the highest casting piece with the large size of from 35 cm to 40 cm; the production efficiency is enhanced obviously; the utility model solves the problem that metal is easy to react with ceramic molds with high temperatures for the long time; the microsegregation of the alloy oriental-congealing organization is eased, and the alloy thermal treatment time following up is shortened, so the utility model also saves the cost.

Description

一种生产定向凝固铸件用的设备A kind of equipment for producing directionally solidified castings

技术领域technical field

本实用新型涉及一种用于生产定向凝固铸件的设备,尤其涉及一种用于铸造大尺寸定向和单晶铸件(如燃气轮机叶片等)的定向凝固铸造的设备。The utility model relates to a device for producing directional solidification castings, in particular to a device for directional solidification casting of large-size directional and single crystal castings (such as gas turbine blades, etc.).

背景技术Background technique

定向凝固技术可以生产消除横向晶界(定向柱晶)或完全消除晶界(单晶)的金属铸件,与传统铸造方法得到的铸件比较,这些铸件具有更好的纵向机械性能。燃气轮机、航空发动机的静动叶片就是定向凝固技术应用的一个例子。Directional solidification technology can produce metal castings with eliminated transverse grain boundaries (orientated columnar grains) or completely eliminated grain boundaries (single crystals), which have better longitudinal mechanical properties compared with castings obtained by traditional casting methods. Static and moving blades of gas turbines and aero-engines are an example of the application of directional solidification technology.

工业化的定向凝固技术主要是指高速凝固法(HRS),如图1所示,模壳(3)放置在水冷结晶器(6)上,并在保温炉(2)中通过加热元件(1)加热到金属的熔点以上,在模壳中浇铸熔融的金属后,模壳被从保温炉中沿箭头方向拉下,形成定向凝固铸件。定向凝固铸件质量的一个关键决定因素是定向凝固设备在整个定向凝固过程中能达到的温度梯度,如果整个铸件在较高的温度梯度下定向凝固,生产效率就较高,产品的合格率也较高。为加大温度梯度,一些HRS设备在保温炉底部使用了隔热挡板(4),在隔热挡板下使用了水冷环(5),这样使模壳的热量一方面通过热传导向水冷结晶器散失,另一方面通过热辐射向水冷环散失。The industrialized directional solidification technology mainly refers to the high-speed solidification method (HRS). As shown in Figure 1, the formwork (3) is placed on the water-cooled crystallizer (6) and passed through the heating element (1) in the holding furnace (2). After heating above the melting point of the metal and casting the molten metal in the formwork, the formwork is pulled from the holding furnace in the direction of the arrow to form a directionally solidified casting. A key determinant of the quality of directional solidification castings is the temperature gradient that directional solidification equipment can achieve during the entire directional solidification process. If the entire casting is directional solidified under a higher temperature gradient, the production efficiency will be higher and the pass rate of the product will be higher. high. In order to increase the temperature gradient, some HRS equipment uses a heat insulation baffle (4) at the bottom of the holding furnace, and uses a water cooling ring (5) under the heat insulation baffle, so that the heat of the mold shell can be transferred to the water cooling crystallization through heat conduction on the one hand. The device is lost, and on the other hand, it is lost to the water cooling ring through heat radiation.

为得到熔融的合金,一般定向凝固设备都采用感应加热方法,如图1所示,高温合金母合金放置在坩埚(11)中,经感应线圈(12)加热熔化后,通过浇道(13)倾倒入保温炉的模壳中。In order to obtain molten alloy, general directional solidification equipment adopts induction heating method, as shown in Figure 1, the superalloy master alloy is placed in the crucible (11), after being heated and melted by the induction coil (12), it passes through the sprue (13) Pour into the formwork of the holding furnace.

