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CN2553882Y - Powder catalyst structure of synthetic high-grade diamond - Google Patents

Powder catalyst structure of synthetic high-grade diamond Download PDF

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Publication number
CN2553882Y
CN2553882Y CN 02268104 CN02268104U CN2553882Y CN 2553882 Y CN2553882 Y CN 2553882Y CN 02268104 CN02268104 CN 02268104 CN 02268104 U CN02268104 U CN 02268104U CN 2553882 Y CN2553882 Y CN 2553882Y
Authority
CN
China
Prior art keywords
synthetic
stem
catalyst structure
diamond
pyrophyllite
Prior art date
Legal status (The legal status is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the status listed.)
Expired - Lifetime
Application number
CN 02268104
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Chinese (zh)
Inventor
卢灿华
胡来运
李玉顺
张兴伍
李金钊
王国成
孟庆伟
Current Assignee (The listed assignees may be inaccurate. Google has not performed a legal analysis and makes no representation or warranty as to the accuracy of the list.)
Zhongnan Diamond Co Ltd
Original Assignee
Henan Zhongnan Industrial Co ltd
Priority date (The priority date is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the date listed.)
Filing date
Publication date
Application filed by Henan Zhongnan Industrial Co ltd filed Critical Henan Zhongnan Industrial Co ltd
Priority to CN 02268104 priority Critical patent/CN2553882Y/en
Application granted granted Critical
Publication of CN2553882Y publication Critical patent/CN2553882Y/en
Anticipated expiration legal-status Critical
Expired - Lifetime legal-status Critical Current

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Abstract

The utility model provides a powder accelerant structure of synthesizing high grade diamond to the technical field of synthesis and preparation of diamond. The utility model is mainly characterized in that a dolomite liner tube is nested in the inner wall of a sleeve barrel cavity which is synthesized by pyrophyllite blocks, the central part of the sleeve barrel cavity of pyrophyllite blocks is arranged with a graphitic synthetic button stem, the external surface of the graphitic synthetic button stem is arranged with an isolated layer, the upper end and the lower end are arranged with electric sheet metals and dolomite rings, wherein the isolated layer and the electric sheet metals are separated into a cavity body through the dolomite rings, a heating plate is arranged in the cavity body, and electric circles are arranged on two ends of the inner wall of the sleeve barrel of the pyrophyllite blocks and are connected with the electric sheet metals. Compared with prior art, due to the adoption of the utility model, the indexes on monocrystal intact rate, high strength ratio and impact strength of synthetical diamond are all improved over once, and the synthesizing power is relatively low. Compared with flaky accelerant and the cavity body, electric power consumption can be saved by one third to one half.