传统的HRS设备由于隔热挡板无法随铸件形状变化而变化,在模壳(3)和隔热挡板(4)之间不可避免地会留下间隙,这会大大降低定向凝固过程的温度梯度;同样,水冷环的冷却效果也受铸件形状的影响;另外,水冷结晶器(6)在定向凝固过程中向下移动,逐渐远离保温炉,通过水冷结晶器的热传导带走的热量越来越少,一般当铸型高度超过7cm时,模壳的热量主要依靠向真空室壁(7)的辐射来带走,因此随铸件长度的增加,HRS设备能达到的温度梯度逐步降低。定向凝固中凝固速度(大致等于水冷结晶器的拉伸速率)、温度梯度与铸件尺寸的关系如图2所示。图中的等轴晶、缩孔、斑点、小角度晶界等都是定向和单晶铸件中常见的缺陷,显然HRS法生产大叶片时,由于设备所能达到的温度梯度很小,生产中只能采用很低的凝固速度(拉伸速率),一方面生产效率极低,另一方面已经接近工艺条件的极限(图中灰色椭圆区),铸件很容易产生缺陷,产品合格率很低。所以,HRS法在生产大尺寸定向和单晶铸件时,成本极高。In the traditional HRS equipment, since the heat insulation baffle cannot change with the shape of the casting, a gap will inevitably be left between the mold shell (3) and the heat insulation baffle (4), which will greatly reduce the temperature of the directional solidification process gradient; similarly, the cooling effect of the water-cooling ring is also affected by the shape of the casting; in addition, the water-cooling crystallizer (6) moves downward during the directional solidification process, gradually away from the holding furnace, and the heat taken away by the heat conduction of the water-cooling crystallizer is getting more and more Generally, when the mold height exceeds 7cm, the heat of the mold shell is mainly taken away by radiation to the vacuum chamber wall (7), so as the length of the casting increases, the temperature gradient that the HRS equipment can achieve gradually decreases. The relationship between solidification speed (approximately equal to the stretching rate of water-cooled crystallizer), temperature gradient and casting size in directional solidification is shown in Figure 2. Equiaxed grains, shrinkage cavities, spots, and small-angle grain boundaries in the figure are all common defects in directional and single crystal castings. Obviously, when producing large blades by HRS method, due to the small temperature gradient that the equipment can achieve, the production Only a very low solidification rate (stretching rate) can be used. On the one hand, the production efficiency is extremely low, and on the other hand, it is close to the limit of the process conditions (the gray ellipse area in the figure), castings are prone to defects, and the product qualification rate is very low. Therefore, the HRS method is extremely costly when producing large-size oriented and single-crystal castings.

发明内容Contents of the invention

本实用新型的目的是提供一种生产定向凝固铸件用的设备,能大幅度提高定向凝固过程中的温度梯度,而且温度梯度在整个定向凝固过程中保持不变,不受铸件尺寸的影响。The purpose of the utility model is to provide a device for producing directional solidification castings, which can greatly increase the temperature gradient in the directional solidification process, and the temperature gradient remains unchanged throughout the directional solidification process without being affected by the size of the castings.

本实用新型提供一种生产定向凝固铸件用的设备,主要包括熔炼室(34)、保温炉(37)、结晶器(40)、升降机构(46)、真空系统(50、51),熔炼室(34)在设备的最上方,熔炼室(34)里有坩埚(32),坩埚(32)四周是感应加热线圈(31),坩埚(32)底上有孔(36),孔(36)用隔片(33)掩盖,保温炉(37)在熔炼室(34)的下面,保温炉(37)里放置铸模(10),四周有加热体(38),铸模(10)上方有漏斗(35),铸模(10)下垫结晶器底盘(58),结晶器(40)在保温炉(37)下面,结晶器(40)装在升降机构(46)上,以控制升降速度,结晶器(40)和保温炉(37)与真空系统(50)相连接,以保持真空,其特征在于:结晶器(40)是低熔点合金熔池,低熔点合金溶液表面上有隔热层(42)。The utility model provides equipment for producing directional solidification castings, which mainly includes a melting chamber (34), a holding furnace (37), a crystallizer (40), a lifting mechanism (46), a vacuum system (50, 51), a melting chamber (34) At the top of the equipment, there is a crucible (32) in the melting chamber (34), surrounded by induction heating coils (31), and there are holes (36) on the bottom of the crucible (32), holes (36) Cover with partition (33), holding furnace (37) is below smelting chamber (34), places mold (10) in holding furnace (37), heating body (38) is arranged around, and funnel (10) is arranged above mold (10) 35), the mold (10) is placed under the crystallizer chassis (58), the crystallizer (40) is under the holding furnace (37), and the crystallizer (40) is installed on the lifting mechanism (46) to control the lifting speed, the crystallizer (40) and holding furnace (37) are connected with vacuum system (50), to keep vacuum, it is characterized in that: crystallizer (40) is low-melting-point alloy melting pool, and there is insulation layer (42) on the surface of low-melting-point alloy solution ).

本实用新型提供的生产定向凝固铸件用的设备,其低熔点合金熔池(40)可以是Sn熔池(40),备有控温系统(41),保持在232~380℃之间。In the equipment for producing directional solidification castings provided by the utility model, the low-melting point alloy molten pool (40) may be a Sn molten pool (40), equipped with a temperature control system (41), which is kept at 232-380°C.

本实用新型提供的生产定向凝固铸件用的设备,其隔热层(42)的形状与铸型形状相适应,其材料是耐高温、热传导系数低、高温下与铸型材料不反应的材料。厚度为0.1~10cm。The utility model provides equipment for producing directional solidification castings, the shape of the heat insulating layer (42) is adapted to the shape of the mold, and the material is high temperature resistant, low thermal conductivity, and does not react with the mold material at high temperature. The thickness is 0.1-10cm.

本实用新型提供的生产定向凝固铸件用的设备,其低熔点合金熔池(40)里自上伸下搅拌器(44)。The equipment for producing directional solidified castings provided by the utility model has an agitator (44) extending from top to bottom in the molten pool of low-melting alloy (40).

本实用新型提供的生产定向凝固铸件用的设备的优点包括:The advantages of the equipment for producing directional solidification castings provided by the utility model include:

1、定向凝固中的温度梯度大幅度提高,温度梯度可从传统HRS工艺40~60K/cm提高到120~180K/cm。可以制备最高35~40cm的大尺寸铸件,在定向凝固中温度梯度与铸件尺寸无关。1. The temperature gradient in directional solidification is greatly increased, and the temperature gradient can be increased from 40-60K/cm in the traditional HRS process to 120-180K/cm. Large-size castings up to 35-40 cm can be prepared, and the temperature gradient has nothing to do with the size of the casting during directional solidification.

2、定向凝固中拉伸速率快,例如7~20mm/min,生产效率明显提高。2. Fast stretching rate in directional solidification, such as 7-20mm/min, the production efficiency is obviously improved.

3、解决金属在长时间高温下容易与陶瓷铸型发生反应的问题。3. Solve the problem that the metal is easy to react with the ceramic mold under long-term high temperature.

4、合金定向凝固组织微观偏析减轻,缩短了合金后续热处理时间,节约成本。4. The micro-segregation of the directional solidification structure of the alloy is reduced, which shortens the subsequent heat treatment time of the alloy and saves costs.

附图说明Description of drawings

图1为传统HRS工艺制备定向凝固铸件示意图。Figure 1 is a schematic diagram of the directionally solidified casting prepared by the traditional HRS process.

图2为定向凝固工艺中温度梯度、拉伸速率与定向凝固铸件尺寸、缺陷关系示意图。Fig. 2 is a schematic diagram of the relationship between temperature gradient, stretching rate, dimension and defect of directional solidification casting in directional solidification process.

图3为本实用新型结构示意图。Fig. 3 is a structural schematic diagram of the utility model.

具体实施方式Detailed ways

实施例1Example 1

一种生产定向凝固铸件用的设备的结构如图3所示,主要包括熔炼室(34)、保温炉、结晶器、升降机构、真空系统(50、51)。A structure of equipment for producing directional solidification castings is shown in Figure 3, mainly including a melting chamber (34), a holding furnace, a crystallizer, a lifting mechanism, and a vacuum system (50, 51).

上部是感应熔炼真空室熔炼室(34),熔炼室(34)里有坩埚(32),坩埚(32)四周是感应线圈(31),坩埚(32)底上有孔(36),孔(36)用隔片(33)掩盖。The upper part is an induction melting vacuum chamber melting chamber (34). There is a crucible (32) in the melting chamber (34). The crucible (32) is surrounded by induction coils (31). There are holes (36) on the bottom of the crucible (32), and the holes ( 36) Cover with spacer (33).

铸模(10)、铸模保温炉(37)和低熔点金属Sn熔池(40)等安装在熔炼室(34)下方的下部真空室里,与真空泵系统包括机械泵、罗茨泵和增压泵相连。铸模(10)置于保温炉里,四周有加热体(38),铸模(10)上方有漏斗(35),铸模(10)下垫底盘(58)。The casting mold (10), the casting mold holding furnace (37) and the low melting point metal Sn molten pool (40) etc. are installed in the lower vacuum chamber below the smelting chamber (34), and the vacuum pump system includes a mechanical pump, a Roots pump and a booster pump connected. Casting mold (10) is placed in holding furnace, has heating body (38) all around, and funnel (35) is arranged on casting mold (10) top, and casting mold (10) underlays chassis (58).