Description

A kind of powder catalyst structure of synthetic high grade diamond
Technical field:
The utility model belongs to the diamond synthesis technical field, is a kind of powder catalyst structure of synthetic high grade diamond.
Background technology:
In technique known, the catalyst that diamond synthesis is used is the sheet alloy material, carbon source is the graphite flake that processes after electrographiteization, catalyst, graphite flake clean up and drying after alternately pack in the synthetic chamber of pyrophyllite, conducting steel ring is loaded onto at two ends, more than 10 hours, can on cubic hinge press, go out diamond through 140 ℃ ± 5 ℃ insulations through high temperature, high pressure synthetically grown.The problem that the slice catalyst diamond synthesis exists is: diamond grit is 40/45~70/80, and color is a yellow green, and underbead crack, bubble are more, and poor transparency has hoary hair's diamond, and resistance to compression, impact strength are very low, and output is lower, and power consumption is big.
Summary of the invention:
The purpose of this utility model provides and a kind ofly can improve resistance to compression, shock resistance, and quality is good, output is high, the powder catalyst structure of the synthetic high grade diamond of little power consumption.
Realize that the technical scheme that the purpose of this utility model is taked is improved on the basis of original slice catalyst diamond synthesis, it has the synthetic sleeve chamber of pyrophyllite in lumps, conductive ring, graphite flake, its main feature is: at pyrophyllite in lumps sleeve cavity wall, be nested with the dolomite bushing pipe, the centre in pyrophyllite in lumps sleeve chamber is provided with synthetic stem stem, the outer surface of synthetic stem stem is provided with metallic spacer, the upper and lower end parts of separation layer is provided with conductive metal sheet and white clouds stone ring, wherein, be divided into cavity by the white clouds stone ring between separation layer and the conductive metal sheet, the built-in heating sheet that is placed with of cavity, conductive ring is arranged on pyrophyllite in lumps sleeve lining two ends, and contacts with conductive metal sheet.
According to the powder catalyst structure that is used for synthetic high grade diamond that such scheme is made, its synthetic diamond grit is 40/45~45/50, and granularity is more concentrated, color is golden yellow, underbead crack, bubble seldom, transparency is good, no hoary hair's diamond, per unit area yield is higher.Compared with prior art, adopt the utility model structure, synthetic diamond is all improved more than 1 times in monocrystalline percentage of head rice, high-strength ratio, impact strength index, synthetic power is lower, compares with cavity with slice catalyst, and power consumption saves 1/3~1/2.
Utilize accompanying drawing to further describe embodiment of the present utility model below.
Description of drawings:
Fig. 1 is a general assembly structural representation of the present utility model.
The specific embodiment:
Referring to Fig. 1, the utlity model has the synthetic sleeve chamber 1 of pyrophyllite in lumps, conductive ring 9, heating plate 3, at pyrophyllite in lumps sleeve chamber 1 inwall, be nested with dolomite bushing pipe 4, the centre in pyrophyllite in lumps sleeve chamber is provided with synthetic stem stem 5, synthetic stem stem 5 is by 35% catalytic alloy powder, 65% graphite powder mixes by doing, granulation, suppression process and constitute the synthetic stem stem of graphite, the outer surface of synthetic stem stem 5 is provided with metallic spacer, this separation layer is to be made of sheet iron strip 6 and iron plate 7, the upper and lower end parts of synthetic stem stem is provided with conductive metal sheet 8 and white clouds stone ring 2, conductive metal sheet can adopt stainless steel substrates, wherein, be divided into cavity by white clouds stone ring 2 between iron plate 7 and the conductive metal sheet 8, the built-in heating sheet 3 that is placed with of cavity, heating sheet 3 is to be made of graphite flake, conductive ring 9 is arranged on 1 inwall two ends, pyrophyllite in lumps sleeve chamber, and contacts with conductive metal sheet 8.After pressing the said structure assembling, through 130 ℃ ± 5 ℃ insulations 36 hours, synthetic high grade diamond promptly was available on the machine.

Claims (6)

1, a kind of powder catalyst structure of synthetic high grade diamond, has the synthetic sleeve chamber [1] of pyrophyllite in lumps, conductive ring [9], graphite flake [3], it is characterized in that: at pyrophyllite in lumps sleeve chamber [1] inwall, be nested with dolomite bushing pipe [4], the centre in pyrophyllite in lumps sleeve chamber [1] is provided with synthetic stem stem [5], the upper and lower end parts of synthetic stem stem [5] is provided with conductive metal sheet [8] and white clouds stone ring [2], conductive ring [9] is arranged on pyrophyllite in lumps sleeve [1] inwall two ends, and contacts with conductive metal sheet [8].
2, the powder catalyst structure of synthetic high grade diamond according to claim 1 is characterized in that: synthetic stem stem [5] by 35% catalytic alloy powder, 65% graphite powder mix by doing, granulation, suppression process constitute the synthetic stem stem of graphite.
3, the last catalyst structure of synthetic high grade diamond powder according to claim 1 is characterized in that: the outer surface of synthetic stem stem [5] is provided with separation layer, is to be made of sheet iron strip [6] and iron plate [7].
4, according to the powder catalyst structure of claim 1 or 3 described synthetic high grade diamonds, it is characterized in that: be divided into cavity by white clouds stone ring [2] between iron plate [7] and the conductive metal sheet [8], the built-in heating sheet [3] that is placed with of cavity.
5, according to the powder catalyst structure of claim 1 or 4 described synthetic high grade diamonds, it is characterized in that: heating sheet [3] is to be made of graphite flake.
6, according to the powder catalyst structure of claim 1 or 4 described synthetic high grade diamonds, it is characterized in that: conductive metal sheet [8] adopts stainless steel substrates.
CN 02268104 2002-07-02 2002-07-02 Powder catalyst structure of synthetic high-grade diamond Expired - Lifetime CN2553882Y (en)