低熔点金属熔池(40)用德国SIEMENS公司控温系统(41)保持在232~380℃之间,合金溶液面上有隔热层(42);低熔点合金熔池(40)里备有搅拌器(44)。The low-melting point metal molten pool (40) is kept between 232~380 DEG C with the temperature control system (41) of German SIEMENS company, and there is a thermal insulation layer (42) on the surface of the alloy solution; Stirrer (44).

下部真空室外设有铸型的拉伸驱动机构控制结晶器底盘(58)的升降速度。The lower vacuum chamber is equipped with a stretching drive mechanism of the mold to control the lifting speed of the crystallizer chassis (58).

采用低熔点金属Sn液态冷却的方法,使铸型接触低熔点合金后迅速冷却;低熔点合金的温度通过控温机构(41)控制,当大型铸件进入低熔点合金熔池(40),使低熔点金属熔池(40)温度升高时,可通过控温机构冷却低熔点熔池温度;低熔点金属表面有一层隔热层(42),当铸型降入低熔点金属熔池(40)时,隔热层(42)保证铸型保温炉的热量不会辐射散失,保证低熔点金属表面不会因热辐射而升高温度;据此:The method of liquid cooling of low-melting-point metal Sn is adopted to make the mold cool rapidly after contacting the low-melting-point alloy; the temperature of the low-melting-point alloy is controlled by the temperature control mechanism (41), and when a large casting enters the low-melting-point alloy molten pool (40), the low When the temperature of the melting point metal molten pool (40) rises, the temperature of the low melting point molten pool can be cooled by the temperature control mechanism; there is a layer of heat insulation layer (42) on the surface of the low melting point metal, and when the mold falls into the low melting point metal molten pool (40) , the heat insulation layer (42) ensures that the heat of the mold holding furnace will not be lost by radiation, and that the surface of the low melting point metal will not increase in temperature due to thermal radiation; accordingly:

1、定向凝固中的温度梯度大幅度提高,温度梯度可从传统HRS工艺40-60K/cm提高到120-180K/cm。可以制备最高35-40cm的大尺寸铸件。温度梯度与铸件尺寸无关。1. The temperature gradient in directional solidification is greatly increased, and the temperature gradient can be increased from 40-60K/cm in the traditional HRS process to 120-180K/cm. Large size castings up to 35-40cm can be prepared. The temperature gradient is independent of casting size.

2、拉伸速率快,例如7-20mm/min,生产效率明显提高。2. The drawing rate is fast, such as 7-20mm/min, and the production efficiency is obviously improved.

3、解决金属在长时间高温下容易与陶瓷铸型发生反应的问题。3. Solve the problem that the metal is easy to react with the ceramic mold under long-term high temperature.

4、合金定向凝固组织微观偏析减轻,缩短了合金后续热处理时间,节约成本。4. The micro-segregation of the directional solidification structure of the alloy is reduced, which shortens the subsequent heat treatment time of the alloy and saves costs.

5、采用低熔点金属Sn液态冷却的方法,可以通过快速淬火(最快5m/s)中断稳态定向凝固,保留高温合金糊状区形貌,从而得到定向凝固中枝晶生长形态、枝晶偏析、固液界面形态等大量信息,对材料科学研究意义重大。5. Using the liquid cooling method of low-melting-point metal Sn, the steady-state directional solidification can be interrupted by rapid quenching (up to 5m/s), and the morphology of the superalloy mushy zone can be retained, so as to obtain the dendrite growth form and dendrite during directional solidification. A large amount of information such as segregation and solid-liquid interface morphology is of great significance to material science research.

实施例2Example 2

一种生产定向凝固铸件用的设备的结构基本上与实施例1相同,区别在于:低熔点合金熔池(40)可以通过滑道(45)拉出或推入真空室,可以将本设备改为传统的HRS设备。The structure of a device for producing directional solidification castings is basically the same as that of Embodiment 1, the difference is that the molten pool of low-melting alloy (40) can be pulled out or pushed into the vacuum chamber through the slideway (45), and the device can be changed to For traditional HRS equipment.

本设备也可以将传统HRS设备的水冷结晶器,改为低熔点金属熔池(40)而获得。This equipment can also be obtained by changing the water-cooled crystallizer of traditional HRS equipment into a low-melting-point metal molten pool (40).

Claims (10)

1、一种生产定向凝固铸件用的设备,主要包括熔炼室(34)、保温炉(37)、结晶器(40)、升降机构(46)、真空系统(50),熔炼室(34)在设备的最上方,熔炼室(34)里有坩埚(32),坩埚(32)四周是感应线圈(31),坩埚(32)底上有孔(36),孔(36)用隔片(33)掩盖,保温炉(37)在熔炼室(34)的下面,保温炉(37)里放置铸模(10),四周有加热体(38),铸模(10)上方有漏斗(35),铸模(10)下垫底盘(58),结晶器(40)在保温炉(37)下面,结晶器(40)装在升降机构(46)上,结晶器(40)和保温炉(37)与真空系统(50)相连接,其特征在于:结晶器(40)是低熔点合金熔池,低熔点合金溶液面上有隔热层(42)。1. An equipment for producing directional solidified castings, mainly comprising a smelting chamber (34), a holding furnace (37), a crystallizer (40), a lifting mechanism (46), a vacuum system (50), and the smelting chamber (34) in At the top of the equipment, there is a crucible (32) in the smelting chamber (34), and the crucible (32) is surrounded by induction coils (31), and there is a hole (36) at the bottom of the crucible (32), and the hole (36) uses a spacer (33 ) to cover up, the holding furnace (37) is below the smelting chamber (34), and the casting mold (10) is placed in the holding furnace (37), and there is a heating body (38) around it, and there is a funnel (35) above the casting mold (10), and the casting mold ( 10) Underlay the chassis (58), the crystallizer (40) is under the holding furnace (37), the crystallizer (40) is installed on the lifting mechanism (46), the crystallizer (40) and the holding furnace (37) are connected with the vacuum system (50) are connected, and it is characterized in that: the crystallizer (40) is a low-melting-point alloy molten pool, and a heat-insulating layer (42) is arranged on the surface of the low-melting-point alloy solution. 2、按照权利要求1所述的生产定向凝固铸件用的设备,其特征在于:所述低熔点合金熔池(40)是Sn熔池。2. The equipment for producing directionally solidified castings according to claim 1, characterized in that: the low-melting point alloy molten pool (40) is a Sn molten pool. 3、按照权利要求2所述的生产定向凝固铸件用的设备,其特征在于:所述Sn熔池(40)备有控温系统(41)。3. The equipment for producing directionally solidified castings according to claim 2, characterized in that: said Sn molten pool (40) is equipped with a temperature control system (41). 4、按照权利要求1所述的生产定向凝固铸件用的设备,其特征在于:所述隔热层(42)的形状与铸型形状相适应。4. The equipment for producing directionally solidified castings according to claim 1, characterized in that: the shape of the heat insulating layer (42) is adapted to the shape of the mold. 5、按照权利要求1~4之一所述的生产定向凝固铸件用的设备,其特征在于:所述隔热层(42)的材料是耐高温、热传导系数低、高温下与铸型材料不反应的材料。5. The equipment for producing directional solidification castings according to any one of claims 1 to 4, characterized in that: the material of the heat insulation layer (42) is high temperature resistant, has low thermal conductivity, and is incompatible with the mold material at high temperature. React material. 6、按照权利要求1~4之一所述的生产定向凝固铸件用的设备,其特征在于:所述隔热层的厚度为0.1~10cm。6. The equipment for producing directionally solidified castings according to any one of claims 1-4, characterized in that: the thickness of the heat insulation layer is 0.1-10 cm. 7、按照权利要求5所述的生产定向凝固铸件用的设备,其特征在于:所述隔热层的厚度为0.1~10cm。7. The equipment for producing directionally solidified castings according to claim 5, characterized in that: the thickness of the heat insulation layer is 0.1-10 cm. 8、按照权利要求1~4之一所述的生产定向凝固铸件用的设备,其特征在于:所述低熔点合金熔池(40)里自上伸下搅拌器(44)。8. The equipment for producing directionally solidified castings according to any one of claims 1-4, characterized in that: the stirrer (44) extends from top to bottom in the low melting point alloy molten pool (40). 9、按照权利要求5所述的生产定向凝固铸件用的设备,其特征在于:所述低熔点合金熔池(40)里自上伸下搅拌器(44)。9. The equipment for producing directionally solidified castings according to claim 5, characterized in that: a stirrer (44) extends from top to bottom in the low melting point alloy molten pool (40). 10、按照权利要求7所述的生产定向凝固铸件用的设备,其特征在于:所述低熔点合金熔池(40)里自上伸下搅拌器(44)。10. The equipment for producing directionally solidified castings according to claim 7, characterized in that: the agitator (44) extends from top to bottom in the low melting point alloy molten pool (40).
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