Priority Applications (1)

Application Number Priority Date Filing Date Title
CN 02268104 CN2553882Y (en) 2002-07-02 2002-07-02 Powder catalyst structure of synthetic high-grade diamond

Applications Claiming Priority (1)

Application Number Priority Date Filing Date Title
CN 02268104 CN2553882Y (en) 2002-07-02 2002-07-02 Powder catalyst structure of synthetic high-grade diamond

Publications (1)

Publication Number Publication Date
CN2553882Y true CN2553882Y (en) 2003-06-04

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Family Applications (1)

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CN 02268104 Expired - Lifetime CN2553882Y (en) 2002-07-02 2002-07-02 Powder catalyst structure of synthetic high-grade diamond

Country Status (1)

Country Link
CN (1) CN2553882Y (en)

Cited By (3)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
CN100444944C (en) * 2004-10-29 2008-12-24 郑州人造金刚石及制品工程技术研究中心 Medium material for diamond synthesis and medium constituted therefrom
CN101890320A (en) * 2010-07-29 2010-11-24 郑州人造金刚石及制品工程技术研究中心有限公司 Bidirectional pressing diamond synthesizing column
CN107051334A (en) * 2017-06-27 2017-08-18 中南钻石有限公司 For synthesizing the synthesis block structure of IIa type diamonds and the synthetic method of IIa type diamonds

Cited By (4)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
CN100444944C (en) * 2004-10-29 2008-12-24 郑州人造金刚石及制品工程技术研究中心 Medium material for diamond synthesis and medium constituted therefrom
CN101890320A (en) * 2010-07-29 2010-11-24 郑州人造金刚石及制品工程技术研究中心有限公司 Bidirectional pressing diamond synthesizing column
CN107051334A (en) * 2017-06-27 2017-08-18 中南钻石有限公司 For synthesizing the synthesis block structure of IIa type diamonds and the synthetic method of IIa type diamonds
CN107051334B (en) * 2017-06-27 2020-05-26 中南钻石有限公司 Synthetic block structure for synthesizing type IIa diamond and method for synthesizing type IIa diamond

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Legal Events

Date Code Title Description
C14 Grant of patent or utility model
GR01 Patent grant
ASS Succession or assignment of patent right

Owner name: NANYANG SINO-SOUTH AFRICAN DIAMOND COMPANY LIMITE

Free format text: FORMER OWNER: HENAN ZHONGNAN INDUSTRIAL CO., LTD.

Effective date: 20080801

C41 Transfer of patent application or patent right or utility model
TR01 Transfer of patent right

Effective date of registration: 20080801

Address after: Nanyang City, Henan Province Town South Gao Gou Cun in Fangcheng County Guangyang company hospital, zip code: 473200

Patentee after: Nanyang Zhongnan Diamond Co., Ltd.

Address before: Fangcheng County of Henan Province, P.O. Box 101, Henan Zhongnan industry limited liability company, zip code: 473200

Patentee before: Nanyang Zhongnan Diamond Co., Ltd.

ASS Succession or assignment of patent right

Owner name: ZHONGNAN DIAMOND CO., LTD.

Free format text: FORMER OWNER: NANYANG SINO-SOUTH AFRICAN DIAMOND COMPANY LIMITED

Effective date: 20091127

C41 Transfer of patent application or patent right or utility model
TR01 Transfer of patent right

Effective date of registration: 20091127

Address after: Fangcheng County of Henan Province, box 101, postal code: 473200

Patentee after: Zhongnan Diamond Co., Ltd.

Address before: Nanyang City, Henan Province Town South Gao Gou Cun in Fangcheng County Guangyang company hospital, zip code: 473200

Patentee before: Nanyang Zhongnan Diamond Co., Ltd.

C17 Cessation of patent right
CX01 Expiry of patent term

Expiration termination date: 20120702

Granted publication date: 20030604